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171753-74-5

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Basic Information
CAS No.: 171753-74-5
Name: Morpholine, 2,6-diMethyl-, (2R,6R)-
Article Data: 4
Molecular Structure:
Molecular Structure of 171753-74-5 (Morpholine, 2,6-diMethyl-, (2R,6R)-)
Formula: C6H13NO
Molecular Weight: 115.175
Synonyms: Morpholine, 2,6-diMethyl-, (2R,6R)-;(2R,6R)-2,6-Dimethylmorpholine;(2R-trans)-2,6-Dimethylmorpholine
Density: 0.862
Boiling Point: 147℃
Flash Point: 49℃
PSA: 21.26000
LogP: 0.71200
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Synthetic route
171753-77-8

(2R,6R)-4-Benzyl-2,6-dimethyl-morpholine

171753-74-5

(2R,6R)-2,6-dimethylmorpholine

Conditions
ConditionsYield
With hydrogen; acetic acid; palladium on activated charcoal In methanol96.6%
With hydrogen; acetic acid; palladium on activated charcoal In methanol under 760 Torr; for 16h; Ambient temperature;84%

C6H13NO*C8H8O3

171753-74-5

(2R,6R)-2,6-dimethylmorpholine

Conditions
ConditionsYield
Stage #1: C6H13NO*C8H8O3 With hydrogenchloride In water pH=1.5;
Stage #2: With sodium hydroxide In water pH=14;		78%
171753-76-7

(R)-2-((R)-2-Hydroxy-1-methyl-ethoxy)-propan-1-ol

171753-74-5

(2R,6R)-2,6-dimethylmorpholine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 98 percent / pyridine / 0 deg C to room t., 4 h
2: 97.6 percent / dioxane / 12.5 h / Heating
3: 96.6 percent / H2, AcOH / 10percent Pd/c / methanol
View Scheme
Multi-step reaction with 3 steps
1: 94 percent / pyridine / 4 h / 0 - 20 °C
2: 85 percent / dioxane / Heating
3: 84 percent / H2, AcOH / 5percent Pd/C / methanol / 16 h / 760 Torr / Ambient temperature
View Scheme
171561-11-8

Methanesulfonic acid (R)-2-((R)-2-methanesulfonyloxy-1-methyl-ethoxy)-propyl ester

171753-74-5

(2R,6R)-2,6-dimethylmorpholine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 97.6 percent / dioxane / 12.5 h / Heating
2: 96.6 percent / H2, AcOH / 10percent Pd/c / methanol
View Scheme
Multi-step reaction with 2 steps
1: 85 percent / dioxane / Heating
2: 84 percent / H2, AcOH / 5percent Pd/C / methanol / 16 h / 760 Torr / Ambient temperature
View Scheme
171753-75-6

R,R-dilactic acid diethyl ester

171753-74-5

(2R,6R)-2,6-dimethylmorpholine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 97 percent / LiAlH4 / diethyl ether / 0.5 h / Heating
2: 94 percent / pyridine / 4 h / 0 - 20 °C
3: 85 percent / dioxane / Heating
4: 84 percent / H2, AcOH / 5percent Pd/C / methanol / 16 h / 760 Torr / Ambient temperature
View Scheme
171753-74-5

(2R,6R)-2,6-dimethylmorpholine

3,7-dichloro-6-fluorobenzo[d]isoxazole-5-carbaldehyde

3,7-dichloro-6-((2R,6R)-2,6-dimethylmorpholino)benzo[d]isoxazole-5-carbaldehyde

Conditions
ConditionsYield
With potassium carbonate In water for 6h; Reflux;100%
With potassium carbonate In water for 6h; Reflux;100%
171753-74-5

(2R,6R)-2,6-dimethylmorpholine

1224944-77-7

5-chloropyrazolo[1,5-a]pyrimidine-3-carboxylic acid ethyl ester

ethyl 5-[(2R,6R)-2,6-dimethylmorpholin-4-yl]pyrazolo[1,5-a]pyrimidine-3-carboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 60℃; for 16h; Inert atmosphere;96%
171753-74-5

(2R,6R)-2,6-dimethylmorpholine

27996-87-8

2-fluoro-5-nitrobenzaldehye

1135561-41-9

2-[(2R,6R)-2,6-dimethylmorpholin-4-yl]-5-nitrobenzaldehyde

Conditions
ConditionsYield
With triethylamine In acetonitrile for 22h; Inert atmosphere; Reflux;93%
171753-74-5

(2R,6R)-2,6-dimethylmorpholine

(R)-3-(6,7-difluoro-5-formylbenzo[d]isoxazol-3-yl)-N,N-dimethyl-2-oxooxazolidine-4-carboxamide

(R)-3-(6-((2R,6R)-2,6-dimethylmorpholino)-7-fluoro-5-formylbenzo[d]isoxazol-3-yl)-N,N-dimethyl-2-oxooxazolidine-4-carboxamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 80℃; for 16h;92%
171753-74-5

(2R,6R)-2,6-dimethylmorpholine

(R)-6,7-difluoro-3-(2-oxo-5-((trifluoromethoxy)methyl)thiazolidin-3-yl)benzo[d]isoxazole-5-carbaldehyde

6-((2R,6R)-2,6-dimethylmorpholino)-7-fluoro-3-((R)-2-oxo-5-((trifluoromethoxy)methyl)thiazolidin-3-yl)benzo[d]isoxazole-5-carbaldehyde

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 90℃; for 12h;91%
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