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CAS No.: | 1943-83-5 |
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Name: | 2-Chloroethyl isocyanate |
Article Data: | 12 |
Molecular Structure: | |
Formula: | C3H4ClNO |
Molecular Weight: | 105.524 |
Synonyms: | 2-CHLOROETHYL ISOCYANATE;1-CHLORO-2-ISOCYANATO-ETHANE;ISOCYANIC ACID 2-CHLOROETHYL ESTER;1-chloro-2-isocyanato-ethan;2-chlorethylisokyanat;nsc87418;2-CHLOROETHYL ISOCYANATE, LOW HCL, 97%;2-Chloroethyl isocyanate 97% |
EINECS: | 217-734-4 |
Density: | 1.237 |
Melting Point: | 135 C |
Boiling Point: | 135 ºC |
Flash Point: | 56 ºC |
Solubility: | reacts |
Appearance: | liquid |
Hazard Symbols: | |
Risk Codes: | R23/24/25;R34;R42 |
Safety: | Moderately toxic by inhalation. Human mutation data reported. A flammable liquid. When heated to decomposition it emits very toxic fumes of Cl− and NOx. See also ISOCYANATES and ESTERS. |
Transport Information: | UN 1993 |
PSA: | 29.43000 |
LogP: | 0.56100 |
C3H4ClN3O
2-chloroethyl isothiocyanate
Conditions | Yield |
---|---|
Heating; | 100% |
Conditions | Yield |
---|---|
With sodium azide In benzene for 5h; Heating; | 52% |
Conditions | Yield |
---|---|
With 1,2,3-trichlorobenzene at 140℃; |
Conditions | Yield |
---|---|
(i) CCl4, (ii) (heating); Multistep reaction; | |
With triethylamine In diethyl ether |
Conditions | Yield |
---|---|
With pyridine; p-toluenesulfonyl chloride |
2-chloroethyl isothiocyanate
Conditions | Yield |
---|---|
With phosphorus trichloride zuletzt auf dem Dampfbad; |
2-chloroethyl isothiocyanate
Conditions | Yield |
---|---|
With phosphorus trichloride zuletzt auf dem Dampfbad; |
ethyl N-(2-chloroethyl)carbamate
phosphorus pentachloride
2-chloroethyl isothiocyanate
Conditions | Yield |
---|---|
Stage #1: carbon dioxide; 2-chloroethanamine hydrochloride With 1,1,1,3,3,3-hexamethyl-disilazane In toluene at 80 - 90℃; for 3h; Stage #2: at 200℃; Further stages.; |
Conditions | Yield |
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With diphenyl phosphoryl azide; triethylamine In toluene at 20 - 80℃; for 1.25h; Inert atmosphere; |
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