CAS No.1822-51-1,4-(Chloromethyl)pyridine hydrochloride Suppliers,MSDS download

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Basic Information

Molecular Structure:
CAS No.:	1822-51-1
Name:	4-(Chloromethyl)pyridine hydrochloride
Article Data:	8

Formula:	C₆H₆ClN^.HCl
Molecular Weight:	164.034
Synonyms:	Pyridine,4-(chloromethyl)-, hydrochloride (6CI,7CI,8CI,9CI);4-(Chloromethyl)pyridinehydrochloride;4-(Chloromethyl)pyridinium chloride;4-Chloromethylpyridinehydrochloride salt;4-Picolyl chloride hydrochloride;4-Pyridylmethyl chloridehydrochloride;
EINECS:	217-350-7
Density:	1.156g/cm³
Melting Point:	166-173 °C(lit.)
Boiling Point:	212 °C at 760 mmHg
Flash Point:	102 °C
Solubility:	water: 750 g/L (20 °C)
Appearance:	White crystalline powder
Hazard Symbols:	C,Xi
Risk Codes:	34-4-22-36/37/38
Safety:	26-36/37/39-45-36
Transport Information:	UN 3261 8/PG 3
PSA:	12.89000
LogP:	2.62240

Synthetic route

: 586-95-8
pyridine-4-methanol

: 1822-51-1
4-picolylchloride hydrochloride

Conditions

Conditions	Yield
With thionyl chloride In acetonitrile at 50℃; for 1h;	100%
With thionyl chloride In acetonitrile
With thionyl chloride In dichloromethane
With thionyl chloride In methanol	26.9 g

: 63608-12-8
4-(phenoxymethyl)pyridine

: 62302-28-7
4-pyridinemethanol hydrochloride

: 1822-51-1
4-picolylchloride hydrochloride

Conditions

Conditions	Yield
With thionyl chloride In benzene	76%

: 1003-67-4
4-methylpyridine-1-oxide

A: 3678-62-4
2-chloro-4-picoline

B: 1822-51-1
4-picolylchloride hydrochloride

Conditions

Conditions	Yield
With diisopropylamine; trichloromethyl chloroformate In dichloromethane at -40 - 20℃;

: 121-44-8
triethylamine

: 1822-51-1
4-picolylchloride hydrochloride

Conditions

Conditions	Yield
In N-methyl-acetamide

: 108-89-4
picoline

: 1822-51-1
4-picolylchloride hydrochloride

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: potassium permanganate / water / 0.58 h / 75 - 80 °C 2: sulfuric acid 3: sodium tetrahydroborate; aluminum (III) chloride / toluene; tetrahydrofuran / 0 - 5 °C 4: thionyl chloride / methanol View Scheme

: 55-22-1
pyridine-4-carboxylic acid

: 1822-51-1
4-picolylchloride hydrochloride

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: sulfuric acid 2: sodium tetrahydroborate; aluminum (III) chloride / toluene; tetrahydrofuran / 0 - 5 °C 3: thionyl chloride / methanol View Scheme

: 124-41-4
sodium methylate

: 1822-51-1
4-picolylchloride hydrochloride

: 70199-60-9
4-(methoxymethyl)pyridine

Conditions

Conditions	Yield
In methanol at 90℃; for 12h;	100%
With methanol
for 4h; Inert atmosphere; Reflux;

: 1822-51-1
4-picolylchloride hydrochloride

: 603-35-0
triphenylphosphine

: 73870-25-4
Triphenyl-4-pyridylmethylphosphonium chloride hydrochloride

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 140℃; for 20h;	100%

: 2,2’-dimethyl-3’-(pyridin-4-ylmethoxy)-[1,1’-biphenyl]-3-ol

: 1822-51-1
4-picolylchloride hydrochloride

: 4,4’-(((2,2’-dimethyl-[1,1’-biphenyl]-3,3’-diyl)bis(oxy))bis-(methylene))dipyridine

Conditions

Conditions	Yield
With caesium carbonate at 20℃;	100%

: 178980-30-8
2-(2-benzyloxyethyl)-5-(3,5-dichlorophenylthio)-4-isopropyl-1-methyl-1H-imidazole

: 1643-19-2
tetrabutylammomium bromide

: 1822-51-1
4-picolylchloride hydrochloride

: 4-[2-(2-benzyloxyethyl)-5-(3,5-dichlorophenylthio)-4-isopropyl-1H-imidazol-1-ylmethyl]pyridine

Conditions

Conditions	Yield
With sodium hydroxide In tetrahydrofuran	98%

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Chemistry

Synonyms: 4-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE;4-(CHLOROMETHYL)PYRIDINIUM CHLORIDE;4-PICOLYL CHLORIDE HYDROCHLORIDE;TIMTEC-BB SBB003917;4-Picolyl chloride HCl (65% in water);4-(Chloromethyl)PYRIDINE HCL;4-Plcolyl Chloride Hydrochloride;PYRIDINE, 4-(chloromethyl)-, hydrochloride
MF: C₆H₇C_l2N
MW: 164.03
EINECS: 217-350-7
MP: 166-173 °C
Storage Temp: 2-8°C
Water Solubility : 750 g/L (20 oC)
Sensitive : Hygroscopic
BRN : 3689154
STructural Formula:

Toxicity Data With Reference

Hazard Codes : C, Xi
Risk Statements :
R34: Causes burns
R4: Forms very sensitive explosive metallic compounds
R22: Harmful if swallowed
R36/37/38: Irritating to eyes, respiratory system and skin

Safety Profile

Safety Statements :
S26: In case of contact with eyes, rinse immediately with plenty of WATER and seek medical advice
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection
S45: In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
S36: Wear suitable protective clothing

Specification

Chemical Stability: Stable under normal temperatures and pressures. Hygroscopic: absorbs moisture or water from the air.
Conditions to Avoid: Incompatible materials, exposure to moist air or water.
Incompatibilities with Other Materials Strong oxidizing agents.
Hazardous Decomposition Products Hydrogen chloride, nitrogen oxides, carbon monoxide, carbon dioxide.
Hazardous Polymerization Will not occur.