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22710-07-2

Basic Information
CAS No.: 22710-07-2
Name: 2,3-Dimethylpyridine-N-oxide
Article Data: 46
Cas Database
Molecular Structure:
Molecular Structure of 22710-07-2 (2,3-Dimethylpyridine-N-oxide)
Formula: C7H9NO
Molecular Weight: 123.155
Synonyms: 2,3-Lutidine,1-oxide (6CI,7CI,8CI);2,3-Dimethylpyridine 1-oxide;2,3-DimethylpyridineN-oxide;2,3-Lutidine-N-oxide;pyridine, 2,3-dimethyl-, 1-oxide;2,3-Lutidine-N-oxide;Dimethylpyridineoxide;
Density: 1 g/cm3
Melting Point: 85-93 °C
Boiling Point: 298.1 °C at 760 mmHg
Flash Point: 134.1 °C
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/37/39
PSA: 25.46000
LogP: 1.73190
Synthetic route
583-61-9

2,3-Lutidine

22710-07-2

2,3-dimethylpyridine 1-oxide

Conditions
ConditionsYield
With sodium tungstate; dihydrogen peroxide In water at 55℃; for 3h; Temperature;99%
With 3-chloro-benzenecarboperoxoic acid In Isopropyl acetate at 10 - 35℃; for 5.83333h; Green chemistry;98.9%
With △-Na8H[PW9O34]·19H2O; dihydrogen peroxide In water at 20℃; for 24h; Green chemistry;94%
583-61-9

2,3-Lutidine

50-00-0

formaldehyd

22710-07-2

2,3-dimethylpyridine 1-oxide

Conditions
ConditionsYield
With sulfuric acid; dihydrogen peroxide In acetic acid
583-61-9

2,3-Lutidine

937-14-4

3-chloro-benzenecarboperoxoic acid

22710-07-2

2,3-dimethylpyridine 1-oxide

Conditions
ConditionsYield
With sodium sulfite In dichloromethane; Petroleum ether
22710-07-2

2,3-dimethylpyridine 1-oxide

63071-09-0

2-hydroxymethyl-3-methyl pyridine

Conditions
ConditionsYield
With trifluoroacetic anhydride In dichloromethane at 23℃; for 40h; Inert atmosphere; Schlenk technique;96%
Multi-step reaction with 2 steps
1: 81 percent / 1 h / Heating
2: 81 percent / 1 N NaOH / methanol / 1.5 h / 25 °C
View Scheme
Multi-step reaction with 2 steps
1: AcOH / 120 °C
2: 2N aq. NaOH / methanol / 2 h / 25 °C
View Scheme
Stage #1: 2,3-dimethylpyridine 1-oxide In dichloromethane at 0℃;
Stage #2: With trifluoroacetic anhydride at 20 - 45℃; for 7h;
22710-07-2

2,3-dimethylpyridine 1-oxide

37699-43-7

2,3-dimethyl-4-nitropyridine N-oxide

Conditions
ConditionsYield
With potassium nitrite; sulfuric acid at -10 - 85℃; for 2h; Temperature; Green chemistry;92.9%
With sulfuric acid; nitric acid at 100℃; for 5h;78%
With sulfuric acid; nitric acid at 95℃; for 20h;53%
22710-07-2

2,3-dimethylpyridine 1-oxide

259807-92-6

2,3-dimethyl-4-bromopyridine N-oxide

Conditions
ConditionsYield
With bromine In water at 0 - 35℃; for 6h; Temperature;92%
22710-07-2

2,3-dimethylpyridine 1-oxide

556-96-7

5-bromo-1,3-xylene

1151985-86-2

2-(3,5-dimethylbenzyl)-3-methylpyridine 1-oxide

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos In toluene at 110℃; for 0.75h; Inert atmosphere; Microwave irradiation;90%
22710-07-2

2,3-dimethylpyridine 1-oxide

108-24-7

acetic anhydride

52814-41-2

2-(acetoxymethyl)-3-methylpyridine

Conditions
ConditionsYield
for 1h; Heating;81%
22710-07-2

2,3-dimethylpyridine 1-oxide

628-71-7

1-Heptyne

82113-65-3

bis(trifluoromethanesulfonyl)amide

1-(hept-1-en-2-yloxy)-2,3-dimethylpyridin-1-ium bis((trifluoromethyl)sulfonyl)amide

Conditions
ConditionsYield
With [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I) at 20℃; for 5h;81%
22710-07-2

2,3-dimethylpyridine 1-oxide

106-38-7

para-bromotoluene

1151985-88-4

3-methyl-2-(4-methylbenzyl)pyridine 1-oxide

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; ruphos In toluene at 70℃; Inert atmosphere;76%
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Specification

The 2,3-Dimethylpyridine-N-oxide, with the CAS registry number 22710-07-2, has the systematic name of 2,3-dimethylpyridine 1-oxide, and it is also called Dimethylpyridineoxide. The molecular formula of the chemical is C7H9NO.

The characteristics of this chemical are as followings: (1)ACD/LogP: -0.28; (2)# of Rule of 5 Violations: 0; (3)#Freely Rotating Bonds: 0; (4)Polar Surface Area: 24.11 Å2; (5)Index of Refraction: 1.509; (6)Molar Refractivity: 36.68 cm3; (7)Molar Volume: 122.7 cm3; (8)Polarizability: 14.54×10-24cm3; (9)Surface Tension: 33.1 dyne/cm; (10)Density: 1 g/cm3; (11)Flash Point: 134.1 °C; (12)Enthalpy of Vaporization: 51.65 kJ/mol; (13)Boiling Point: 298.1 °C at 760 mmHg; (14)Vapour Pressure: 0.00229 mmHg at 25°C.

You should be cautious while dealing with this chemical. It irritates to eyes, respiratory system and skin. Therefore, you had better take the following instructions: Wear suitable protective clothing, gloves and eye/face protection, and if in case of contacting with eyes, rinse immediately with plenty of water and seek medical advice.

Addtionally, the following datas could be converted into the molecular structure:
(1)SMILES: [O-][n+]1cccc(c1C)C
(2)InChI: InChI=1/C7H9NO/c1-6-4-3-5-8(9)7(6)2/h3-5H,1-2H3
(3)InChIKey: QWLULCKKOHDCIE-UHFFFAOYAL