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223734-62-1

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Basic Information
CAS No.: 223734-62-1
Name: 2-[[(1S)-1-(3-Butyn-1-yl)hexyl]oxy]tetrahydro-2H-pyran
Article Data: 2
Molecular Structure:
Molecular Structure of 223734-62-1 (2-[[(1S)-1-(3-Butyn-1-yl)hexyl]oxy]tetrahydro-2H-pyran)
Formula: C15H26O2
Molecular Weight: 238.37
Synonyms: 2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran;
PSA: 18.46000
LogP: 3.89190
Related products
Synthetic route
678992-52-4

1-(trimethylsilyl)-O-tetrahydropyran-2-yl-1-decyn-5-(S)-ol

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
With sodium hydroxide In ethanol at 20℃; for 20h;
110-87-2

3,4-dihydro-2H-pyran

(+-)-4-hydroxy-3-methyl-butan-2-one

(+-)-4-hydroxy-3-methyl-butan-2-one

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: TsOH*pyridine / CH2Cl2 / 15 h / 20 °C
2: BuLi / tetrahydrofuran; hexane / 15 h / 0 - 20 °C
3: NaOH / ethanol / 20 h / 20 °C
View Scheme
81007-64-9

(S)-1-chloroheptane-2-ol

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: TsOH*pyridine / CH2Cl2 / 15 h / 20 °C
2: BuLi / tetrahydrofuran; hexane / 15 h / 0 - 20 °C
3: NaOH / ethanol / 20 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1.1: sodium hydroxide / tert-butyl methyl ether / 18 h / 25 °C
2.1: magnesium; iodine; mercury dichloride / diethyl ether / 0 - 36 °C / Inert atmosphere
2.2: 0.5 h
3.1: pyridinium p-toluenesulfonate / dichloromethane / 24 h / 0 - 25 °C
View Scheme
Multi-step reaction with 4 steps
1.1: sodium hydroxide / tert-butyl methyl ether / 18 h / 25 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 3.5 h / -50 - -35 °C / Inert atmosphere
2.2: 2.5 h / -40 - -20 °C
3.1: sodium hydroxide; ethanol / 2 h / 25 °C
4.1: pyridinium p-toluenesulfonate / dichloromethane / 24 h / 0 - 25 °C
View Scheme
Multi-step reaction with 5 steps
1: sodium hydroxide / tert-butyl methyl ether / 18 h / 25 °C
2: copper(l) iodide / tetrahydrofuran / 3 h / 0 - 5 °C / Inert atmosphere
3: pyridinium p-toluenesulfonate / dichloromethane / 25 °C
4: pyridine; pyridinium perbromide hydrobromide / dichloromethane / 3 h / 0 - 5 °C
5: sodium amide / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / Inert atmosphere; Reflux
View Scheme
678992-51-3

(S)-1-chloro-O-tetrahydropyran-2-yl-heptan-2-ol

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: BuLi / tetrahydrofuran; hexane / 15 h / 0 - 20 °C
2: NaOH / ethanol / 20 h / 20 °C
View Scheme
61229-03-6

(S)-2-pentyloxirane

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: magnesium; iodine; mercury dichloride / diethyl ether / 0 - 36 °C / Inert atmosphere
1.2: 0.5 h
2.1: pyridinium p-toluenesulfonate / dichloromethane / 24 h / 0 - 25 °C
View Scheme
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 3.5 h / -50 - -35 °C / Inert atmosphere
1.2: 2.5 h / -40 - -20 °C
2.1: sodium hydroxide; ethanol / 2 h / 25 °C
3.1: pyridinium p-toluenesulfonate / dichloromethane / 24 h / 0 - 25 °C
View Scheme
Multi-step reaction with 4 steps
1: copper(l) iodide / tetrahydrofuran / 3 h / 0 - 5 °C / Inert atmosphere
2: pyridinium p-toluenesulfonate / dichloromethane / 25 °C
3: pyridine; pyridinium perbromide hydrobromide / dichloromethane / 3 h / 0 - 5 °C
4: sodium amide / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / Inert atmosphere; Reflux
View Scheme
1374332-11-2

(5S)-dec-1-en-5-ol

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridinium p-toluenesulfonate / dichloromethane / 25 °C
2: pyridine; pyridinium perbromide hydrobromide / dichloromethane / 3 h / 0 - 5 °C
3: sodium amide / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / Inert atmosphere; Reflux
View Scheme
110-87-2

3,4-dihydro-2H-pyran

848609-05-2

(S)-Dec-1-yn-5-ol

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
With pyridinium p-toluenesulfonate In dichloromethane at 0 - 25℃; for 24h; Temperature;65.1 g

C15H28O2

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; pyridinium perbromide hydrobromide / dichloromethane / 3 h / 0 - 5 °C
2: sodium amide / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / Inert atmosphere; Reflux
View Scheme

C15H28Br2O2

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
With sodium amide In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene Inert atmosphere; Reflux;

C13H26OSi

223734-62-1

2-[[(1S)-1-(3-butynyl)hexyl]oxy]tetrahydro-2H-pyran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydroxide; ethanol / 2 h / 25 °C
2: pyridinium p-toluenesulfonate / dichloromethane / 24 h / 0 - 25 °C
View Scheme
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