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| CAS No.: | 17579-99-6 | ||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|
| Name: | METHYLTRIPHENOXYPHOSPHONIUM IODIDE | ||||||||||
| Article Data: | 5 | ||||||||||
| Molecular Structure: | |||||||||||
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| Formula: | C19H18 O3 P . I | ||||||||||
| Molecular Weight: | 452.228 | ||||||||||
| Synonyms: | Phosphorus(1+),methyltriphenoxy-, iodide (8CI); Phosphorus(1+), methyltriphenoxy-, iodide,(T-4)- (9CI); Methyltriphenoxyphosphonium iodide; Triphenylphosphine methiodide | ||||||||||
| EINECS: | 241-551-9 | ||||||||||
| Density: | g/cm3 | ||||||||||
| Melting Point: |
142-146 °C(lit.) |
||||||||||
| Boiling Point: | °Cat760mmHg | ||||||||||
| Flash Point: | °C | ||||||||||
| Hazard Symbols: |
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| Risk Codes: | 36/37/38 | ||||||||||
| Safety: |
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| PSA: | 41.28000 | ||||||||||
| LogP: | 2.61980 | ||||||||||
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| Conditions | Yield |
|---|---|
| im geschlossenen Rohr; |
- 1400677-76-0
tert-butyl (4S,7S,10aS)-7-formyl-5-oxooctahydro-2H-pyrido[2,1-b][1,3]thiazepin-4-ylcarbamate
- 17579-99-6
methyltriphenoxyphosphonium iodide
- 1400677-77-1
tert-butyl (4S,7S,10aS)-5-oxo-7-vinyloctahydro-2H-pyrido[2,1-b][1,3]thiazepin-4-ylcarbamate
| Conditions | Yield |
|---|---|
| Stage #1: methyltriphenoxyphosphonium iodide With potassium hexamethylsilazane In tetrahydrofuran; toluene at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: tert-butyl (4S,7S,10aS)-7-formyl-5-oxooctahydro-2H-pyrido[2,1-b][1,3]thiazepin-4-ylcarbamate In tetrahydrofuran; toluene at -78 - 20℃; for 3h; | 91% |
- 17579-99-6
methyltriphenoxyphosphonium iodide
- 59859-77-7
2-benzyloxycarbonylamino-3-hydroxy-propionic Acid tert-butyl Ester
| Conditions | Yield |
|---|---|
| In DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 3.5h; | 85% |
- 17579-99-6
methyltriphenoxyphosphonium iodide
- 95-55-6
2-amino-phenol
- 57602-63-8
2-methyl-2',3'-dihydro-3H-2λ5-[2,2']spirobi(benzo[1,3,2]oxazaphosphole)
| Conditions | Yield |
|---|---|
| With n-butyllithium In tetrahydrofuran; hexane | 75% |
| Conditions | Yield |
|---|---|
| In methanol; chloroform; N,N-dimethyl-formamide | 58% |
- 64-17-5
ethanol
- 17579-99-6
methyltriphenoxyphosphonium iodide
A
- 7526-26-3
diphenyl methylphosphonate
B
- 75-03-6
ethyl iodide
C
- 108-95-2
phenol
- 61898-54-2, 83805-51-0
3-isopropyl-pentane-1,5-diol
- 17579-99-6
methyltriphenoxyphosphonium iodide
- 98998-09-5
1-iodo-3-(2-iodo-ethyl)-4-methyl-pentane
- 22821-77-8
p-methylsulfonylbenzyl alcohol
- 17579-99-6
methyltriphenoxyphosphonium iodide
- 100960-84-7
(4-iodomethyl-phenyl)-methyl sulfone
- 1805-11-4, 96611-57-3, 103188-73-4
3β-acetoxy-6α-hydroxymethyl-5α-pregnan-20-one
- 17579-99-6
methyltriphenoxyphosphonium iodide
- 103129-42-6
3β-acetoxy-6α-iodomethyl-5α-pregnan-20-one
| Conditions | Yield |
|---|---|
| With methyl iodide |
- 17579-99-6
methyltriphenoxyphosphonium iodide
- 7526-26-3
diphenyl methylphosphonate
| Conditions | Yield |
|---|---|
| at 220℃; | |
| With sodium hydroxide | |
| With sodium hydroxide | |
| With butan-1-ol In acetonitrile at -40℃; |
- Total:16 Page 1 of 1 1
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