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22972-51-6

Basic Information
CAS No.: 22972-51-6
Name: (+)-(1S,4R)-P-MENTHA-2,8-DIEN-1-OL
Article Data: 35
Molecular Structure:
Molecular Structure of 22972-51-6 ((+)-(1S,4R)-P-MENTHA-2,8-DIEN-1-OL)
Formula: C10H16O
Molecular Weight: 152.236
Synonyms: 2-Cyclohexen-1-ol,1-methyl-4-(1-methylethenyl)-, (1S-cis)-;(+)-(1S,4R)-p-Mentha-2,8-dien-1-ol;(+)-cis-p-Mentha-2,8-dien-1-ol;(+)-p-Mentha-2,8-dien-1-ol;(1S,4R)-p-Menth-2,8-dien-1-ol;cis-Isolimonenol;p-Mentha-2,8-dien-1-b-ol;
Density: 0.947 g/cm3
Boiling Point: 216.873 °C at 760 mmHg
Flash Point: 86.957 °C
Solubility: 4.2g/L
Appearance: white solid
PSA: 20.23000
LogP: 2.27970
Synthetic route

C16H22O2S

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

Conditions
ConditionsYield
With piperidine In dimethyl sulfoxide at 170℃; for 4h;75%
1415961-21-5

(1S,2S,5R)-2-hydroxy-N,N,2-trimethyl-5-(prop-1-en-2-yl)cyclohexanamineoxide

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

Conditions
ConditionsYield
at 180℃; under 1 Torr; Cope Elimination; Pyrolysis;74%
With dihydrogen peroxide In ethanol; water at 150 - 162℃; Reflux; Schlenk technique; Glovebox; Inert atmosphere;38.2 g
74756-11-9

(1S,2S,4R)-2-phenylseleninyl-p-menth-8-en-1-ol

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

Conditions
ConditionsYield
In chloroform for 0.5h; Heating;53%
In chloroform at 62℃; for 6h; Inert atmosphere;512 g
6909-30-4

(1S,2R,4R)-limonene-1,2-epoxide

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

Conditions
ConditionsYield
Stage #1: (1S,2R,4R)-limonene-1,2-epoxide With sodium tetrahydroborate; diphenyl diselenide for 2h; Heating;
Stage #2: With dihydrogen peroxide for 7h; Heating; Further stages.;
31.6%
Multi-step reaction with 2 steps
1.1: H2O / 18 h / 150 °C
2.1: H2O2 / H2O / 18 h / 20 °C
2.2: 150 - 180 °C
View Scheme
Multi-step reaction with 3 steps
1: H2O / 150 °C / sealed vessel
2: 30percent H2O2 / H2O
3: pyrolysis
View Scheme
5989-27-5

D-limonene

A

52154-82-2

(1R,4R)-p-mentha-2,8-dien-1-ol

B

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

Conditions
ConditionsYield
With oxygen; rose bengal In methanol at 0℃; for 8.5h; UV-irradiation;A 5.3%
B 13.4%
With air Erwaermen des Reaktionsprodukts mit wss. Natriumsulfit-Loesung;
(i) O2, MeOH, (irradiation), (ii) LiAlH4, Et2O; Multistep reaction;
(i) O2, rose bengal, MeOH, (irradiation), (ii) LiAlH4, Et2O; Multistep reaction;
With air Erwaermen des Reaktionsprodukts mit wss. Natriumsulfit-Loesung;
5989-27-5

D-limonene

B

18383-51-2

(-)-trans-carveol

C

52154-82-2

(1R,4R)-p-mentha-2,8-dien-1-ol

D

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

E

2102-62-7

p-Menthadiene-<1(7),8>-trans-ol-(2)

F

10374-04-6

p-Menthadiene<1(7),8>-cis-ol-(2)

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane; air; zinc 5,10,15,20-tetraphenylporphyrin; triphenylphosphine In benzene for 3h; Irradiation; multistep reaction: photosensitized oxygenation of olefines;
With sodium tetrahydroborate; tetraphenylporphyrine; oxygen Product distribution; 1.) acetonitrile, irradiation, 2.) methanol; other sensitizers;A 5 % Chromat.
B 7 % Chromat.
C 9 % Chromat.
D 40 % Chromat.
E 16 % Chromat.
F 23 % Chromat.
With oxygen; fullerene-C60 In toluene at 0 - 10℃; for 4h; Product distribution; Irradiation; other sensitizer in other solvent;
138-86-3

limonene.

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

Conditions
ConditionsYield
With oxygen Irradiation;
5989-27-5

D-limonene

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

Conditions
ConditionsYield
With oxygen Irradiation;
Multi-step reaction with 4 steps
1: 3-chloro-benzenecarboperoxoic acid / chloroform / 1.5 h / -5 - 20 °C
2: water / 18 h / 20 °C / Reflux
3: dihydrogen peroxide / water; acetonitrile / 2 h / 20 °C / Cooling with ice
4: 180 °C / 1 Torr / Pyrolysis
View Scheme
Multi-step reaction with 4 steps
1.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 5 °C
2.1: sodium tetrahydroborate / ethanol / 1 h / 8 °C / Inert atmosphere
2.2: 4 h / 8 - 80 °C / Inert atmosphere
3.1: dihydrogen peroxide / ethanol; tetrahydrofuran / 6 h / 6 - 20 °C / Inert atmosphere
4.1: chloroform / 6 h / 62 °C / Inert atmosphere
View Scheme

(+)-trans-N.N-Dimethylamino-2-p-menthen-8-ol-1-N-oxyd

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

Conditions
ConditionsYield
at 140℃;

(1S,2S,4R)-4-Isopropenyl-1-methyl-2-nitroso-cyclohexanol

22972-51-6

(1S,4R)-p-mentha-2,8-dien-1-ol

Conditions
ConditionsYield
pyrolysis; Yield given;
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    Product Name: (+)-(1S,4R)-P-MENTHA-2,8-DIEN-1-OL CAS: 22972-51-6 MF: C10H16O MW: 152.23 EINECS: Product Categories: Mol File: 22972-51-6.mol (+)-(1S,4R)-P-MENTHA-2,8-DIEN-1-OL Structure (+)-(1S,4R)-P-MENTHA-2,8-DIEN-1-OL Chem

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    (1S,4r)-1-methyl-4-(prop-1-en-2-yl)cyclohex-2-enol Synonyms: (+)-(1s,4r)-p-mentha-2,8-dien-1-ol CAS No.: 22972-51-6 Molecular Formula: C10H16O Molecular Weigith: 152.23 Product description:Colorless or Light Yellow Liquid Assay: 99%min Water:0

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  • High purity trans-Mentha-2,8-dien-1-ol

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Specification

The trans-Mentha-2,8-dien-1-ol is a chemical which the formula C10H16O. With the CAS registry number 22972-51-6, it is also named as (+)-(1S,4R)-p-Mentha-2,8-dien-1-ol ; (1S,4R)-1-methyl-4-(prop-1-en-2-yl)cyclohex-2-enol ;  (1S,4R) 1-methyl-4-(1-methylethenyl)-2-cyclohexen-1-ol . It is white solid. This product should be stored on the place where the temperature is at 0-5°C. At this temperature, the product can be kept perfect.

The trans-Mentha-2,8-dien-1-ol has many suppliers, such as PharmaSci Shanghai Co., Ltd. and Ring Specialty Chemicals Inc. The price of this product changes with the market.