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CAS No.: | 2162-74-5 |
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Name: | Bis(2,6-diisopropylphenyl)carbodiimide |
Molecular Structure: | |
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Formula: | C25H34N2 |
Molecular Weight: | 362.558 |
Synonyms: | Carbodiimide,bis(2,6-diisopropylphenyl)- (7CI,8CI);Additin RC 8500;Bis(2,6-diisopropylphenyl)carbodiimide;Bis(o,o'-diisopropylphenyl)carbodiimide;Carbo D;EN 160;N,N'-(2,2',6,6'-Tetraisopropyldiphenyl)carbodiimide;N,N'-Bis(2,6-diisopropylphenyl)carbodiimide;Raschig 7000;Stabaxol 1;StabaxolI;Stabaxol I-LF;Stabaxol P 1;Stabilizer 7000;Stabilizer 7000F; |
EINECS: | 218-487-5 |
Density: | 0.953 g/cm3 |
Melting Point: | 51 °C |
Boiling Point: | 477.699 °C at 760 mmHg |
Flash Point: | 235.604 °C |
Solubility: | 50μg/L at 20℃ |
Appearance: | White to off-white crystalline powder |
Risk Codes: | 36/37/38 |
Safety: | 26-36/37/39 |
PSA: | 24.72000 |
LogP: | 8.31730 |
N,N'-bis(2,6-diisopropylphenyl)thiourea
N,N'-bis(2,6-diisopropylphenyl)carbodiimide
Conditions | Yield |
---|---|
With bis(trichloromethyl) carbonate; sodium hydrogencarbonate In ethyl acetate at 20℃; for 0.25h; | 95% |
With dmap; iodine In tetrahydrofuran at 0 - 20℃; Reagent/catalyst; | 90% |
With magnesium sulfate; mercury(II) oxide In toluene for 12h; Reflux; | 87% |
Conditions | Yield |
---|---|
In toluene at 20℃; under 760.051 Torr; for 0.166667h; Mechanism; | 86% |
2,6-diisopropylphenyl isocyanate
N,N'-bis(2,6-diisopropylphenyl)carbodiimide
Conditions | Yield |
---|---|
With 3,4-dimethyl-1-phenyl-3-phospholene 1-oxide In xylene for 12h; Heating; | 78% |
at 150℃; | |
With methylphospholene oxide at 160 - 170℃; |
2,5-dihydro-3-methyl-1-phenyl-1H-phosphole 1-oxide
2,6-diisopropylphenyl isocyanate
B
N,N'-bis(2,6-diisopropylphenyl)carbodiimide
Conditions | Yield |
---|---|
A 1.43 g (79%) B n/a |
2,6-diisopropylbenzenamine
N,N'-bis(2,6-diisopropylphenyl)carbodiimide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / water 2: tetrachloromethane; triphenylphosphine; triethylamine / dichloromethane View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / water / Inert atmosphere; Schlenk technique 2: triethylamine; triphenylphosphine / tetrachloromethane; dichloromethane / Inert atmosphere; Schlenk technique View Scheme |
A
N,N'-bis(2,6-diisopropylphenyl)carbodiimide
Conditions | Yield |
---|---|
In chlorobenzene at 90℃; for 2h; Inert atmosphere; Schlenk technique; |
2,6-diisopropyl-1-azidobenzene
N,N'-bis(2,6-diisopropylphenyl)carbodiimide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diethyl ether / 0.5 h / 20 °C 2: toluene / 0.17 h / 20 °C / 760.05 Torr View Scheme |
tetrahydrofuran
N,N'-bis(2,6-diisopropylphenyl)carbodiimide
phenyllithium
[PhC(NC6H4iPr2-2,6)2]Li(THF)
Conditions | Yield |
---|---|
In dibutyl ether at 20℃; for 2h; | 100% |
Conditions | Yield |
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In hexane at 20℃; Schlenk technique; Inert atmosphere; | 99% |
In hexane N2-atmosphere; addn. of soln. of AlMe3 (slight excess) to soln. of carbodiimide, stirring at room temp. for 18 h; evapn.; NMR spectroscopy; | 74% |
Conditions | Yield |
---|---|
Stage #1: phenylacetylene With (tri(3,5-dimethylpyrazolyl)borate)CpGd(CH2Ph)(THF) In toluene for 0.5h; Inert atmosphere; Glovebox; Schlenk technique; Stage #2: N,N'-bis(2,6-diisopropylphenyl)carbodiimide In toluene at 110℃; for 22h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Time; Concentration; Inert atmosphere; Glovebox; Schlenk technique; | 99% |
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Product Name:Bis-(2,6-diisopropylphenyl)carbodiimide(2162-74-5)
CAS No:2162-74-5
Molecular Formula : C25H34N2
Molecular Formula:362.55
CBNumber : CB1347186
Formula Weight : 362.55
MP : 51 °C
Synonyms of Bis-(2,6-diisopropylphenyl)carbodiimide(2162-74-5):BIS(2,6-DIISOPROPYLPHENYL)CARBODIIMIDE;(2,6-diisopropylphenyl)carbodiimide;2,2’,6,6’-Tetraisopropyldiphenylcarbodiimide;bis(2,6-diisopropylphenyl)-carbodiimid;carbod;n,n’-methanetetraylbis(2,6-bis(1-methylethyl)-benzenamin;n,n’-methanetetraylbis(2,6-bis(1-methylethyl)benzenamine);n,n’-methanetetraylbis[2,6-bis(1-methylethyl)-benzenamin
Molecular Structure of Bis-(2,6-diisopropylphenyl)carbodiimide(2162-74-5):
1. | orl-rat LD50:200 mg/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) OTS0545280 . | ||
2. | ihl-rat LCLo:100 mg/m3/6H | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) OTS0545280 . | ||
3. | ipr-rat LD50:200 mg/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) OTS0545280 . | ||
4. | ihl-mus LCLo:1 g/m3/1H | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) OTS0545280 . | ||
5. | ihl-rbt LCLo:100 mg/m3/6H | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) OTS0545280 . | ||
6. | ihl-gpg LCLo:100 mg/m3/6H | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) OTS0545280 . |