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2592-18-9

Basic Information
CAS No.: 2592-18-9
Name: Boc-L-Threonine
Article Data: 98
Molecular Structure:
Molecular Structure of 2592-18-9 (Boc-L-Threonine)
Formula: C9H17NO5
Molecular Weight: 219.238
Synonyms: Threonine,N-carboxy-, N-tert-butyl ester (7CI);Threonine, N-carboxy-, N-tert-butylester, L- (8CI);L-N-(tert-Butoxycarbonyl)threonine;N-(tert-Butoxycarbonyl)threonine;N-BOC-L-Threonine;N-tert-Butoxycarbonyl-L-threonine;N-tert-Butyloxycarbonyl-L-threonine;N-a-tert-Butoxycarbonyl-L-threonine;NSC 334305;
EINECS: 219-987-6
Density: 1.202 g/cm3
Melting Point: 80-82 °C(lit.)
Boiling Point: 387.1 °C at 760 mmHg
Flash Point: 187.9 °C
Appearance: White amorphous powder
Hazard Symbols: HarmfulXn
Risk Codes: 20/21/22-36/37/38
Safety: 24/25-36-26
PSA: 95.86000
LogP: 0.73600
Synthetic route
72-19-5

L-threonine

24424-99-5

di-tert-butyl dicarbonate

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With sodium hydrogencarbonate In methanol; water at 20℃; for 72h;99%
With sodium hydroxide In 1,4-dioxane; water at 0 - 20℃; for 24h;99%
With sodium carbonate In acetone at 20℃; Cooling with ice;95%
72-19-5

L-threonine

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With triethylamine In water; N,N-dimethyl-formamide for 8h; Ambient temperature;98%
89985-91-1

tert-butyl pyridin-2-yl carbonate

L-threonine, dicyclohexylammonium salt

A

142-08-5

2-hydroxypyridin

B

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With triethylamine In water; N,N-dimethyl-formamide for 8h; Ambient temperature;A n/a
B 98%
72-19-5

L-threonine

75844-68-7

tert-butyl 2-oxo-1,3-oxazole-3(2H)-carboxylate

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With dmap In 1,4-dioxane; water for 15h; Ambient temperature;96%
15260-10-3

N-Boc-O-benzyl-L-threonine

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With ammonium formate; magnesium In ethylene glycol for 0.05h; microwave irradiation;95%
With magnesium; hydrazinium monoformate In methanol at 25℃; for 1h;90%
With formic acid; palladium on activated charcoal In methanol at 20℃; for 0.0833333h;
105678-24-8

O-(tert-butyl) S-(pyridin-2-yl)carbonothioate

L-threonine, dicyclohexylammonium salt

A

2637-34-5

2-Mercaptopyridine

B

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With triethylamine In water; N,N-dimethyl-formamide for 12h; Ambient temperature;A n/a
B 92%
77313-56-5

Boc-Thr-ONbn

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride In N,N-dimethyl-formamide Ambient temperature;90%
126587-71-1

Boc-threonine [(2-trimethylsilyl)ethoxy]methyl ester

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With magnesium bromide In dichloromethane for 4h; Ambient temperature; addition at -20 deg C, 0.5 h;80%
72-19-5

L-threonine

104272-95-9

t-butyl S-3,6-diisopropylpyrazin-2-ylthiolcarbonate

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With dmap; triethylamine In water; acetonitrile for 24h; Ambient temperature;51%
72-19-5

L-threonine

104272-92-6

2-t-butoxycarbonyloxy-3,6-diisopropylpyrazine

2592-18-9

Boc-Thr-OH

Conditions
ConditionsYield
With triethylamine In water; acetonitrile for 24h; Ambient temperature;48%
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Chemistry

The molecular formula of Boc-L-Threonine(2592-18-9) is C9H17NO5  and its formula weight is 219.23.
Boc-L-Threonine(2592-18-9) has a  melting point of  80-82 °C(lit.).The refractive index is about  -7 ° (C=1, AcOH).
The chemical synonyms of Boc-L-Threonine(2592-18-9) are N-TERT-BUTYLOXYCARBONYL-L-THREONINE;N-(TERT-BUTOXYCARBONYL)-L-THREONINE;N-(TERT-BUTOXYCARBONYL)-P-THREONINE;N-T-BUTOXYCARBONYL-L-THREONINE;N-BOC-L-THREONINE;N-ALPHA-T-BUTOXYCARBONYL-L-THREONINE;N-ALPHA-TERT-BUTYLOXYCARBONYL-L-THREONINE;N-ALPHA-T-BOC-L-THREONINE
The molecular structure of Boc-L-Threonine(2592-18-9):

Toxicity Data With Reference

RTECS#: CAS# 2592-18-9: None listed
LD50/LC50: RTECS: Not available. 
Carcinogenicity: BOC-L-Threonine - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65.
Other: The toxicological properties have not been fully investigated.

Safety Profile

Hazard Codes  Xn
Risk Statements  20/21/22-36/37/38
Safety Statements  24/25-36-26
WGK Germany  3

Specification

Chemical Stability: Stable under normal temperatures and pressures. 
Conditions to Avoid: Incompatible materials. 
Incompatibilities with Other Materials Strong oxidizing agents. 
Hazardous Decomposition Products Carbon monoxide, oxides of nitrogen, carbon dioxide. 
Hazardous Polymerization Will not occur.