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1722-12-9

Basic Information
CAS No.: 1722-12-9
Name: 2-Chloropyrimidine
Article Data: 42
Cas Database
Molecular Structure:
Molecular Structure of 1722-12-9 (2-Chloropyrimidine)
Formula: C4H3ClN2
Molecular Weight: 114.534
Synonyms: 2 Chloro Pyridine;2-Chlorpyrimidin;2-Chloro-4-deoxyuracil;2-Chloropyrimidine D001;Pyrimidine, 2-chloro-;
EINECS: 217-020-2
Density: 1.303 g/cm3
Melting Point: 63-66 °C(lit.)
Boiling Point: 199.2 °C at 760 mmHg
Flash Point: 109.2 °C
Solubility: Slightly soluble in water. 33.3 mg soluble in 1 mL of alcohol.
Appearance: yellowish to pale orange crystals or cryst. powder
Hazard Symbols: HarmfulXn,IrritantXi
Risk Codes: 22-36-36/38-36/37/38
Safety: 26-37/39-36
Transport Information: N/A
PSA: 25.78000
LogP: 1.13000
Synthetic route
557-01-7

2-hydroxypyrimidine

1722-12-9

2-chloropyrimidine

Conditions
ConditionsYield
With trichlorophosphate Chlorination;70%
131242-36-9

2-sulfanylpyrimidine

1722-12-9

2-chloropyrimidine

Conditions
ConditionsYield
Stage #1: 2-sulfanylpyrimidine With trichloroisocyanuric acid; water; benzyltrimethylammonium chloride In acetonitrile at -30 - -25℃; for 0.5h;
Stage #2: With isobutylamine In acetonitrile Further stages.;
70%
With hydrogenchloride; sodium hypochlorite In dichloromethane; water
With thionyl chloride; dihydrogen peroxide In water; acetonitrile at 25℃;
1003845-06-4

(2-chloropyrimidin-5-yl)boronic acid

1722-12-9

2-chloropyrimidine

Conditions
ConditionsYield
With 2-bromo-pyridine; tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; toluene Reflux;65%
100-99-2

triisobutylaluminum

32779-36-5

5-Bromo-2-chloropyrimidine

A

1722-12-9

2-chloropyrimidine

B

2-chloro-5-isobutylpyrimidine

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 24h; Heating;A 30%
B 50%
97-93-8

triethylaluminum

32779-36-5

5-Bromo-2-chloropyrimidine

A

1722-12-9

2-chloropyrimidine

B

111196-81-7

2-chloro-5-ethylpyrimidine

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 24h; Heating;A 30%
B 42%
3934-20-1

2,6-Dichloropyrimidine

97-93-8

triethylaluminum

A

1722-12-9

2-chloropyrimidine

B

188707-99-5

2-chloro-4-ethylpyrimidine

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 24h; Heating;A 25%
B 37%
109-12-6

2-aminopyrimidine

1722-12-9

2-chloropyrimidine

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite In water at -15 - 0℃; for 2.25h;34%
With hydrogenchloride; sodium nitrite
With hydrogenchloride; zinc(II) chloride; sodium nitrite In dichloromethane; water
With hydrogenchloride; zinc(II) chloride; sodium nitrite In dichloromethane; water
With hydrogenchloride; copper dichloride; sodium nitrite In dichloromethane
3934-20-1

2,6-Dichloropyrimidine

1722-12-9

2-chloropyrimidine

Conditions
ConditionsYield
With zinc
With potassium acetate; palladium diacetate; bis(pinacol)diborane; tricyclohexylphosphine In 1,4-dioxane at 110℃; for 0.166667h; Inert atmosphere;
With hydrogen In methanol; ethanol at 20℃;
38353-09-2

2-pyrimidinone hydrochloride

1722-12-9

2-chloropyrimidine

Conditions
ConditionsYield
With phosphorus pentachloride; trichlorophosphate
With trichlorophosphate
930-36-9

1-methyl-1H-pyrazole

67-66-3

chloroform

A

4513-94-4

1H-pyrrole-2-carbonitrile

B

1722-12-9

2-chloropyrimidine

C

51269-82-0

5-chloronicotinonitrile

Conditions
ConditionsYield
at 550 - 555℃; Yield given. Title compound not separated from byproducts;
at 550 - 555℃; Title compound not separated from byproducts;
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Chemistry

2-Chloropyrimidine is the chemical compound with the formula C4H3ClN2.Its molecular weight is 114.53.It is  white crystalline.
EINECS  217-020-2
Molecular Structure:
Melting point:66 oC
Boiling point:75-76 oC (10 mmHg)
Flash point:98 oC
Storage temp. : Refrigerator
Sensitive : Moisture Sensitive

Uses

2-Chloropyrimidine is the intermediate of Medicine and 2-Chloropyrimidine also is the  intermediate of pesticide

Safety Profile

2-Chloropyrimidine's Hazard Symbols: Xi
2-Chloropyrimidine's Risk Codes:
36/38:Irritating to eyes and skin 
2-Chloropyrimidine's Safety Description:
26:In case of contact with eyes, rinse immediately with plenty of WATER and seek medical advice 
37/39:Wear suitable gloves and eye/face protection 

Standards and Recommendations

Loss on drying:≤0.3
Content:≥98%