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2106-05-0

Basic Information
CAS No.: 2106-05-0
Name: 5-Chloro-2-fluoroaniline
Article Data: 5
Molecular Structure:
Molecular Structure of 2106-05-0 (5-Chloro-2-fluoroaniline)
Formula: C6H5ClFN
Molecular Weight: 145.564
Synonyms: Aniline,5-chloro-2-fluoro- (6CI,8CI);(5-Chloro-2-fluorophenyl)amine;3-Chloro-6-fluoroaniline;5-Chloro-2-fluorobenzenamine;NSC 10291;
EINECS: 218-284-1
Density: 1.349 g/cm3
Boiling Point: 214.4 °C at 760 mmHg
Flash Point: 83.5 °C
Appearance: COLORLESS TO BROWN LIQUID
Hazard Symbols: HarmfulXn, IrritantXi, ToxicT
Risk Codes: 36/37/38-20/21/22-23/24/25
Safety: 26-36-2636/37/39-23-36/37/39-45
Transport Information: UN 2810
PSA: 26.02000
LogP: 2.64250
Synthetic route
345-18-6

2-fluoro-5-chloronitrobenzene

2106-05-0

5-chloro-2-fluoroaniline

Conditions
ConditionsYield
With hydrogen; platinum on activated charcoal In 1,2-dimethoxyethane under 2585.74 Torr; for 24h; Catalytic hydrogenation;
89-61-2

2,5-dichloronitrobenzene

potassium-compound of 1-<4-hydroxy-phenyl>-ethanone

potassium-compound of 1-<4-hydroxy-phenyl>-ethanone

2106-05-0

5-chloro-2-fluoroaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 52 percent / KF; 18-crown-6 / tetrahydrothiophene 1,1-dioxide / 32 h / 180 °C
2: H2 / 5 percent Pt/C / 1,2-dimethoxy-ethane / 24 h / 2585.74 Torr
View Scheme
345-18-6

2-fluoro-5-chloronitrobenzene

A

348-54-9

2-Fluoroaniline

B

2106-05-0

5-chloro-2-fluoroaniline

Conditions
ConditionsYield
With 5%-palladium/activated carbon; hydrazine hydrate In methanol at 80℃; for 0.0833333h; Overall yield = 25 %;

C15H14ClFN2

2106-05-0

5-chloro-2-fluoroaniline

Conditions
ConditionsYield
With sodium tetrahydroborate; copper(l) chloride In ethanol at 20℃;24 mg
2106-05-0

5-chloro-2-fluoroaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: bis(dibenzylideneacetone)-palladium(0); N-fluorobis(benzenesulfon)imide; potassium nitrate / ethyl acetate / 12 h / 90 °C / Sealed tube
2: sodium tetrahydroborate; copper(l) chloride / ethanol / 20 °C
View Scheme

1-(3-chlorophenyl)-2-(2,4,6-trimethylphenyl)diazene

2106-05-0

5-chloro-2-fluoroaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: bis(dibenzylideneacetone)-palladium(0); N-fluorobis(benzenesulfon)imide; potassium nitrate / ethyl acetate / 12 h / 100 °C / Sealed tube
2: sodium tetrahydroborate; copper(l) chloride / ethanol / 20 °C
View Scheme

C12H7Cl2FN2

2106-05-0

5-chloro-2-fluoroaniline

Conditions
ConditionsYield
With sodium tetrahydroborate; copper(l) chloride In ethanol at 20℃;28.8 mg
2106-05-0

5-chloro-2-fluoroaniline

C6H4ClFIN

Conditions
ConditionsYield
With iodine; silver sulfate In ethanol at 0 - 20℃; for 1h; Large scale;98%
1089278-78-3

methyl 3-(3-{2-[(3-{[2-(dimethylamino)ethyl]oxy}phenyl)amino]-4-pyrimidinyl}-imidazo[1,2-a]pyridin-2-yl)benzoate

2106-05-0

5-chloro-2-fluoroaniline

1089278-77-2

N-(5-chloro-2-fluorophenyl)-3-(3-{2-[(3-{[2-(dimethylamino)ethyl]oxy}phenyl)amino]-4-pyrimidinyl}imidazo[1,2-a]pyridin-2-yl)benzamide

Conditions
ConditionsYield
Stage #1: methyl 3-(3-{2-[(3-{[2-(dimethylamino)ethyl]oxy}phenyl)amino]-4-pyrimidinyl}-imidazo[1,2-a]pyridin-2-yl)benzoate; 5-chloro-2-fluoroaniline With sodium hexamethyldisilazane In tetrahydrofuran at 20℃; for 0.5h;
Stage #2: With methanol In tetrahydrofuran
94%
2106-05-0

5-chloro-2-fluoroaniline

116369-24-5

4-bromo-5-chloro-2-fluoroaniline

Conditions
ConditionsYield
With N-Bromosuccinimide In acetonitrile at 25℃; for 1h;91%
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    2-Fluoro-5-chloroaniline

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Chemistry

MF: C6H5ClFN
Synonyms: BUTTPARK 44\01-98;5-CHLORO-2-FLUOROPHENYLAMINE;5-CHLORO-2-FLUOROANILINE;5-Chloro-2-fluoroaniline 98%;5-Chloro-2-fluoroaniline98%
MW: 145.56
EINECS: 218-284-1
Product Categories: Anilines, Aromatic Amines and Nitro Compounds;Aniline;Miscellaneous
density : 1.29 g/mL at 25 °C(lit.)
bp : 102-105 °C20 mm Hg(lit.)
refractive index : n 20/D 1.561(lit.)
Fp : 219 °F

Safety Profile

Risk Statements : 36/37/38-20/21/22-23/24/25
Safety Statements : 26-36-2636/37/39-23-36/37/39-45
Hazard Codes : Xi,T,Xn
Hazard Note : Toxic
RIDADR : UN2810
WGK Germany : 3
HazardClass : 6.1
PackingGroup : III