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CAS No.: | 2305-36-4 |
---|---|
Name: | 2-Amino-4-methylbenzoic acid |
Article Data: | 26 |
Molecular Structure: | |
Formula: | C8H9 N O2 |
Molecular Weight: | 151.165 |
Synonyms: | p-Toluicacid, 2-amino- (6CI,7CI,8CI); 2-Amino-4-methylbenzoic acid; 2-Amino-p-toluicacid; 4-Methylanthranilic acid; NSC 39155 |
EINECS: | 218-976-3 |
Density: | 1.254 g/cm3 |
Melting Point: | 174-177 ºC |
Boiling Point: | 329.8 °C at 760 mmHg |
Flash Point: | 153.3 °C |
Appearance: | white crystalline powder |
Hazard Symbols: | |
Risk Codes: | R36/37/38 |
Safety: | S26;S37/39 |
PSA: | 63.32000 |
LogP: | 1.85660 |
4-methyl-2-nitrobenzoic acid
4-methylanthranilic acid
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In ethanol at 20℃; under 760.051 Torr; | 100% |
With platinum (IV) oxide; hydrogen In methanol for 3h; | 98% |
With palladium on activated carbon; hydrogen In ethyl acetate at 20℃; for 14h; Saturated gas; | 95% |
With hydrogenchloride; tin | |
With iron(III) chloride; hydrazine hydrate; sodium hydroxide In water at 70℃; for 1h; Temperature; |
Conditions | Yield |
---|---|
With ammonium hydroxide; L-2-O-methyl-chiro-inositol; copper(II) acetate monohydrate In 1-methyl-pyrrolidin-2-one at 110℃; for 12h; | 87% |
Conditions | Yield |
---|---|
With selenium; nitrobenzene; sodium hydroxide In methanol; water; dimethyl sulfoxide at 90℃; for 5h; Inert atmosphere; | 70% |
2-bromo-5-methylaniline
4-methylanthranilic acid
Conditions | Yield |
---|---|
With tert.-butyl lithium In hydrogenchloride; diethyl ether; water; pentane | 59% |
Conditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide |
7-methyl-3-m-tolyl-1H-quinazoline-2,4-dione
4-methylanthranilic acid
Conditions | Yield |
---|---|
With potassium hydroxide |
2-amino-4-methylbenzamide
4-methylanthranilic acid
Conditions | Yield |
---|---|
With potassium hydroxide |
5-methyl-2-cyanoaniline
4-methylanthranilic acid
Conditions | Yield |
---|---|
With potassium hydroxide |
methanol
6-methylindoline-2,3-dione
A
methyl 4-methylanthranilate
B
4-methylanthranilic acid
Conditions | Yield |
---|---|
With dihydrogen peroxide; sodium methylate 1.) 0-10 deg C 2.) room temperature, 30 min; Yield given. Multistep reaction; |
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