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200399-47-9

Basic Information
CAS No.: 200399-47-9
Name: Salacinol
Article Data: 5
Cas Database
Molecular Structure:
Molecular Structure of 200399-47-9 (Salacinol)
Formula: C9H18O9S2
Molecular Weight: 334.369
Synonyms: SALACINOL;
EINECS: N/A
Density: N/A
Melting Point: N/A
Boiling Point: N/A
Flash Point: N/A
Solubility: N/A
Appearance: N/A
Hazard Symbols: N/A
Risk Codes: N/A
Safety:
Transport Information: N/A
PSA: 218.98000
LogP: -3.45510
Synthetic route

2,3,5-tri-O-p-methoxybenzyl-1,4-dideoxy-1,4-{[(2S,3S)-2,4-benzylidenedioxy-3-(sulfooxy)butyl]-episulfoniumylidene}-D-arabinitol inner salt

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
With trifluoroacetic acid at 20℃; for 0.5h;86%
942610-80-2

2,3,5-tri-O-benzyl-1,4-dideoxy-1,4-{(S)-[(2S,3S)-2,4-O-isopropylidene-3-(sulfooxy)butyl]episulfonioylidene}-D-arabinitol

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
With hydrogen; acetic acid; palladium on activated charcoal at 50℃; for 5h;82%
438576-21-7

1,4-dideoxy-1,4-{(S)-[(2S,3S)-2,4-O-isopropylidene-3-(sulfooxy)butyl]episulfonioylidene}-D-arabinitol

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
With hydrogenchloride at 40℃; for 4h;74%

2,3,5-tri-O-benzyl-1,4-dideoxy-1,4-{[(2S,3S)-2,4-benzylidenedioxy-3-(sulfooxy)butyl]-episulfoniumylidene}-D-arabinitol inner salt

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
With hydrogen; palladium dihydroxide In water; acetic acid65%

2,3,5-tri-O-benzyl-1,4-dideoxy-1,4-{[(2S,3S)-2,4-di(benzyloxy)-3-(sulfooxy)butyl]-episulfoniumylidene}-D-arabinitol inner salt

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
With hydrogen; palladium dihydroxide In water; acetic acid65%
160882-25-7

3-O-benzyl-1-deoxy-4-thio-D-arabino-furanose

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 90 percent / sodium hydride / dimethylformamide / 0.5 h / 0 °C
2: 99 percent / potassium carbonate / various solvent(s) / 6 h / Heating
3: 82 percent / aq. acetic acid; hydrogen / Pd/C / 5 h / 50 °C
View Scheme
187590-77-8

1,4-anhydro-2,3,5-tri-O-benzyl-4-thio-D-arabinitol

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 99 percent / potassium carbonate / various solvent(s) / 6 h / Heating
2: 82 percent / aq. acetic acid; hydrogen / Pd/C / 5 h / 50 °C
View Scheme
Multi-step reaction with 2 steps
1: 94 percent / K2CO3 / various solvent(s) / 14 h / Heating
2: 65 percent / H2 / Pd(OH)2 / acetic acid; H2O
View Scheme
Multi-step reaction with 2 steps
1: 45 percent / K2CO3 / various solvent(s) / 14 h / Heating
2: 65 percent / H2 / Pd(OH)2 / acetic acid; H2O
View Scheme
160882-26-8

(2R,3S,4S)-2-(hydroxymethyl)tetrahydrothiophene-3,4-diol

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 87 percent / NaH / tetrahydrofuran / 13 h / 20 - 55 °C
2: 100 percent / K2CO3 / various solvent(s) / Heating
3: 86 percent / aq. trifluoroacetic acid / 0.5 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 5 °C
1.2: 6 h / 0 - 25 °C
2.1: 2,6-dimethylpyridine / acetone / 13 h / 70 °C
3.1: diethylamine / methanol / 3 h / 25 °C
4.1: trifluoroacetic acid / water / 2 h / 25 °C
View Scheme
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 5 °C
1.2: 3 h / 0 - 25 °C
2.1: 2,6-dimethylpyridine / acetone / 24 h / 70 °C
3.1: diethylamine / methanol / 1 h / 25 °C
4.1: hydrogen; acetic acid; 20% palladium hydroxide-activated charcoal / 2 h / 50 °C
View Scheme
635316-05-1

(2R,3S,4S)-3,4-bis((4-methoxybenzyl)oxy)-2-(((4-methoxybenzyl)oxy)methyl)tetrahydrothiophene

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 100 percent / K2CO3 / various solvent(s) / Heating
2: 86 percent / aq. trifluoroacetic acid / 0.5 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: 2,6-dimethylpyridine / acetone / 13 h / 70 °C
2: diethylamine / methanol / 3 h / 25 °C
3: trifluoroacetic acid / water / 2 h / 25 °C
View Scheme
Multi-step reaction with 3 steps
1: 2,6-dimethylpyridine / acetone / 13 h / 70 °C
2: diethylamine; methanol / 3 h / 25 °C
3: water; trifluoroacetic acid / 2 h / 25 °C
View Scheme
Multi-step reaction with 3 steps
1: 2,6-dimethylpyridine / acetone / 13 h / 70 °C
2: diethylamine / methanol / 3 h / 25 °C
3: trifluoroacetic acid / water / 2 h / 25 °C
View Scheme

(4S,5S)-4-(((2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophen-1-ium)-1-yl)methyl-2-(1,3-dimethoxy-1,3-dioxopropan-2-yl)-1,3-dioxan-5-yl sulfate

200399-47-9

(2S,3S)-4-((1S,2R,3S,4S)-3,4-dihydroxy-2-(hydroxymethyl)tetrahydro-1H-thiophene-1-ium-1-yl)-1,3-dihydroxybutan-2-yl sulfate

Conditions
ConditionsYield
With diethylamine In water; ethyl acetate at 25℃; for 0.833333h; Reagent/catalyst; Solvent;1.05 g
With water; diethylamine In ethyl acetate at 25℃; for 0.833333h; Reagent/catalyst; Temperature; Solvent;1.05 g
With diethylamine In water; ethyl acetate at 25℃; for 0.833333h; Reagent/catalyst; Solvent; Temperature;1.05 g
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    CAS No.:200399-47-9 Other Name:Salacinol MF:C9H18O9S2 Place of Origin:Hebei, China Type:Pharmaceutical intermediates Purity:99.9% Brand Name:hbnj Application:organic chemical Appearance:White powder Storage:Cool Dry Place Sample:Availiable

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    CAS 200399-47-9 Salacinol

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    Do best quality products, erect the morality model Application:Please email us, thanks

    Wuxi Morality Chemical Co., Ltd is specialized in the development and manufacture of industrial additives, bulk chemical intermediates, pharmaceutical raw materials and pesticide

  • Wuxi Morality Chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-510-83597286 17768505220

    Address:B/7F, 321th WuYun Rd, Wanda Plaza, Wuxi City, 214174, China

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  • 200399-47-9

  • Casno:

    200399-47-9

    200399-47-9

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    Hebei Ruishun Trade Co.,Ltd registered capital one million, we have a production of pharmaceutical raw materials, pharmaceutical raw materials factory reagent r&d center, we do

  • Hebei Ruishun Trade Co.,Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-311-68037669

    Address:WanDa commerce building ,yuhua district

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  • Salacinol

  • Casno:

    200399-47-9

    Salacinol

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    200399-47-9

    Actavis is one of the world's leading players in the development, manufacture, and sale of first-class generic pharmaceuticals. The successful integration of a number of acquisitio

  • ACTAVIS GROUP

    Aruba  |  Contact Details

    Business Type:Trading Company

    Tel:297-236-456977

    Address:Bubali

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  • Salacinol

  • Casno:

    200399-47-9

    Salacinol

    Min.Order: 0

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    Topbatt Chemical Co., Ltd., Established in 2019, located in Shenzhen, Guangdong Province, is a Manufacturer and Trading company which specialized in fine chemicals like Pharmaceutical Reference Standards and Stable Isotopes. Our Stable Isotopes produ

    Topbatt Chemical Co. Ltd., Established in 2019, located in Shenzhen, Guangdong Province, is a Manufacturer and Trading company which specialized in fine chemicals like Pharmaceutic

  • Topbatt Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-755-86210921

    Address:402A, 4th floor, Building 2, Shenzhen Biological Incubator Base, No. 10, Gaoxin Zhongyi Road, Mailing Community, Yuehai Street, Nanshan District

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  • Casno:

    200399-47-9

    Salacinol

    Min.Order: 0

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    We are a bespoke specialist sourcing company for the fine chemical and pharmaceutical industry, offering an outsourcing service for fine chemicals, intermediates and custom synthes

  • Leancare Ltd.

    United Kingdom  |  Contact Details

    Business Type:Trading Company

    Tel:+33 962096793

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