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Basic Information
CAS No.: 1973-04-2
Name: 2,4-Dichloro-6-methyl-1,3,5-triazine
Article Data: 35
Molecular Structure:
Molecular Structure of 1973-04-2 (2,4-Dichloro-6-methyl-1,3,5-triazine)
Formula: C4H3 Cl2 N3
Molecular Weight: 163.994
Synonyms: s-Triazine,2,4-dichloro-6-methyl- (6CI,7CI,8CI); 2,4-Dichloro-6-methyl-1,3,5-triazine;2,4-Dichloro-6-methyl-s-triazine; 2,4-Dichloro-6-methyltriazine;2-Methyl-4,6-dichlorotriazine; 4,6-Dichloro-2-methyl-1,3,5-triazine
Density: 1.5g/cm3
Melting Point: 97-98 °C
Boiling Point: 345.3°Cat760mmHg
Flash Point: 193.4°C
PSA: 38.67000
LogP: 1.48680
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Synthetic route
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1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

Conditions
ConditionsYield
With hydrogenchloride; aluminum (III) chloride In water; 1,2-dichloro-ethane at -5 - 5℃; for 8h; Reagent/catalyst; Solvent;99%
With hydrogenchloride; aluminum (III) chloride In dichloromethane at -5 - 5℃; under 750.075 Torr; for 12h;
108-77-0

1,3,5-trichloro-2,4,6-triazine

75-16-1

methylmagnesium bromide

1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

Conditions
ConditionsYield
In diethyl ether; dichloromethane at 0 - 22℃; for 3h; Inert atmosphere;90%
In diethyl ether; dichloromethane at 0 - 20℃;89%
In diethyl ether; dichloromethane at -10 - -5℃; for 4h;87%
108-77-0

1,3,5-trichloro-2,4,6-triazine

676-58-4

methylmagnesium chloride

1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

Conditions
ConditionsYield
In dichloromethane at -20 - -15℃; for 4.5h;65%
In tetrahydrofuran; diethyl ether at 0 - 20℃; Inert atmosphere;
In dichloromethane at 20℃; for 0.5h;
108-77-0

1,3,5-trichloro-2,4,6-triazine

1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

Conditions
ConditionsYield
With methylmagnesium bromide; magnesium sulfate In dichloromethane; water65%
1934-75-4

sodium dicyanamide

75-36-5

acetyl chloride

1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

Conditions
ConditionsYield
With hydrogenchloride In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; acetic acid methyl ester37%
915774-28-6

4-amino-2-(3-methyl-but-2-enyloxy)-benzonitrile

1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

933045-45-5

4-(4-chloro-6-methyl-[1,3,5]triazin-2-ylamino)-2-(3-methyl-but-2-enyloxy)-benzonitrile

Conditions
ConditionsYield
With sodium hydrogencarbonate98%
1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

1141898-92-1

N-({2-[(trifluoromethyl)oxy]phenyl}methyl)-2,3-dihydro-1H-indole-5-carboxamide

1141899-73-1

1-(4-chloro-6-methyl-1,3,5-triazin-2-yl)-N-({2-[(trifluoromethyl)oxy]phenyl}methyl)-2,3-dihydro-1H-indole-5-carboxamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 40℃; for 1h; Product distribution / selectivity;91%
1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

542-02-9

2-methyl-4,6-diamino-1,3,5-triazine

Conditions
ConditionsYield
With ammonia In acetone at 40 - 45℃;87%
1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

99-88-7

4-Isopropylaniline

C13H15ClN4

Conditions
ConditionsYield
In acetone at 20℃; for 1h;85%
1973-04-2

2,4-dichloro-6-methyl-1,3,5-triazine

C20H40N3(1+)*Br(1-)

C24H42ClN6(1+)*Br(1-)

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 3.25h;83%
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