CAS No.2343-89-7,METHYL 2-FLUOROACRYLATE Suppliers

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Basic Information

Molecular Structure:
CAS No.:	2343-89-7
Name:	METHYL 2-FLUOROACRYLATE
Article Data:	34

Formula:	C₄H₅FO₂
Molecular Weight:	104.081
Synonyms:	Acrylicacid, 2-fluoro-, methyl ester (6CI,7CI,8CI);Methyl a-fluoroacrylate;a-Fluoroacrylic acid methyl ester;
Density:	1.057 g/cm³
Boiling Point:	75.9 °C at 760 mmHg
Flash Point:	1.1 °C
Solubility:	Slightly soluble in water.
Hazard Symbols:	Xi
Risk Codes:	10-36/37/38
Safety:	16-26-36
Transport Information:	UN 1993
PSA:	26.30000
LogP:	0.64260

Synthetic route

: 85345-88-6
Methyl 2-Fluoro-3-(4-toluenesulfonyloxy)propanoate

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With potassium phtalimide at -78 - 150℃; under 0.01 Torr;	97%

: 55900-27-1
Methyl 3-chloro-2-fluoropropanoate

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With 2,6-di-tert-butyl-4-methyl-phenol; sodium phosphate In 1-methyl-pyrrolidin-2-one at 150℃; under 112.511 - 225.023 Torr;	95%
With dimethyl amine In diethyl ether; benzene

: 67-56-1
methanol

: 430-99-9
2-fluoroacrylic acid

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With thionyl chloride at 5 - 35℃; for 2h; Concentration; Reagent/catalyst;	93%

: dimethyl 2-fluoro-2-chloromethylmalonate

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With 2,6-di-tert-butyl-4-methyl-phenol; sodium carbonate In 1-methyl-pyrrolidin-2-one at 150℃; under 225.023 Torr; for 4h;	92%

: 67-56-1
methanol

: 2317-91-1
1-chloro-1-fluoroethane

: 201230-82-2
carbon monoxide

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With dichloro[ferrocene-1,1'-diylbis(diisopropylphosphine-P)]palladium(II); triethylamine at 100℃; under 5250.53 Torr; for 8h; Reagent/catalyst; Autoclave;	91.8%
With bis(tri-t-butylphosphine)palladium(0) at 100℃; for 18h; Reagent/catalyst; Time; Autoclave;	77.4%

...Expand

: 67-56-1
methanol

: 420-25-7
1-bromo-1-fluoroethylene

: 201230-82-2
carbon monoxide

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With bis-triphenylphosphine-palladium(II) chloride; lithium carbonate; triethylamine at 90℃; for 6h; Reagent/catalyst; Temperature; Autoclave;	90.7%
With dichloro[4,5-bis(diphenylphosphino)-9,9’-dimethylxanthene]palladium(II); triethylamine at 100℃; under 7500.75 Torr; for 8h; Reagent/catalyst; Autoclave;	90.1%
With bis-triphenylphosphine-palladium(II) chloride; tributyl-amine; lithium carbonate at 90℃; under 7500.75 Torr; for 6h; Reagent/catalyst; Autoclave;	71.8 g

...Expand

: 1-chloro-1-fluoro-2,2-dimethoxycyclopropane

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With 2,6-di-tert-butyl-4-methyl-phenol; methoxybenzene at 120 - 130℃; under 500 Torr; Reagent/catalyst; Temperature;	89.5%
With 2,6-di-tert-butyl-4-methyl-phenol at 145℃; under 360 Torr;	12.3 g

: 2365-93-7
methyl 3-bromo-2-fluoro-2-chloropropanoate

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With 10H-phenothiazine; sulfuric acid; zinc In water at 82 - 86℃; for 0.333333h;	85%
With hydrogen sulfide; sodium N-nitroso-N-phenylhydroxylaminate; zinc In water at 100℃;	82%
With zinc	80%
With sulfuric acid; zinc

: C13H13FO6

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With 10H-phenothiazine In sulfolane at 180℃; for 6h;	83.9%

: C14H15FO6

: 2343-89-7
methyl 2-fluoroprop-2-enoate

Conditions

Conditions	Yield
With 4-methoxy-phenol at 170℃; for 9h;	81.2%

Raw Materials

399-86-0

50-00-0

453-18-9

2365-93-7

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Specification

The cas register number of Methyl 2-fluoroacrylate is 2343-89-7. In addition, the molecular formula is C₄H₅FO₂ and the molecular weight is 104.08. The systematic name about this chemical is methyl 2-fluoroprop-2-enoate. Besides, it is a irritating chemical and should be stored in a cool and dry place.

Physical properties about Methyl 2-fluoroacrylate are: (1)ACD/LogP: 0.68; (2)ACD/LogD (pH 5.5): 0.68; (3)ACD/LogD (pH 7.4): 0.68; (4)ACD/BCF (pH 5.5): 1.95; (5)ACD/BCF (pH 7.4): 1.95; (6)ACD/KOC (pH 5.5): 56.12; (7)ACD/KOC (pH 7.4): 56.12; (8)#H bond acceptors: 2; (9)#Freely Rotating Bonds: 2; (10)Polar Surface Area: 26.3 Å²; (11)Index of Refraction: 1.366; (12)Molar Refractivity: 22.08 cm³; (13)Molar Volume: 98.3 cm³; (14)Polarizability: 8.75 ×10^-24cm³; (15)Surface Tension: 21 dyne/cm; (16)Density: 1.057 g/cm³; (17)Flash Point: 1.1 °C; (18)Enthalpy of Vaporization: 31.7 kJ/mol; (19)Boiling Point: 75.9 °C at 760 mmHg; (20)Vapour Pressure: 103 mmHg at 25°C.

When you are using this chemical, please be cautious about it as the following:
This chemical is flammable and it is irritating to eyes, respiratory system and skin. When you are using it, wear suitable protective clothing. And you should keep away from sources of ignition. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1)SMILES: F/C(=C)C(=O)OC
(2)Std. InChI: InChI=1S/C4H5FO2/c1-3(5)4(6)7-2/h1H2,2H3
(3)Std. InChIKey: ZTZJVAOTIOAZGZ-UHFFFAOYSA-N