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2398-37-0

Basic Information
CAS No.: 2398-37-0
Name: 3-Bromoanisole
Molecular Structure:
Molecular Structure of 2398-37-0 (3-Bromoanisole)
Formula: C7H7BrO
Molecular Weight: 187.04
Synonyms: Anisole,m-bromo- (6CI,7CI,8CI);1-Bromo-3-methoxybenzene;3-Methoxy-1-bromobenzene;3-Methoxyphenyl bromide;NSC82293;m-Anisyl bromide;m-Bromoanisole;m-Methoxybromobenzene;
EINECS: 219-264-5
Density: 1.442 g/cm3
Melting Point: 2 °C
Boiling Point: 210.5 °C at 760 mmHg
Flash Point: 93.3 °C
Solubility: Miscible in methanol, benzene, hexane, toluene and dichloromethane. Practically insoluble in water.
Appearance: colorless clear liquid
Hazard Symbols: IrritantXi
Risk Codes:
Safety: 23-24/25
Transport Information:
PSA: 9.23000
LogP: 2.45770
Synthetic route
591-20-8

3-Bromophenol

74-88-4

methyl iodide

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
With potassium hydroxide In tetrahydrofuran for 16h;99%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h;92%
591-20-8

3-Bromophenol

77-78-1

dimethyl sulfate

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
Stage #1: 3-Bromophenol With potassium carbonate In acetone for 0.25h;
Stage #2: dimethyl sulfate In acetone for 10h; Reflux;
95%
With sodium hydroxide
With sodium hydroxide
591-20-8

3-Bromophenol

616-38-6

carbonic acid dimethyl ester

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In sulfolane at 220℃; for 0.166667h;95%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 220℃; for 0.166667h; Inert atmosphere;94%
67-56-1

methanol

585-79-5

3-Bromonitrobenzene

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
Stage #1: methanol With tetrabutyl-ammonium chloride; potassium hydroxide In cyclohexane at 55℃; for 0.0833333h;
Stage #2: m-nitrobromobenzene In cyclohexane at 55 - 60℃; for 3h; Reagent/catalyst;
83%
585-79-5

3-Bromonitrobenzene

124-41-4

sodium methylate

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
With tetrabutylammomium bromide; potassium hydroxide In n-heptane at 20 - 50℃; for 3h; Reagent/catalyst;82%

3-methoxybenzenediazonium o-benzenedisulfonimide

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
With tetrabutylammomium bromide; copper In acetonitrile at 20℃; for 0.75h; Substitution;78%
With tetrabutylammomium bromide In acetonitrile at 60℃; for 0.75h; Substitution;72%
67-56-1

methanol

3-bromophenyl(mesityl)iodonium bromide

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
Stage #1: methanol With sodium hydride In tert-butyl methyl ether; mineral oil at 20℃; for 0.25h; Inert atmosphere; Sealed tube;
Stage #2: 3-bromophenyl(mesityl)iodonium bromide In tert-butyl methyl ether; mineral oil at 50℃; for 1h; Inert atmosphere; Sealed tube; chemoselective reaction;
77%
1464149-60-7

(2,4,6-trimethylphenyl)(3’-methoxyphenyl)iodonium triflate

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
With copper(I) bromide In acetonitrile at 80℃; for 2h;64%
536-90-3

m-Anisidine

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
Stage #1: m-Anisidine With Bromotrichloromethane; sodium nitrite In dichloromethane; water at 23℃; for 0.0833333h;
Stage #2: With acetic acid In dichloromethane; water at 23℃; for 24h; Temperature;
28%
With sulfuric acid; sodium nitrite anschliessend Erwaermen mit Kupfer(I)-bromid;
With hydrogen bromide; sodium nitrite anschliessend Erwaermen mit Kupfer-Pulver;
67-56-1

methanol

m-bromobenzene diazonium nitrate

A

108-86-1

bromobenzene

B

2398-37-0

3-methoxyphenyl bromide

67-56-1

methanol

3-bromo-benzenediazonium; sulfate

A

108-86-1

bromobenzene

B

2398-37-0

3-methoxyphenyl bromide

591-20-8

3-Bromophenol

80-48-8

methyl p-toluene sulfonate

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
With potassium hydroxide
77-78-1

dimethyl sulfate

alkaline m-bromo-phenol

alkaline m-bromo-phenol

2398-37-0

3-methoxyphenyl bromide

3-methoxyphenyl(phenyl)iodonium tetrafluoroborate

A

108-86-1

bromobenzene

B

591-50-4

iodobenzene

C

2398-37-0

3-methoxyphenyl bromide

D

766-85-8

3-methoxy-1-iodobenzene

Conditions
ConditionsYield
With BrNBu4 In chloroform at 55℃;
591-19-5

3-bromoaniline

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aqueous H2SO4 / Diazotization.Kochen der Diazoniumsalz-Loesung
2: aqueous NaOH
View Scheme
Multi-step reaction with 2 steps
1: aqueous H2SO4 / Diazotization.Kochen der Diazoniumsalz-Loesung
2: aqueous KOH
View Scheme
578-57-4

2-bromoanisole

A

2398-37-0

3-methoxyphenyl bromide

B

591-20-8

3-Bromophenol

870485-34-0

(3-methoxyphenyl)(triphenyl-λ5-phosphanyl)gold

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
With N-Bromosuccinimide In chloroform-d1 at 20℃; chemoselective reaction;> 95 %Spectr.
766-85-8

3-methoxy-1-iodobenzene

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid
2: copper(I) bromide / acetonitrile / 2 h / 80 °C
View Scheme
89598-96-9

(3-bromophenyl)boronic acid

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere
1.2: 0.5 h / 20 °C
2.1: sodium hydride / tert-butyl methyl ether; mineral oil / 0.25 h / 20 °C / Inert atmosphere; Sealed tube
2.2: 1 h / 50 °C / Inert atmosphere; Sealed tube
View Scheme
466639-53-2

3-bromo-4-iodoanisole

2398-37-0

3-methoxyphenyl bromide

Conditions
ConditionsYield
With nickel(II) iodide; 1,4-bis(dicyclohexylphosphino)butane; sodium carbonate; cesium iodide In tetrahydrofuran at 35℃; for 72h; Irradiation;
119-61-9

benzophenone

2398-37-0

3-methoxyphenyl bromide

78238-98-9

(3-methoxyphenyl)(diphenyl)methanol

Conditions
ConditionsYield
Stage #1: 3-methoxyphenyl bromide With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere;
Stage #2: benzophenone In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere;
100%
With magnesium 1.) ether, 2.) a) RT, 6 h, b) reflux, 1 h; Yield given. Multistep reaction;
With n-butyllithium
2398-37-0

3-methoxyphenyl bromide

100-66-3

methoxybenzene

Conditions
ConditionsYield
With tetraphenyldisilane; cesium fluoride In acetonitrile at 100℃; for 0.0833333h;100%
With tetrakis(triphenylphosphine) palladium(0); formaldehyd; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h;85%
With N,N,N,N,-tetramethylethylenediamine; C39H46IrN4 In acetonitrile at 45℃; for 48h; Sealed tube; Glovebox; Inert atmosphere;80%
2398-37-0

3-methoxyphenyl bromide

591-31-1

3-methoxy-benzaldehyde

55360-45-7

bis(3-methoxyphenyl)methanol

Conditions
ConditionsYield
With n-butyllithium In hexane; ethyl acetate100%
With magnesium In diethyl ether for 1h; Ambient temperature;62%
With magnesium 1.) ether, ultrasound; Yield given. Multistep reaction;
Stage #1: 3-methoxyphenyl bromide With magnesium In tetrahydrofuran at 0℃; Reflux; Inert atmosphere;
Stage #2: 3-methoxy-benzaldehyde In tetrahydrofuran at 0 - 20℃; Inert atmosphere;
Stage #3: With hydrogenchloride; water In tetrahydrofuran
Stage #1: 3-methoxyphenyl bromide With magnesium In diethyl ether at 20℃; for 2h; Inert atmosphere;
Stage #2: 3-methoxy-benzaldehyde In diethyl ether at 20℃; for 2h; Inert atmosphere;
2398-37-0

3-methoxyphenyl bromide

644-97-3

Dichlorophenylphosphine

216164-54-4

bis(3-methoxyphenyl)(phenyl)phosphine oxide

Conditions
ConditionsYield
Stage #1: 3-methoxyphenyl bromide With magnesium Metallation;
Stage #2: Dichlorophenylphosphine Arylation;
Stage #3: With water; dihydrogen peroxide In tetrahydrofuran Oxidation; Further stages.;
100%
With magnesium Yield given;
2398-37-0

3-methoxyphenyl bromide

98-80-6

phenylboronic acid

2113-56-6

3-methoxybiphenyl

Conditions
ConditionsYield
With potassium phosphate; 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride; bis(η3-allyl-μ-chloropalladium(II)) In 1,4-dioxane at 80℃; for 12h; Suzuki cross-coupling;100%
With potassium carbonate In 5,5-dimethyl-1,3-cyclohexadiene100%
With potassium phosphate; naphthidine di(radical cation)s-stabilized Pd nanoparticles In 1,4-dioxane at 80℃; for 5h; Suzuki-Miyaura cross-coupling reaction;99%
2398-37-0

3-methoxyphenyl bromide

141-32-2

acrylic acid n-butyl ester

346586-17-2

(E)-n-butyl 3-(3-methoxyphenyl)acrylate

Conditions
ConditionsYield
With potassium carbonate; bis(dibenzylideneacetone)-palladium(0); 3-(2,6-diisopropylphenyl)-1-(2-diphenylphosphanylbenzyl)-3H-imidazol-1-ium chloride In N,N-dimethyl acetamide at 140℃; for 12h; Heck reaction;100%
With di-tert-butylneopentylphosphonium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0) In N,N-dimethyl-formamide at 24℃; for 24h; Heck Reaction; Glovebox;98%
With bis(1,1'-ethylene-3,3'-divinylimidazole-2,2'-diylidene)nickel(II) dibromide dihydrate; potassium carbonate In N,N-dimethyl-formamide at 100℃; for 4h; Heck Reaction; Inert atmosphere; Schlenk technique;96%
2398-37-0

3-methoxyphenyl bromide

5471-63-6

1,3-diphenylisobenzofuran

1-methoxy-9,10-diphenyl-9,10-dihydro-9,10-epoxyanthracene

Conditions
ConditionsYield
With Me2Zn(TMP)Li In tetrahydrofuran at 20℃; for 12h;100%
With bis(2,2,6,6-tetramethylpiperidin-1-yl)magnesium-bis(lithium chloride) complex In tetrahydrofuran at -78 - 20℃; for 8h; Inert atmosphere;84%
2398-37-0

3-methoxyphenyl bromide

88-18-6

2-tert-Butylphenol

3-tert-butyl-3'-methoxybiphenyl-2-ol

Conditions
ConditionsYield
With caesium carbonate; diisopropyl(2-tert-butyl)phenoxyphosphine; RhCl(PPh3)3 In toluene for 18h; Heating;100%
2398-37-0

3-methoxyphenyl bromide

536-90-3

m-Anisidine

92248-06-1

3-methoxy-N-(3-methoxyphenyl)benzenamine

Conditions
ConditionsYield
With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 110℃; for 48h; Buchwald-Hartwig amination;100%
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium t-butanolate In toluene at 100℃; for 18h; Buchwald-Hartwig Coupling; Inert atmosphere;72%
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) In toluene at 120℃;40%
With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene for 72h; Reflux; Inert atmosphere;
2398-37-0

3-methoxyphenyl bromide

2142-63-4

1-(3-Bromophenyl)ethanone

1180015-29-5

1-(3-bromo-phenyl)-1-(3-methoxy-phenyl)-ethanol

Conditions
ConditionsYield
Stage #1: 3-methoxyphenyl bromide With bromine; magnesium In diethyl ether at 20℃;
Stage #2: 1-(3-Bromophenyl)ethanone In diethyl ether for 3h; Reflux;
100%
2398-37-0

3-methoxyphenyl bromide

582322-76-7

4-methyl-3-(triisopropylsilyloxy)aniline

1643447-98-6

N-(3-methoxyphenyl)-4-methyl-3-(triisopropylsilyloxy)aniline

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 100℃; for 31h; Buchwald-Hartwig Coupling; Inert atmosphere;100%
2398-37-0

3-methoxyphenyl bromide

27492-84-8

Methyl 4-amino-2-methoxybenzoate

1644060-68-3

methyl 2-Methoxy-4-[(3-methoxyphenyl)amino]benzoate

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 100℃; for 21h; Inert atmosphere;100%
2398-37-0

3-methoxyphenyl bromide

108-44-1

1-amino-3-methylbenzene

1449248-83-2

3-methoxy-N-(3-methylphenyl)aniline

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 100℃; for 15h; Buchwald-Hartwig Coupling; Inert atmosphere;100%
2398-37-0

3-methoxyphenyl bromide

284044-40-2

4-amino-2-(benzyloxy)benzonitrile

4-(3-methoxyphenylamino)-2-benzyloxybenzonitrile

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; caesium carbonate In toluene at 100℃; for 31h; Buchwald-Hartwig Coupling;100%
274-76-0

imidazo[1,2-a]pyridine

2398-37-0

3-methoxyphenyl bromide

1338248-69-3

3-(3-methoxyphenyl)imidazo[1,2-a]pyridine

Conditions
ConditionsYield
With C27H22N4O2Pd; potassium acetate In N,N-dimethyl acetamide at 140℃; for 18h; Catalytic behavior; Schlenk technique; Inert atmosphere;100%
With palladium diacetate; potassium hydroxide In water at 100℃; for 24h; Inert atmosphere;53%
2398-37-0

3-methoxyphenyl bromide

81166-84-9

(2-cyclopropylethynyl)trimethylsilane

445424-01-1

1-(2-cyclopropylethynyl)-3-methoxybenzene

Conditions
ConditionsYield
Stage #1: 3-methoxyphenyl bromide With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; cesium fluoride In water at 20℃; for 0.25h; Sealed tube; Inert atmosphere;
Stage #2: (2-cyclopropylethynyl)trimethylsilane In water at 80℃; for 16h; Sealed tube; Inert atmosphere;
100%
288-32-4

1H-imidazole

2398-37-0

3-methoxyphenyl bromide

10040-94-5

1-(3-methoxyphenyl)-1H-imidazole

Conditions
ConditionsYield
With potassium phosphate; copper(l) iodide; L-lysine at 130℃; for 5h; Microwave irradiation;99%
With copper(l) iodide; N-((4-nitro-1-oxy-pyridin-2-yl)methyl)oxalamic acid; tetrabutylammomium bromide; potassium hydroxide In water at 100℃; for 36h; Schlenk technique; Inert atmosphere; Sealed tube;99%
With potassium tert-butylate; copper(I) oxide In N,N-dimethyl-formamide at 130℃; for 24h;91%
123-39-7

N-Methylformamide

2398-37-0

3-methoxyphenyl bromide

14924-70-0

N-methyl-N-(3-methoxyphenyl)carboxamide

Conditions
ConditionsYield
With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; for 16h;99%
With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; for 16h; Arylation;98%
2398-37-0

3-methoxyphenyl bromide

73183-34-3

bis(pinacol)diborane

401797-04-4

2-(3-bromo-5-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Conditions
ConditionsYield
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1-(4,4'-di-tert-butyl-[2,2'-bipyridin]-6-yl)-2-(dimethyl(phenyl)silyl)-2,3-dihydro-1H-benzo[d][1,3,2]diazaborole Inert atmosphere; Schlenk technique; Sealed tube;99%
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; cyclopentyl methyl ether; 1,1'-di(pyridin-2-yl)-1,1',3,3'-tetrahydro-2,2'-bibenzo[d][1,3,2]diazaborole at 100℃; for 16h; Schlenk technique; Inert atmosphere;96%
With Pinacolborane; 4,4'-di-tert-butylbipyridine In cyclohexane at 80℃;77%
2398-37-0

3-methoxyphenyl bromide

5720-05-8

4-methylphenylboronic acid

24423-07-2

3-methoxy-4'-methylbiphenyl

Conditions
ConditionsYield
With cetyltrimethylammonim bromide; sodium hydroxide In water at 25℃; for 1h; Catalytic behavior; Suzuki Coupling; Microwave irradiation;99%
With caesium carbonate; [PdCl(NNCNHC-nBu)]BF4 In water; N,N-dimethyl-formamide at 80℃; for 2h; Suzuki-Miyaura reaction;95%
With potassium phosphate; N-[(4-diphenylphosphinophenyl)methyl] D-gluconamide; PdCl2(GLCAphos)2 In water at 80℃; for 16h;93%
110-91-8

morpholine

2398-37-0

3-methoxyphenyl bromide

32040-09-8

4-(3-methoxyphenyl)morpholine

Conditions
ConditionsYield
With [Pd(N,N'-bis(2,6-bis(di-p-tolylmethyl)-4-methylphenyl)-imidazol-2-ylidene)(acetylacetonate)Cl]; lithium hexamethyldisilazane In 1,4-dioxane at 110℃; for 3h; Buchwald-Hartwig Coupling; Inert atmosphere; Sealed tube;99%
With sodium t-butanolate; palladium diacetate In toluene at 80℃; for 0.5h; Buchwald-Hartwig amination;98%
With C27H34N5P; sodium hydroxide; bis(dibenzylideneacetone)-palladium(0) In tert-Amyl alcohol at 100℃; Inert atmosphere;97.77%
2398-37-0

3-methoxyphenyl bromide

13922-41-3

1-Naphthylboronic acid

27331-43-7

1-(3-methoxybiphenyl)naphthalene

Conditions
ConditionsYield
With potassium fluoride; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane at 100℃; for 18h; Suzuki coupling;99%
With KF; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) In 1,2-dioxacyclohexane99%
With potassium phosphate In ethanol; water at 20℃; for 1h; Suzuki-Miyaura Coupling; Inert atmosphere; Green chemistry;98%
With ethyl 2-hydroxypropionate; palladium diacetate; potassium carbonate In water at 80℃; for 2h; Suzuki-Miyaura Coupling; Green chemistry;50%
With Br(1-)*C25H29BrN5O6(1+); potassium carbonate In water at 100℃; for 2h; Suzuki-Miyaura coupling;> 99 %Spectr.
2398-37-0

3-methoxyphenyl bromide

16419-60-6

2-Methylphenylboronic acid

135227-03-1

3'-methoxy-2-methyl-1,1'-biphenyl

Conditions
ConditionsYield
With cetyltrimethylammonim bromide; sodium hydroxide In water at 30℃; for 2h; Catalytic behavior; Temperature; Time; Suzuki Coupling; Microwave irradiation;99%
With C20H12N2O8PdS2(2-)*2Na(1+); sodium hydroxide In water at 100℃; for 3h;95%
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; water for 24h; Heating;90%
2398-37-0

3-methoxyphenyl bromide

3866-16-8

3-methoxyphenyl azide

Conditions
ConditionsYield
With sodium azide In ethylene glycol at 100℃; for 3h; Green chemistry;99%
With copper(l) iodide; sodium azide; sodium L-ascorbate; (1S,2S)-N,N'-dimethyl-1,2-diaminocyclohexane In ethanol for 0.666667h; Heating;95%
With copper(l) iodide; sodium azide; L-proline; sodium hydroxide In ethanol at 95℃; for 24h;92%
123-75-1

pyrrolidine

2398-37-0

3-methoxyphenyl bromide

32040-07-6

1-(3-methoxyphenyl)pyrrolidine

Conditions
ConditionsYield
With copper(l) iodide; potassium carbonate; L-proline In dimethyl sulfoxide at 90℃; for 31h;99%
With potassium phosphate; copper(l) iodide; N-((1-oxy-pyridin-2-yl)methyl)oxalamic acid In dimethyl sulfoxide at 80℃; for 48h; Schlenk technique; Inert atmosphere; Sealed tube; chemoselective reaction;71%
With 8-Hydroxyquinoline-N-oxide; caesium carbonate; copper(I) bromide In dimethyl sulfoxide at 50℃; for 60h; Ullmann coupling; Inert atmosphere; Sealed tube; chemoselective reaction;
2398-37-0

3-methoxyphenyl bromide

536-74-3

phenylacetylene

37696-01-8

1-methoxy-3-(phenylethynyl)benzene

Conditions
ConditionsYield
With copper(l) iodide; ethanolamine; bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran; water at 60℃; for 26h; Sonogashira coupling;99%
With UC Pd; potassium carbonate; XPhos In ethanol; water at 50℃; for 5h; Sonogashira coupling; Inert atmosphere;95%
With potassium phosphate; bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)-1,2-ethylenediamine In 1,4-dioxane at 105℃; for 20h; Sonogashira coupling; Inert atmosphere;94%
2398-37-0

3-methoxyphenyl bromide

363-72-4

Pentafluorobenzene

198975-36-9

2,3,4,5,6-pentafluoro-3'-methoxy-1,1'-biphenyl

Conditions
ConditionsYield
With potassium phosphate; chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)]palladium (II); Trimethylacetic acid In N,N-dimethyl acetamide at 80℃; Glovebox;99%
With potassium phosphate; chloro[(tri-tert-butylphosphine)-2-(2-aminobiphenyl)] palladium(II); Trimethylacetic acid In N,N-dimethyl acetamide at 80℃; for 2 - 4h;98%
With [Pd(trifluoroacetato)2(1,3-diisopropylbenzimidazolin-2-ylidene)(C2N3CH2Ph3)]; potassium carbonate In N,N-dimethyl acetamide at 120℃; for 24h;95%
2398-37-0

3-methoxyphenyl bromide

71-43-2

benzene

2113-56-6

3-methoxybiphenyl

Conditions
ConditionsYield
With C34H52Cl2N2Pd; potassium carbonate; Trimethylacetic acid In N,N-dimethyl acetamide at 120℃; for 16h; Reagent/catalyst;99%
With pentamethylcyclopentadienyltricarbonylrhenium for 2.5h; Schlenk technique; Inert atmosphere; UV-irradiation;92%
With potassium tert-butylate at 100℃; for 24h; Inert atmosphere;89%
2398-37-0

3-methoxyphenyl bromide

536-90-3

m-Anisidine

Conditions
ConditionsYield
With bis(tri-ortho-tolylphosphine)palladium(0); (R)-(-)-1-[(S)-2-(dicyclohexylphosphino)ferrocenyl]ethyl-di-tert-butylphosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 80℃; for 5h; Inert atmosphere;99%
With copper(l) iodide; 2-carboxyquinoline N-oxide; potassium carbonate; ammonium hydroxide In dimethyl sulfoxide at 80℃; for 23h; Inert atmosphere;93%
With ammonium hydroxide; copper(l) iodide; diethylenetriaminopentaacetic acid; potassium hydroxide In water at 100℃; for 12h; Sealed tube;90%
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  • High quality M-Bromoanisole supplier in China

  • Casno:

    2398-37-0

    High quality M-Bromoanisole supplier in China

    Min.Order: 0 Metric Ton

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    Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

    Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional

  •  Simagchem Corporation

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:+86-592-2680277

    Address:21/F Hualong Office Building,No.6 Hubin East Road, Xiamen,China

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  • Casno:

    2398-37-0

    1-bromo-3-methoxybenzene

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    Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:86-0311-66561638

    Address:Zhang zhe, guangzong county, xingtai city, hebei province

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  • Casno:

    2398-37-0

    3-Bromoanisole

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  •  Henan Allgreen Chemical Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

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    Address:No 260 Dongming Road,Jinshui District

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    2398-37-0

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    2398-37-0

    3-Bromoanisole

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    Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA.Our main production base is located in Xuzhou industry park. We produce a wide range of organics including Active pharmaceutical ingredients(APIs), Veterinary, Indole derivatives, Aro

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:021-51086038

    Address:High-Tech Industrial park,Chemical Economical Development Zone,Xuzhou, Jiangsu-Province, P.R.China

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  • Casno:

    2398-37-0

    MSDS/COA Download

    3-Bromoanisole in stock

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    As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis

    Dayang Chem (Hangzhou) Co.,Ltd. dedicated to the development, production and marketing of chemicals which is specialized in Organic compounds; Active Pharmaceutical Ingredi

  •  Dayang Chem (Hangzhou) Co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-88938639

    Address:9/F, Unit 2 Changdi Torch Building, 259# WenSan Road, Xihu District, Hangzhou City 310012, P.R.China

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  • Casno:

    2398-37-0

    Factory Supply 3-Bromoanisole

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    3-Bromoanisole Basic information Product Name: 3-Bromoanisole Synonyms: M-BROMOANISOLE;META BROMO ANISOLE;5-bromoanisole;3-BROMO ANISOL;3-BROMOANISOLE;TIMTEC-BB SBB007886;BROMOANISOLE(3-);1-BROMO-3-METHOXYBENZENE CAS: 2398-37-0 MF: C7H7BrO

    Ality Group, established in 2007, is a comprehensive Chemical Supply Group with Patent Technology as its core. Ality Group operates branches in Hong Kong, Singapore and mainland Ch

  •  Ality Chemical Corporation

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:0513-87616220

    Address:Fine chemical industry park, Nantong,Jiangsu

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  • 3-Bromoanisole

  • Casno:

    2398-37-0

    3-Bromoanisole

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    Product Description Product website: http://www.finerchem.com/pro01en/id/1986.html Product Name 3-Bromoanisole CAS No. 2398-37-0 A

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-531-88989536

    Address:New Material Industry Park, Jinan Ciyt, China

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    2398-37-0

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    Good quantity 3-Bromoanisole Basic information Product Name: 3-Bromoanisole Synonyms: M-BROMOANISOLE;META BROMO ANISOLE;BROMOANISOLE(3-);1-BROMO-3-METHOXYBENZENE;5-bromoanisole;3-BROMO

    Our company engages in Electronic chemicals such as OLED,Photoresist chemical,Electrolyte additive and Intermediate Pharmaceutical production; development of noble metal catalysts,

  •  Henan Tianfu Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-371-55170693/55170694

    Address:Zhengzhou International Trade New Territory,Jinshui District,Zhengzhou ,China

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    2398-37-0

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    Hubei Xinrunde Chemical Co., Ltd. dedicated to the development, production and marketing of chemicals which is specialized in Organic compounds; Active Pharmaceutical Ingredient(s)

  •  Hubei XinRunde Chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+8615102730682

    Address:No.43, Xinandu Industrial Park, East and West Lake District, Wuhan, Hubei, China

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    2398-37-0

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-18871490254

    Address:High-tech Industrial Park,Tianmen city,Hubei province.

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    2398-37-0

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    WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

    Zhuo Zhou Wen Xi Import and Export Co., Ltd. is a company mainly engaged in the export of pharmaceutical raw materials. Its parent company is (Wen Xi Pharma), including three subs

  •  Zhuozhou Wenxi import and Export Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-13111626072

    Address:Room 1710, Baoxin International Phase I, 19 Guanyun East Road, Zhuozhou, Hebei

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    2398-37-0

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    BLOOM TECH Advanced API/Technology support 1-Bromo-3-methoxybenzene CAS 2398-37-0

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    WHO WE ARE 1.We Focus on the technology of Organic Synthesis since 2008. 2.API/Pharmaceutical intermediate/Fine chemical/New material/Extraction etc. 3.Chemical reagent: Over 300,0

  •  Shaanxi BLOOM TECH Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-29-86470566

    Address:Block A of Central Mansion, No.113 of Weiyang Rd, ETDZ, Xi'an, Shaanxi 710016, China

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    2398-37-0

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    Mulei (Wuhan) New Material Technology Co. Ltd is a scientific and technological company integrating product research and development, manufacture and trading of chemical intermedia

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8619831967063

    Address:Office1201#, Block C, Hanjie Headquarters International Plaza, Zhongbei Rd, Wuchang District, Wuhan

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    2398-37-0

    m-Bromoanisole ;3-Bromoanisole

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    ProName: 3-Bromoanisole CasNo: 2398-37-0 Molecular Formula: C7H7BrO Appearance: liquid Application: Pharmaceutical intermediates DeliveryTime: 10day PackAge: According to the demand of customer Port: shanghai Prod

    Antimex Chemical Limied, was founded in 2001, we are specializing in manufacturing & researching of Active pharmaceutical Ingredients,Veterinary pharm APIs,cosmetic ingredients,and

  •  Antimex Chemical Limied

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-21-50563169

    Address:Room1027,No.Jinyu Road,Pudong

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  • Casno:

    2398-37-0

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    We are Hebei miaobian Biotechnology Co., Ltd , mainly deal in pharmaceutical intermediates and various chemicals. It is with a registered capital of 3 million yuan, is one of the m

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:17633233896

    Address:Federal Business Plaza, Qiaoxi District,Shijiazhuang

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    2398-37-0

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    Shanghai Upbio Tech Co.,Ltd (Former Onchem (China)Co.,Ltd) is a comprehensive manufacturer and an international distribution of chemicals throughout the world, The predecessor of

  •  Shanghai Upbio Tech Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-21-52196435

    Address:No.2 Floor,No.979 Yunhan Rd,Nicheng,Pudong New Area,Shanghai,China

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  • Casno:

    2398-37-0

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    Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.1) Standard:BP/USP/EP/Enterprise standard2) All Purity≥99%3) We are manufacturer and can provide high quality products with factory pric

    Shaanxi Mingqi Chemical Co., Ltd is committed to the development of import and export trade in the production, operation and plant extracts of pharmaceutical raw materials and inte

  •  Shaanxi Mingqi Chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:18092428356

    Address:Weiyang District

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  • 3-Bromoanisole 2398-37-0 supplier

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    2398-37-0

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Address:13th Floor, Tower B, Century Plaza, Zhongnan Road, Wuchang District, Wuhan, China.

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    2398-37-0

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Address:No.66, Yuhua West Road

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    2398-37-0

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    Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

    Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, special chemicals and OLED materials &

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:86-592-3327115

    Address:Unit 603,No.879,Xiahe Road,Meixin Building,Xiamen,China

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    2398-37-0

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-371-86658258

    Address:Building 3 of Innovation Park, East District of the National University Science Park

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    2398-37-0

    3-Bromoanisole

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    span lang="EN-US" style="font-size: 9.0pt;font-family:"Arial",sans-serif;color:#4D4D4D">As a leading manufacturer and supplier of chemicals in china, weckchem not only supply popular chemicals, but also weckchem’s r&d center off

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     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86-15158040660

    Address:Xiaoshan district

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  • 3-BROMOANISOLE

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    2398-37-0

    3-BROMOANISOLE

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    Betterbiochem is specialized in APIs, pharmaceutical intermediates & fine chemicals. 1. The best quality, competitive price. 2. The best service before or after shipment. 3. Rich experience in export operation. 4. Rich experience in

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-18013506594

    Address:No. 8 Building, 18 nong, Xi Yingnan Road, Pudong, Shanghai,China

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    2398-37-0

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    Product Name: 3-Bromoanisole Synonyms: m-Bromophenylmethylether;m-Methoxybromobenzene;m-Methoxyphenyl bromide;m-Bromoanisoles;m-bromoanisole(MBA);3-BROMOANISOLE, 98+%;3-Bromoanisole99%;3-BROMO ANISOLE FOR SYNTHESIS CAS: 2398-37-0 MF: C7H7BrO

    Wuhan Zenuo Biopharmaceutical Technology Co., Ltd. is a global biopharmaceutical and chemical enterprise, mainly engaged in the customized synthesis, large-scale production and sal

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:(+86-27)8700-2750

    Address:Floor 19th,No.76,Longyang Road

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    2398-37-0

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    We, Jilin Tely Imp & Exp Co., Ltd. mainly supply and export products including: pharmaceutical raw materials,Chemical reagents, Food additives, pharmaceutical and pesticide interme

  •  Jilin Tely Imp.& Exp.Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-431-81915458

    Address:Room 302, 47 Changping Street, Chaoyang District, Changchun, Jilin Province,China

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    2398-37-0

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    Hangzhou Jinlan Pharm-Drugs Technology Co.,Ltd is located in Hangzhou, Zhejiang Province. Neighboring Ningbo port, Shanghai port, Hangzhou Xiaoshan Int’l Airport and Shanghai Pudon

  •  Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-571-85829053

    Address:Rm A606, Fuyi Center, jianqiao street, Jianggan Area

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    2398-37-0

    3-Bromoanisole

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    Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

    Shandong Hanjiang Chemical Co., Ltd. is located in Qilu Petrochemical Industrial Park, Zibo City, Shandong Province, involving pesticide, medicine, chemical industry, coating, dy

  •  Shandong Hanjiang Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:18369939125

    Address:95A, Xingyuan East Road, Zhangdian District

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    2398-37-0

    3-BROMOANISOLE

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    Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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    2398-37-0

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    J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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    3-Bromoanisole Basic information

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Specification

1. Introduction of 3-Bromoanisole
3-Bromoanisole is also named as 1-Bromo-3-methoxybenzene; 3-Methoxy-1-bromobenzene; 3-Methoxybromobenzene; NSC 82293; m-Bromoanisole; m-Bromomethoxybenzene; m-Bromophenyl methyl ether; m-Methoxybromobenzene. 3-Bromoanisole is colorless clear liquid.

2. Properties of 3-Bromoanisole
Melting Point: 2 °C
Boiling Point: 210.5 °C at 760 mmHg 
Flash Point: 93.3 °C
Index of Refraction: 1.539
Molar Refractivity: 40.62 cm3
Molar Volume: 129.6 cm3
Surface Tension: 34.6 dyne/cm 
Enthalpy of Vaporization: 42.86 kJ/mol
Vapour Pressure: 0.278 mmHg at 25 °C
XLogP3: 3
H-Bond Acceptor: 1
Rotatable Bond Count: 1
Exact Mass: 185.968027
MonoIsotopic Mass: 185.968027
Topological Polar Surface Area: 9.2
Heavy Atom Count: 9

3. Structure Descriptors of 3-Bromoanisole
Canonical SMILES: COC1=CC(=CC=C1)Br
InChI: InChI=1S/C7H7BrO/c1-9-7-4-2-3-6(8)5-7/h2-5H,1H3
InChIKey: PLDWAJLZAAHOGG-UHFFFAOYSA-N

4. Safety Information of 3-Bromoanisole

Hazard Codes: IrritantXi
Safety Statements: 23-24/25 
S23:Do not breathe vapour. 
S24/25:Avoid contact with skin and eyes.
WGK Germany: 3
F: 8
Hazard Note: Irritant
TSCA: T
HS Code: 29093038 

5. Use of
3-Bromoanisole
3-Bromoanisole is used in organic synthesis.

6. Preparation of 3-bromoanisole
Comprising methoxydenitrating 3-bromonitrobenzene in the presence of a phase-transfer catalyst (PTC), and the preparation of 3-bromonirtobenzene by the bromination of nitrobenzene with bromine in oleum. The methoxydenitration reagent in an alkali metal methoxide, which is selected from sodium methoxide and potassium methoxide. The amount of methoxide used is 1-1.5 mol per mol of 3-bromonitrobenzene. The alkali methoxide can be a pre-prepared solid or it can be prepared in situ, by the reaction of the corresponding alkali hydroxide and methanol. In the case when pre-prepared solid methoxide is used, the effective amount of alkali hydroxide is between 1.2-1.7 mol per mol of 3-bromonitrobenzebe. The reaction temperatures are between about 40 to 80° C., with preference to reaction temperatures of 50 to 55° C. In the case in which methoxide is prepared in situ, the effective amount of alkali hydroxide is between 2.2-2.4 mol per mol of 3-bromonitrobenzene. The reaction temperatures are between about 50 to 80° C. with preference to reaction temperatures of 55 to 65° C.