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Basic Information
| CAS No.: | 23117-71-7 |
|---|---|
| Name: | 2-(bromomethyl)-9H-thioxanthen-9-one |
| Article Data: | 4 |
| Molecular Structure: | |
|
|
|
| Formula: | C14H9 Br O S |
| Molecular Weight: | 305.195 |
| Synonyms: | Thioxanthen-9-one,2-(bromomethyl)- (8CI); 2-(Bromomethyl)-9-oxothioxanthene |
| Density: | 1.593g/cm3 |
| Melting Point: | 194-195 °C(Solv: acetone (67-64-1)) |
| Boiling Point: | 450.2°Cat760mmHg |
| Flash Point: | 226°C |
| PSA: | 45.31000 |
| LogP: | 4.30960 |
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Synthetic route
- 15774-82-0
2-methyl-9H-thioxanthen-9-one
- 23117-71-7
2-bromomethyl-9H-thioxanthene-9-one
Conditions
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide; dibenzoyl peroxide | |
| With N-Bromosuccinimide; dibenzoyl peroxide In cyclohexane for 4h; Reflux; | |
| With N-Bromosuccinimide; dibenzoyl peroxide In cyclohexane for 4h; Reflux; | 1.8 g |
- 108-88-3
toluene
- 23117-71-7
2-bromomethyl-9H-thioxanthene-9-one
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1.1: sulfuric acid / 1 h / 25 °C 1.2: 2 h / 20 - 25 °C 2.1: N-Bromosuccinimide / dibenzoyl peroxide / cyclohexane / 4 h / Reflux View Scheme | |
| Multi-step reaction with 2 steps 1.1: sulfuric acid / 1 h / 20 °C 1.2: 2 h / 20 °C 2.1: N-Bromosuccinimide; dibenzoyl peroxide / cyclohexane / 4 h / Reflux View Scheme |
- 119-80-2
2,2'-dithiobenzoic acid
- 23117-71-7
2-bromomethyl-9H-thioxanthene-9-one
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1.1: sulfuric acid / 1 h / 25 °C 1.2: 2 h / 20 - 25 °C 2.1: N-Bromosuccinimide / dibenzoyl peroxide / cyclohexane / 4 h / Reflux View Scheme |
- 527-89-9
dithiosalicylic acid
- 23117-71-7
2-bromomethyl-9H-thioxanthene-9-one
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1.1: sulfuric acid / 1 h / 20 °C 1.2: 2 h / 20 °C 2.1: N-Bromosuccinimide; dibenzoyl peroxide / cyclohexane / 4 h / Reflux View Scheme |
- 30095-98-8
methyl (2-nitrophenyl)acetate
- 23117-71-7
2-bromomethyl-9H-thioxanthene-9-one
- 957003-97-3
C23H17NO5S
Conditions
| Conditions | Yield |
|---|---|
| With potassium tert-butylate In tetrahydrofuran at 20℃; for 18h; | 93% |
- 23117-71-7
2-bromomethyl-9H-thioxanthene-9-one
- 147-93-3
Thiosalicylic acid
Conditions
| Conditions | Yield |
|---|---|
| With potassium carbonate In N,N-dimethyl-formamide at 80℃; | 93% |
- 1821-27-8
N,N-bis(p-nitrophenyl)amine
- 23117-71-7
2-bromomethyl-9H-thioxanthene-9-one
Conditions
| Conditions | Yield |
|---|---|
| With potassium carbonate In acetonitrile at 80℃; for 5h; | 90% |
- 110-86-1
pyridine
- 23117-71-7
2-bromomethyl-9H-thioxanthene-9-one
Conditions
| Conditions | Yield |
|---|---|
| In chloroform at 20 - 25℃; for 48h; | 84% |
- 1074-36-8
4-mercaptobenzoic acid
- 23117-71-7
2-bromomethyl-9H-thioxanthene-9-one
Conditions
| Conditions | Yield |
|---|---|
| With potassium carbonate In N,N-dimethyl-formamide at 80℃; | 83% |
Conditions
| Conditions | Yield |
|---|---|
| With potassium hydroxide for 3h; Heating; | 77% |
- Total:24 Page 1 of 1 1
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2-(bromomethyl)-9H-thioxanthen-9-one
