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| CAS No.: | 25505-64-0 |
|---|---|
| Name: | 2,5-DIMETHOXY-4-METHYL-BETA-NITROSTYRENE, >95% |
| Article Data: | 3 |
| Molecular Structure: | |
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|
| Formula: | C11H13NO4 |
| Molecular Weight: | 223.229 |
| Synonyms: | Benzene, 1,4-dimethoxy-2-methyl-5-(2-nitroethenyl)- (en); |
| Density: | 1.168±0.06 g/cm3(Predicted) |
| Melting Point: | 126 °C |
| Boiling Point: | 363.0±37.0 °C(Predicted) |
| PSA: | 64.28000 |
| LogP: | 2.78280 |
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- 73441-42-6METHYL-5-CHLORO-2,2-DIMETHYLVALERATE
- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 75-52-5
nitromethane
- 4925-88-6
2,5-dimethoxy-4-methylbenzaldehyde
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
| Conditions | Yield |
|---|---|
| With ammonium acetate In benzene | |
| With potassium hydroxide; sodium acetate; acetic anhydride 1) ethanol, water, 5 deg C, 2 days 2) reflux, 20 min.; Yield given. Multistep reaction; |
- 95-71-6
2-methylbenzene-1,4-diol
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: 82 percent / potassium hydroxide / methanol / 8 h / steam distillation 2: 1) HCl, aluminium chloride 2) aqueous H2SO4 / 1) tetrachloroethane, 8 h, 65-70 deg C 2) overnight, room temperature 3) steam distillation 3: 1) KOH 2) acetic anhydride, sodium acetate / 1) ethanol, water, 5 deg C, 2 days 2) reflux, 20 min. View Scheme |
- 24599-58-4
2,5-dimethoxy toluene
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 1) HCl, aluminium chloride 2) aqueous H2SO4 / 1) tetrachloroethane, 8 h, 65-70 deg C 2) overnight, room temperature 3) steam distillation 2: 1) KOH 2) acetic anhydride, sodium acetate / 1) ethanol, water, 5 deg C, 2 days 2) reflux, 20 min. View Scheme |
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
- 74422-80-3
2,5-dimethoxy-4-methyl-6,β-dinitrostyrene
| Conditions | Yield |
|---|---|
| With nitric acid at 0℃; for 0.416667h; | 5% |
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
- 124-41-4
sodium methylate
- 98537-47-4
1-(2,5-dimethoxy-4-methylphenyl)-1-methoxy-2-nitroethane
| Conditions | Yield |
|---|---|
| 1.) methanol; 2.) methanol, 0 deg C, 4 h; Yield given. Multistep reaction; |
- 685-91-6
diethylacetamide
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
- 33877-68-8
N,N-Diethyl-3-(2,5-dimethoxy-4-methylphenyl)-4-nitrobutyramid
| Conditions | Yield |
|---|---|
| (i) nBuLi, THF, hexane, (ii) /BRN= 1209428/; Multistep reaction; |
- 127-19-5
N,N-dimethyl acetamide
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
- 33877-59-7
3-(2,5-Dimethoxy-4-methylphenyl)-N,N-dimethyl-4-nitrobutyramid
| Conditions | Yield |
|---|---|
| (i) LDA, THF, hexane, (ii) /BRN= 2505975/, AcOH; Multistep reaction; |
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
- 24333-19-5
alpha demethyl DOM
| Conditions | Yield |
|---|---|
| With lithium aluminium tetrahydride In tetrahydrofuran |
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
- 42203-89-4
1-(2,5-Dimethoxy-4-methyl-phenyl)-2-nitroethan
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate In 1,4-dioxane |
- 25505-64-0
1-(2,5-dimethoxy-4-methylphenyl)-2-nitroethene
- 42203-90-7
2,4-Di-(2,5-dimethoxy-4-methylphenyl)-1,3-dinitrobutan
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate In 1,4-dioxane |
- Total:20 Page 1 of 1 1
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