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2196-18-1

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Basic Information
CAS No.: 2196-18-1
Name: α,4'-Dihydroxy-3'-methoxypropiophenone
Article Data: 8
Molecular Structure:
Molecular Structure of 2196-18-1 (α,4'-Dihydroxy-3'-methoxypropiophenone)
Formula: C10H12O4
Molecular Weight: 196.203
Synonyms: Propiophenone,3,4'-dihydroxy-3'-methoxy;
Density: 1.246g/cm3
Boiling Point: 408.2°Cat760mmHg
Flash Point: 165.4°C
PSA: 66.76000
LogP: 0.96590
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3-chloro-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

Conditions
ConditionsYield
With sodium hydroxide In water at 20 - 65℃; for 1.5h; Reagent/catalyst; Temperature; Solvent; Industrial scale;100%
22317-34-6

β-hydroxy-α-(2-methoxyphenoxy)4-hydroxy-3-methoxypropiophenone

A

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

B

90-05-1

2-methoxy-phenol

Conditions
ConditionsYield
With formic acid; N-ethyl-N,N-diisopropylamine; Lumogen F Orange 240 In acetonitrile at 25℃; for 8h; Reagent/catalyst; UV-irradiation; Inert atmosphere;A 99%
B 96%
With formic acid; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 24h; Inert atmosphere; Irradiation;A 69%
B 74%
7382-59-4

guaiacylglycerol-β-guaiacyl ether

A

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

B

90-05-1

2-methoxy-phenol

C

498-02-2

1-(3-methoxy-4-hydroxyphenyl)ethanone

Conditions
ConditionsYield
With oxygen; rose bengal In acetonitrile at 13℃; Irradiation;A 28 % Chromat.
B 15 % Chromat.
C 30 % Chromat.
...Expand
3-acetoxy-1-<4-hydroxy-3-methoxy-phenyl>-propanone-(1)

3-acetoxy-1-<4-hydroxy-3-methoxy-phenyl>-propanone-(1)

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

Conditions
ConditionsYield
With water; barium carbonate
3-bromo-1-<4-hydroxy-3-methoxy-phenyl>-propanone-(1)

3-bromo-1-<4-hydroxy-3-methoxy-phenyl>-propanone-(1)

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

Conditions
ConditionsYield
With sodium hydroxide
1835-11-6

4-benzyloxy-3-methoxyacetophenone

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 69 percent / Br2 / CHCl3; CCl4 / 1) 5 deg C, 20 min, 2) 5 deg C -> 40 deg C, 2 h
2: 95 percent / K2CO3 / dimethylformamide / 2 h / 25 °C
3: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h
4: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C
5: 28 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation
View Scheme
22317-34-6

β-hydroxy-α-(2-methoxyphenoxy)4-hydroxy-3-methoxypropiophenone

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C
2: 28 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation
View Scheme
1835-12-7

3-methoxy-4-benzyloxy-α-bromoacetophenone

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 95 percent / K2CO3 / dimethylformamide / 2 h / 25 °C
2: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h
3: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C
4: 28 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation
View Scheme
22317-29-9

1-(4-(benzyloxy)-3-methoxyphenyl)-2-(2-methoxyphenoxy)ethan-1-one

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h
2: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C
3: 28 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation
View Scheme
7382-59-4

guaiacylglycerol-β-guaiacyl ether

A

2196-18-1

3-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-1-propanone

B

90-05-1

2-methoxy-phenol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: oxygen; N-hydroxyphthalimide / acetone / 30 h / 20 °C / 760.05 Torr / Irradiation
2: N-ethyl-N,N-diisopropylamine; formic acid / acetonitrile / 24 h / 20 °C / Inert atmosphere; Irradiation
View Scheme
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