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2605-14-3

Basic Information
CAS No.: 2605-14-3
Name: 2-Chloro-6-methoxybenzothiazole
Article Data: 14
Molecular Structure:
Molecular Structure of 2605-14-3 (2-Chloro-6-methoxybenzothiazole)
Formula: C8H6ClNOS
Molecular Weight: 199.661
Synonyms: 2-Chloro-6-methoxy-1,3-benzothiazole;2-Chloro-6-methoxybenzo[d]thiazole;6-Methoxy-2-chlorobenzothiazole;NSC 118120;
Density: 1.404 g/cm3
Melting Point: 54°C
Boiling Point: 293.495 °C at 760 mmHg
Flash Point: 131.302 °C
Hazard Symbols: HarmfulXn, IrritantXi
Risk Codes: 22-36
Safety: 26
PSA: 50.36000
LogP: 2.95830
Synthetic route
1747-60-0

6-methoxybenzothiazol-2-ylamine

2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

Conditions
ConditionsYield
With polyethylene glycol; copper dichloride; isopentyl nitrite In acetonitrile at 65℃; for 3h;83.5%
Stage #1: 6-methoxybenzothiazol-2-ylamine With sodium nitrite In ethanol at 15℃; for 3h;
Stage #2: With hydrogenchloride; copper(l) chloride In water at 60℃; for 2h;
78.1%
Stage #1: 6-methoxybenzothiazol-2-ylamine With hydrogenchloride; sodium nitrite In ethanol; water at 15℃; for 3h;
Stage #2: With copper(l) chloride In ethanol; water at 60℃; for 2h;
69.5%
75-15-0

carbon disulfide

104-94-9

4-methoxy-aniline

2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

Conditions
ConditionsYield
(i) KSCN, Br2, (ii) aq. NaOH, (iii) /BRN= 1098293/, (iv) SO2Cl2; Multistep reaction;
diazotized 6-methoxy-benzothiazol-2-ylamine

diazotized 6-methoxy-benzothiazol-2-ylamine

2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

Conditions
ConditionsYield
With hydrogenchloride; copper(l) chloride
20174-70-3

2-hydrazinyl-6-methoxybenzo[d]thiazole

2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

Conditions
ConditionsYield
With thionyl chloride at 50℃; for 2h;
104-94-9

4-methoxy-aniline

2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: bromine; acetic acid / 0.5 h / 0 °C
2: hydrazine hydrochloride; hydrazine hydrate / ethylene glycol / 2 h / 140 °C
3: thionyl chloride / 2 h / 50 °C
View Scheme
2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

2591-16-4

2-chloro-6-hydroxy-benzothiazole

Conditions
ConditionsYield
With boron trichloride; tetra-(n-butyl)ammonium iodide In n-heptane; dichloromethane at -78 - 20℃;95%
With aluminum (III) chloride In toluene at 110℃; for 1.5h;93%
With boron tribromide In dichloromethane at -10 - 25℃; for 64h;86%
2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

62-53-3

aniline

539811-75-1

6-methoxy-N-phenylbenzo[d]thiazol-2-amine

Conditions
ConditionsYield
at 100℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube; Green chemistry;90%
2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

536-74-3

phenylacetylene

1440509-66-9

C16H11NOS

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In N,N-dimethyl-formamide at 20℃; for 33h; Catalytic behavior; Sonogashira Cross-Coupling; Inert atmosphere; Schlenk technique;87%
2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

4-(6'-methoxy-benzothiazole-2'-yloxy)-1-oxyl-2,2,6,6-tetramethylpiperidine

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 20℃;84.6%
With sodium hydride In N,N-dimethyl-formamide at 20℃;84.6%
2605-14-3

2-chloro-6-(methyloxy)-1,3-benzothiazole

potassium vinyltrifluoroborate

C10H9NOS

Conditions
ConditionsYield
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; triethylamine In isopropyl alcohol for 16h; Reflux; Inert atmosphere;83%
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  • 2605-14-3            C8H6ClNOS           2-Chloro-6-methoxybenzothiazole

  • Casno:

    2605-14-3

    2605-14-3 C8H6ClNOS 2-Chloro-6-methoxybenzothiazole

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    2-Chloro-6-methoxybenzothiazole Basic information Product Name: 2-Chloro-6-methoxybenzothiazole Synonyms: 2-CHLORO-6-METHOXYBENZO[D]THIAZOLE;2-CHLORO-6-METHOXYBENZO

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Chemistry

Molecular Formula: C8H6ClNOS
Molar mass: 199.6573 g/mol
Density: 1.404 g/cm3
Melting point: 54°C
Flash Point: 131.3 °C
Index of Refraction: 1.654
Boiling Point: 293.5 °C at 760 mmHg
Vapour Pressure: 0.00301 mmHg at 25°C
Structure of 2-Chloro-6-methoxybenzothiazole (2605-14-3) :
                          
Synonyms of 2-Chloro-6-methoxybenzothiazole (2605-14-3) : Chloromethoxybenzothiazole ; 2-Chloro-6-methoxy-1,3-benzothiazole ; 2-Chloro-6-methoxybenzo[d]thiazole
Product Categories of 2-Chloro-6-methoxybenzothiazole (2605-14-3) : Heterocycles series;Thiazoles;Halogenated Heterocycles;BENZOTHIAZOLE;Thiazoles Heterocyclic Building Blocks

Safety Profile

Hazard Note: Irritant
Hazard Codes: Xi,Xn
Risk Statements:
22:  Harmful if swallowed 
36:  Irritating to the eyes
Safety Statements:
22:  Do not breathe dust
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice