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197958-29-5

Basic Information
CAS No.: 197958-29-5
Name: 2-Pyridineboronic acid
Article Data: 7
Molecular Structure:
Molecular Structure of 197958-29-5 (2-Pyridineboronic acid)
Formula: C5H6BNO2
Molecular Weight: 122.919
Synonyms: Boronicacid, 2-pyridinyl- (9CI);(2-Pyridinyl)boronic acid;
Density: 1.23 g/cm3
Melting Point: >300 °C
Boiling Point: 308.782 °C at 760 mmHg
Flash Point: 140.547 °C
Appearance: White to light yellow crystal powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/37/39
PSA: 53.35000
LogP: -1.23860
Synthetic route
109-04-6

2-bromo-pyridine

5419-55-6

Triisopropyl borate

197958-29-5

pyridin-2-ylboronic acid

Conditions
ConditionsYield
Stage #1: 2-bromo-pyridine; Triisopropyl borate With n-butyllithium In tetrahydrofuran; hexane; toluene at -30℃; for 3h; Inert atmosphere;
Stage #2: With hydrogenchloride In tetrahydrofuran; hexane; water; toluene at 20℃; for 1h; Inert atmosphere;
81%
Stage #1: 2-bromo-pyridine; Triisopropyl borate With n-butyllithium In tetrahydrofuran; hexane; toluene at -30 - 20℃; for 6h;
Stage #2: With hydrogenchloride In tetrahydrofuran; hexane; toluene at 20℃; for 1h;
81%
With n-butyllithium In tetrahydrofuran; hexane; toluene at -30 - 20℃; for 6h; Inert atmosphere;81%
Stage #1: 2-bromo-pyridine With n-butyllithium In diethyl ether; hexane at -78℃; for 0.5h;
Stage #2: Triisopropyl borate In diethyl ether; hexane at -78 - 20℃;
73%
109-04-6

2-bromo-pyridine

121-43-7

Trimethyl borate

197958-29-5

pyridin-2-ylboronic acid

Conditions
ConditionsYield
Stage #1: 2-bromo-pyridine With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h;
Stage #2: Trimethyl borate In tetrahydrofuran; hexane for 2h;
77%
Stage #1: 2-bromo-pyridine With n-butyllithium In tetrahydrofuran at -78℃; for 1h; Inert atmosphere;
Stage #2: Trimethyl borate In tetrahydrofuran at 20℃; for 2h; Inert atmosphere;
66.8%
109-04-6

2-bromo-pyridine

197958-29-5

pyridin-2-ylboronic acid

Conditions
ConditionsYield
Stage #1: 2-bromo-pyridine With isopropylmagnesium chloride In tetrahydrofuran at 20℃; for 2h;
Stage #2: With tris(trimethylsilyl)borate In tetrahydrofuran at 0 - 20℃; for 24h;
Stage #3: With hydrogenchloride at 0℃; pH=6 - 7;
70%

C31H28N2O2

197958-29-5

pyridin-2-ylboronic acid

C36H30BN3O2

Conditions
ConditionsYield
In methanol; toluene for 15h; Inert atmosphere; Reflux;99%
197958-29-5

pyridin-2-ylboronic acid

142-08-5

2-hydroxypyridin

Conditions
ConditionsYield
With hydrazine hydrate; caesium carbonate In water at 80℃; for 12h;96%

potassium cyanide

197958-29-5

pyridin-2-ylboronic acid

33893-89-9

5-(2-pyridyl)-1H-tetrazole

Conditions
ConditionsYield
With sodium azide; potassium carbonate In ethanol; water for 5h; Catalytic behavior; Reflux; Inert atmosphere; Green chemistry;96%

C29H20BBrN2

197958-29-5

pyridin-2-ylboronic acid

C34H24BN3

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In toluene at 110℃; for 3h; Inert atmosphere;95%
197958-29-5

pyridin-2-ylboronic acid

108-98-5

thiophenol

3111-54-4

2-phenylsulfanylpyridine

Conditions
ConditionsYield
With copper slag In N,N-dimethyl-formamide at 100℃; for 0.166667h; Temperature; Wavelength; Microwave irradiation; Green chemistry;94%
72754-04-2

3,7-dibromo-1,8-naphthyridine

197958-29-5

pyridin-2-ylboronic acid

C13H8BrN3

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene for 8h; Inert atmosphere; Reflux;93.7%
932372-99-1

2-bromo-5-iodophenol

197958-29-5

pyridin-2-ylboronic acid

C11H8BrNO

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 90℃; for 5h; Inert atmosphere;93%
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  • 2-Pyridineboronic acid CAS No.197958-29-5

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    197958-29-5

    2-Pyridineboronic acid CAS No.197958-29-5

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Chemistry

The molecular formula of 2-Pyridineboronic acid(197958-29-5) is C5H6BNO2 and its formula weight is 122.9177.
The chemical synonyms of 2-Pyridineboronic acid(197958-29-5) are PYRIDIN-2-YLBORONIC ACID;PYRIDIN-2-YL-2-BORONIC ACID;PYRIDINE-2-BORONIC ACID;2-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PYRIDINE;2-PYRIDINEBORNIC ACID;2-PYRIDINEBORONIC ACID;2-PYRIDINYLBORONIC ACID;Boronic acid, 2-pyridinyl- (9CI)
The molecular structure of 2-Pyridineboronic acid(197958-29-5):

Safety Profile

Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-36/37/39
Hazard Note  Irritant/Keep Cold under -20C