CAS No.216854-23-8,(S)-3-N-Boc-aminopiperidine Suppliers

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Basic Information

Molecular Structure:
CAS No.:	216854-23-8
Name:	(S)-3-N-Boc-aminopiperidine
Article Data:	3

Formula:	C₁₀H₂₀N₂O₂
Molecular Weight:	200.281
Synonyms:	Carbamicacid, (3S)-3-piperidinyl-, 1,1-dimethylethyl ester (9CI);(S)-(-)-3-(tert-Butoxycarbonylamino)piperidine;(S)-3-tert-Butoxycarbonylaminopiperidine;(S)-tert-ButylN-[piperidin-3-yl]carbamate;tert-Butyl ((3S)-piperidin-3-yl)carbamate;
EINECS:	626-980-5
Density:	1.02 g/cm³
Melting Point:	122-127 °C
Boiling Point:	304.8 °C at 760 mmHg
Flash Point:	138.2 °C
Hazard Symbols:	Xi
Risk Codes:	37/38-41
Safety:	26-39
PSA:	50.36000
LogP:	1.98280

Synthetic route

: 92235-39-7
3(S)-<(butoxycarbonyl)amino>-2-oxopiperidine

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

Conditions

Conditions	Yield
With borane-THF In tetrahydrofuran at 0 - 25℃; for 6.75h;	30%

: 607376-86-3
(S)-2-(tert-butoxycarbonylamino)pentane-1,5-diyl dimethanesulfonate

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

Conditions

Conditions	Yield
With ammonium hydroxide In acetonitrile for 48h; Ambient temperature; Yield given;

: 56-86-0
L-glutamic acid

2-benzyloxycarbonylaminomethyl-4-benzyliden-Δ2-oxazolinone-(5): 2-benzyloxycarbonylaminomethyl-4-benzyliden-Δ2-oxazolinone-(5)

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: H2SO4 / 2 h / Heating 2: Et3N / dioxane; H2O / 2 h / 0 °C 3: NaBH4, CaCl2 / ethanol / 2 h / 0 °C 4: Et3N / CH2Cl2 / 1 h / -10 - 0 °C 5: aq. NH4OH / acetonitrile / 48 h / Ambient temperature View Scheme

: 6525-53-7, 16422-27-8, 40149-68-6
L-glutamic acid dimethyl ester

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: Et3N / dioxane; H2O / 2 h / 0 °C 2: NaBH4, CaCl2 / ethanol / 2 h / 0 °C 3: Et3N / CH2Cl2 / 1 h / -10 - 0 °C 4: aq. NH4OH / acetonitrile / 48 h / Ambient temperature View Scheme

: 59279-60-6, 130622-05-8
dimethyl (2S)-2-[(tert-butoxycarbonyl)amino]pentanedioate

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: NaBH4, CaCl2 / ethanol / 2 h / 0 °C 2: Et3N / CH2Cl2 / 1 h / -10 - 0 °C 3: aq. NH4OH / acetonitrile / 48 h / Ambient temperature View Scheme

: 162955-48-8
[(1S)-4-hydroxy-1-(hydroxymethyl)butyl]carbamic acid tert-butyl ester

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: Et3N / CH2Cl2 / 1 h / -10 - 0 °C 2: aq. NH4OH / acetonitrile / 48 h / Ambient temperature View Scheme

: 1188914-98-8
1-[4-chloro-6-(4-morpholinyl)-1,3,5-triazin-2-yl]-2-(difluoromethyl)-4-methoxy-1H-benzimidazole

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

: 1188915-59-4
tert-butyl (R)-1-[4-[2-(difluoromethyl)-4-methoxy-1H-benzimidazol-1-yl]-6-(4-morpholinyl)-1,3,5-triazin-2-yl]piperidin-3-ylcarbamate

Conditions

Conditions	Yield
at 20℃;	100%

: 1527525-60-5
1-[5-(difluoromethyl)-6-fluoro-2-pyridyl]-6-(6-methylpyrazin-2-yl)pyrazolo[4,3-c]pyridine

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

: 1527525-62-7
tert-butyl N-[(3S)-1-[3-(difluoromethyl)-6-[6-(6-methylpyrazin-2-yl)pyrazolo[4,3-c]pyridin-1-yl]-2-pyridyl]-3-piperidyl]carbamate

Conditions

Conditions	Yield
With 4-methyl-morpholine In 1-methyl-pyrrolidin-2-one at 100℃; Sealed tube;	100%

: 23680-84-4
2-chloro-6,7-dimethoxyquinazolin-4-amine

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

: tert-butyl (S)-(1-(4-amino-6,7-dimethoxyquinazolin-2-yl)piperidin-3-yl)carbamate

Conditions

Conditions	Yield
In i-Amyl alcohol at 130℃; under 760.051 Torr; for 0.833333h; Microwave irradiation;	100%

: 1188914-98-8
1-[4-chloro-6-(4-morpholinyl)-1,3,5-triazin-2-yl]-2-(difluoromethyl)-4-methoxy-1H-benzimidazole

: 216854-23-8
tert-butyl (S)-piperidin-3-yl-carbamate

: 1188915-61-8
tert-butyl (S)-1-[4-[2-(difluoromethyl)-4-methoxy-1H-benzimidazol-1-yl]-6-(4-morpholinyl)-1,3,5-triazin-2-yl]piperidin-3-ylcarbamate

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃;	100%

Total:133 Page 1 of 4 1 2 3 4 Next>>

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Chemistry

IUPAC Name: tert-butyl N-[(3S)-piperidin-3-yl]carbamate
Synonyms: (S)-TERT-BUTYL-PIPERIDIN-3-YLCARBAMATE;Carbamic acid, (3S)-3-piperidinyl-, 1,1-dimethylethyl ester (9CI);(S)-PIPERIDIN-3-YL-CARBAMIC ACID TERT-BUTYL ESTER;;(S)-3-N-BOC-AMINOPIPERIDINE;(S)-3-BOC-AMINOPIPERIDINE;CARBAMIC ACID, (3S)-3-PIPERIDINYL-, 1,1-DIMETHYLETHYL ESTER;(S)-(-)-3-TERT-BUTOXYCARBONYLAMINOPIPERIDINE;(S)-3-(TERT-BUTOXYCARBONYLAMINO)PIPERIDINE
The Molecular formula of (S)-3-N-Boc-aminopiperidine(216854-23-8): C₁₀H₂₀N₂O₂
The Molecular Weight of (S)-3-N-Boc-aminopiperidine(216854-23-8): 200.28
Molecular Structure :
Melting point: 122-127°C
alpha: -3 ^o (c=1, DMF)

Safety Profile

The Hazard Codes of (S)-3-N-Boc-aminopiperidine(216854-23-8): Xi
The Risk Statements information of (S)-3-N-Boc-aminopiperidine(216854-23-8):
41: Risk of serious damage to eyes
37/38: Irritating to respiratory system and skin
The Safety Statements information of (S)-3-N-Boc-aminopiperidine(216854-23-8):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
39: Wear eye/face protection
WGK Germany: 3