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| CAS No.: | 2212-32-0 |
|---|---|
| Name: | N-Methyl-N-(N,N-dimethylaminoethyl)-aminoethanol |
| Molecular Structure: | |
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|
|
| Formula: | C7H18N2O |
| Molecular Weight: | 146.233 |
| Synonyms: | Toyocat RX 5;N-(Dimethylaminoethyl)-N-methylethanolamine;N-(2-Dimethylaminoethyl)-N-methylethanolamine;N,N,N'-Trimethylaminoethylethanolamine;N,N,N'-Trimethyl-N'-(hydroxyethyl)ethylenediamine;N,N,N'-Trimethyl-N'-(2-hydroxyethyl)ethylenediamine;Kaolizer 28;Jeffcat Z 110;Dabco T;2-[[2-(Dimethylamino)ethyl]methylamino]ethanol; |
| EINECS: | 218-658-4 |
| Density: | 0.937 g/cm3 |
| Boiling Point: | 206.999 °C at 760 mmHg |
| Flash Point: | 66 °C |
| Solubility: | 1000g/L at 20℃ |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 36/37/38 |
| Safety: | 26-36/37/39 |
| PSA: | 26.71000 |
| LogP: | -0.52790 |
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- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 50-00-0
formaldehyd
- 111-41-1
2-(2-Aminoethylamino)ethanol
- 2212-32-0
2-{[2-(dimethylamino)ethyl]methylamino}ethanol
| Conditions | Yield |
|---|---|
| Stage #1: formaldehyd; 2-(2-Aminoethylamino)ethanol at 80 - 90℃; for 0.5h; Stage #2: With formic acid at 80 - 90℃; for 2h; Stage #3: In butan-1-ol at 120℃; for 4h; Temperature; Solvent; | 95.2% |
| With 5%-palladium/activated carbon; hydrogen at 100 - 110℃; under 11251.1 Torr; for 4.5h; Reagent/catalyst; Temperature; Pressure; Inert atmosphere; Autoclave; | 90.4% |
| With formic acid In water for 4h; Heating; | 70% |
| With formic acid |
- 109-83-1
(2-hydroxyethyl)(methyl)amine
- 107-99-3
2-(dimethylamino)ethyl chloride
- 2212-32-0
2-{[2-(dimethylamino)ethyl]methylamino}ethanol
| Conditions | Yield |
|---|---|
| With potassium carbonate In ethanol Heating; |
- 2212-32-0
2-{[2-(dimethylamino)ethyl]methylamino}ethanol
| Conditions | Yield |
|---|---|
| In toluene the aminoalcohol is added to a soln. of Ce(OiPr)4 in toluene at room temp, stirring for 12 h (under argon using Schlenk tubes); evapn. to dryness, the crude product is recrystd. in a mixt. of toluene and CH2Cl2, crystals are obtained at -30°C, elem. anal.; | 96% |
- 2212-32-0
2-{[2-(dimethylamino)ethyl]methylamino}ethanol
| Conditions | Yield |
|---|---|
| In hexane byproducts: HN(Si(CH3)3)2; under dry N2; alcohol added to soln. of Zn-compd., exothermic reaction, stirred for 16h,; volatiles removed in vac., solidified on standing for 1-2d; elem. anal.; | 95% |
- 2212-32-0
2-{[2-(dimethylamino)ethyl]methylamino}ethanol
| Conditions | Yield |
|---|---|
| In toluene the aminoalcohol is added to a soln. of Ce(OiPr)4 (ratio 2:1) in toluene at room temp, stirring for 12 h (under argon using Schlenk tubes); isolated by concentration from the reaction medium, elem. anal.; | 95% |
| Conditions | Yield |
|---|---|
| Stage #1: 2-{[2-(dimethylamino)ethyl]methylamino}ethanol With sodium hydride In tetrahydrofuran at -20℃; for 1h; Inert atmosphere; Schlenk technique; Stage #2: carbon disulfide In tetrahydrofuran for 1h; Inert atmosphere; Schlenk technique; | 91% |
| Conditions | Yield |
|---|---|
| With triethylamine In diethyl ether at 20℃; for 16h; Inert atmosphere; | 88% |
| Conditions | Yield |
|---|---|
| With triethylamine In diethyl ether at 20℃; for 16h; Inert atmosphere; | 85% |
- 2212-32-0
2-{[2-(dimethylamino)ethyl]methylamino}ethanol
| Conditions | Yield |
|---|---|
| With n-butyllithium In hexane at -40 - 20℃; for 4h; Schlenk technique; Inert atmosphere; | 85% |
| With n-butyllithium In hexane at -40 - 20℃; for 4h; Schlenk technique; Glovebox; Inert atmosphere; | 85% |
- 2212-32-0
2-{[2-(dimethylamino)ethyl]methylamino}ethanol
- 1184-54-9, 18213-24-6
copper(II) methoxide
| Conditions | Yield |
|---|---|
| In not given prepd. by the alcohol-exchange procedure described by Singh, J. V.; Baranwal, B. P.; Mehrotra, R. C.; T. Anorg. Allg. Chem. 1981, 477, 235; crystn. from hexane and distn. of mother liquor; | 83% |
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Chemistry
Molecular Structure:
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Molecular Formula: C7H18N2O
Molecular Weight: 146.2306
IUPAC Name: 2-[2-Dimethylaminoethyl(methyl)amino]ethanol
Synonyms of Ethanol, 2-((2-(dimethylamino)ethyl)methylamino)- (CAS NO.2212-32-0): 2-((2-(Dimethylamino)ethyl)methylamino)-ethanol ; EINECS 218-658-4 ; N,N,N'-Trimethyl-N'-(2-hydroxyethyl)-1,2-ethanediamine ; N-(2-(Dimethylamino)ethyl)-N-methylethanolamine
CAS NO: 2212-32-0
Classification Code: Amino Alcohols ; Organic Building Blocks ; Oxygen Compounds
Index of Refraction: 1.468
Molar Refractivity: 43.45 cm3
Molar Volume: 156 cm3
Surface Tension: 34.6 dyne/cm
Density: 0.936 g/cm3
Flash Point: 66 °C
Enthalpy of Vaporization: 51.56 kJ/mol
Boiling Point: 207 °C at 760 mmHg
Vapour Pressure: 0.0541 mmHg at 25°C
Safety Profile
Hazard Codes of Ethanol, 2-((2-(dimethylamino)ethyl)methylamino)- (CAS NO.2212-32-0): 
Xi
Risk Statements: 36/37/38
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection.
WGK Germany: 3