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17447-35-7

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Basic Information
CAS No.: 17447-35-7
Name: (+)-4'-CHLOROTARTRANILIC ACID
Article Data: 2
Molecular Structure:
Molecular Structure of 17447-35-7 ((+)-4'-CHLOROTARTRANILIC ACID)
Formula: C10H10 Cl N O5
Molecular Weight: 259.646
Synonyms: Butanoicacid, 4-[(4-chlorophenyl)amino]-2,3-dihydroxy-4-oxo-, [R-(R*,R*)]-; Tartranilicacid, 4'-chloro-, (2R,3R)-(+)- (8CI); L-Tartaric acid p-chloroanilide
Density: 1.644g/cm3
Melting Point: 193 °C
Boiling Point: 609.1°Cat760mmHg
Flash Point: 322.2°C
Risk Codes: 36/37/38
Safety:
Risk Statements 36/37/38
Safety Statements 26-36/37/39
PSA: 106.86000
LogP: 0.15790
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Synthetic route
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17447-35-7

(R,R)-(+)-4-chlorotartranilic acid

Conditions
ConditionsYield
In dichloromethane for 15h; Heating;68%
253168-94-4

2-(3-ethoxy-4-methoxyphenyl)-1-(methylsulfonyl)eth-2-ylamine

17447-35-7

(R,R)-(+)-4-chlorotartranilic acid

C12H19NO4S*C10H10ClNO5

Conditions
ConditionsYield
With hydrogenchloride In water at 60 - 70℃; Solvent; Resolution of racemate; Heating;92%
6859-99-0

3-hydroxypiperazine

17447-35-7

(R,R)-(+)-4-chlorotartranilic acid

(2R,3R)-N-(4-Chloro-phenyl)-2,3-dihydroxy-succinamic acid; compound with (R)-piperidin-3-ol

Conditions
ConditionsYield
In ethanol at 40℃;74%
943964-30-5

(+/-)-5-(4-amino-3-methylphenyl)-8-methyl-8,9-dihydro-7H-1,3-dioxolo[4,5-h][2,3]benzodiazepine

17447-35-7

(R,R)-(+)-4-chlorotartranilic acid

943964-32-7

(S)-(-)-5-(4-amino-3-methylphenyl)-8-methyl-8,9-dihydro-7H-1,3-dioxolo[4,5-h][2,3]benzodiazepine salt with L-tartaric acid semi-4-chloroanilide

Conditions
ConditionsYield
In ethanol at 20℃; for 20h; Heating / reflux;36%
17447-35-7

(R,R)-(+)-4-chlorotartranilic acid

608141-41-9

Apremilast

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrogenchloride / water / 60 - 70 °C / Resolution of racemate; Heating
2: acetic acid / 24 h / Reflux
View Scheme
Multi-step reaction with 2 steps
1: chloroform / Heating; Resolution of racemate
2: acetic acid / 24 h / Reflux
View Scheme
253168-94-4

2-(3-ethoxy-4-methoxyphenyl)-1-(methylsulfonyl)eth-2-ylamine

17447-35-7

(R,R)-(+)-4-chlorotartranilic acid

A

C12H19NO4S*C10H10ClNO5

B

C12H19NO4S*C10H10ClNO5

Conditions
ConditionsYield
In chloroform Solvent; Heating; Resolution of racemate; Overall yield = 94 %;A n/a
B n/a
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