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18523-47-2

Basic Information
CAS No.: 18523-47-2
Name: 3-azidopropanoic acid
Article Data: 49
Molecular Structure:
Molecular Structure of 18523-47-2 (3-azidopropanoic acid)
Formula: C3H5N3O2
Molecular Weight: 115.092
Synonyms: 3-azido-propionic acid;3-azidopropionic acid;3-Azidopropanoic acid;azidopropionic acid;2-azidopropionic acid;
PSA: 87.05000
LogP: 0.22416
Synthetic route
590-92-1

3-Bromopropionic acid

18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sodium azide In water100%
With sodium azide In acetonitrile at 85℃; for 5h;90%
With sodium azide In N,N-dimethyl-formamide for 4h; Reflux;89%
79-10-7

acrylic acid

18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With trimethylsilylazide In neat (no solvent) at 60℃; for 0.5h;99%
With trimethylsilylazide In water at 60℃; for 0.5h; Reagent/catalyst; Flow reactor; Green chemistry;99%
With trimethylsilylazide; Amberlite IRA900F at 30℃; for 2h; Michael addition; neat (no solvent);73%
107-94-8

chloropropionic acid

18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sodium azide In water for 15h;85%
With sodium azide In water at 100℃; for 22h;81%
With sodium azide In water at 85℃; for 12h;73%
With sodium azide In water at 20℃; for 168h;
57-57-8

β-Propiolactone

18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sodium azide In water at 20℃; for 6h; Inert atmosphere;15%
With sodium azide In water at 20℃; for 6h;15%
With sodium azide
aceton-<β-azido-propionyl-hydrazone>

aceton-<β-azido-propionyl-hydrazone>

18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sulfuric acid
23605-39-2

azido-b-alanine methyl ester

18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With methanol; lithium hydroxide at 20℃;
With sodium hydroxide In methanol at 20℃; for 48h;
107-95-9

3-amino propanoic acid

18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate In methanol at 20℃; for 16h;
40139-55-7

3-azidopropionic acid ethyl ester

18523-47-2

3-azidopropanoic acid

Conditions
ConditionsYield
With sodium hydroxide In methanol Inert atmosphere;
18523-47-2

3-azidopropanoic acid

14468-87-2

3-azidopropionyl chloride

Conditions
ConditionsYield
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃;100%
With oxalyl dichloride In dichloromethane at 20℃; for 6h;
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane for 3h;
With oxalyl dichloride In dichloromethane for 6h;
With thionyl chloride In dichloromethane at 20℃; for 12h;
18523-47-2

3-azidopropanoic acid

536-74-3

phenylacetylene

40139-46-6

3-(4-phenyl-1H-[1,2,3]triazol-1-yl)-propionic acid

Conditions
ConditionsYield
With copper(II) acetate monohydrate; triethylamine In water; acetonitrile at 20℃; for 8h;100%
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; tert-butyl alcohol at 20℃; for 12h;46%
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