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2697-85-0

Basic Information
CAS No.: 2697-85-0
Name: ANDROST-5-EN-3B ,7,17B -TRIOL
Article Data: 14
Molecular Structure:
Molecular Structure of 2697-85-0 (ANDROST-5-EN-3B ,7,17B -TRIOL)
Formula: C19H30 O3
Molecular Weight: 306.445
Synonyms: Androst-5-ene-3b,7b,17b-triol (7CI,8CI); 3b,7b,17b-Androst-5-enetriol
Density: 1.19±0.1 g/cm3(Predicted)
Melting Point: 235-237℃
Boiling Point: 474.3±45.0 °C(Predicted)
PSA: 60.69000
LogP: 2.64180
Synthetic route
566-19-8

5-androstene-3β-ol-7,17-dione

2697-85-0

5-androstene-3β,7β,17β-triol

Conditions
ConditionsYield
With sodium tetrahydroborate; cerium(III) chloride In methanol; dichloromethane at 0 - 5℃; for 0.5h; pH=15;88%

A

2226-65-5

3beta,17beta-Dihydroxyandrost-5-en-7-one

B

2697-85-0, 62357-04-4, 2226-66-6

Androst-5-ene-3beta,7alpha,17beta-triol

C

2697-85-0

5-androstene-3β,7β,17β-triol

Conditions
ConditionsYield
With Mortierella isabellina AM212 fungal strain for 24h; Enzymatic reaction;A 8.2%
B 47.9%
C 21.8%
With Absidia coerulea AM93 In methanol at 20℃; for 48h; Time; Enzymatic reaction;A 3%
B 23%
C 45%
53-43-0

dehydroepiandrosterone

A

2487-48-1, 7522-54-5, 62357-03-3, 53-00-9

3β,7α-dihydroxyandrost-5-ene-17-one

B

2697-85-0, 62357-04-4, 2226-66-6

Androst-5-ene-3beta,7alpha,17beta-triol

C

2697-85-0

5-androstene-3β,7β,17β-triol

Conditions
ConditionsYield
With Mucor silvaticus In acetone at 28℃; for 96h; regioselective reaction;A 38.4%
B 14.7%
C 6.2%
13209-60-4

3β, 17β-diacetoxyandrost-5-ene-7-one

2697-85-0

5-androstene-3β,7β,17β-triol

Conditions
ConditionsYield
With aluminum isopropoxide; isopropyl alcohol Abdestillieren des entstehenden Acetons;
With aluminum isopropoxide; isopropyl alcohol Abdestillieren des entstehenden Acetons;
13209-60-4

3β, 17β-diacetoxyandrost-5-ene-7-one

555-31-7

aluminum isopropoxide

67-63-0

isopropyl alcohol

2697-85-0

5-androstene-3β,7β,17β-triol

Conditions
ConditionsYield
unter Abdestillieren des entstehenden Acetons;
2099-26-5

androstenediol-3,17-diacetate

2697-85-0

5-androstene-3β,7β,17β-triol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: CrO3; aqueous acetic acid / 60 °C
2: aluminium isopropylate; isopropyl alcohol / Abdestillieren des entstehenden Acetons
View Scheme
13209-60-4

3β, 17β-diacetoxyandrost-5-ene-7-one

L-Selectride

2697-85-0

5-androstene-3β,7β,17β-triol

Conditions
ConditionsYield
With potassium hydroxide; sodium chloride In tetrahydrofuran; methanol
566-19-8

5-androstene-3β-ol-7,17-dione

A

2226-65-5

3beta,17beta-Dihydroxyandrost-5-en-7-one

B

2697-85-0, 62357-04-4, 2226-66-6

Androst-5-ene-3beta,7alpha,17beta-triol

C

2697-85-0

5-androstene-3β,7β,17β-triol

Conditions
ConditionsYield
With Mortierella isabellina AM212 fungal strain for 12h; Enzymatic reaction;A 3.5 %Chromat.
B 30 %Chromat.
C 12 %Chromat.
Conditions
ConditionsYield
With water In ethanol for 120h; Microbiological reaction;

A

58-22-0

testosterone

B

2487-48-1

5-androsten-3β,7β-diol-17-one

C

2697-85-0, 62357-04-4, 2226-66-6

Androst-5-ene-3beta,7alpha,17beta-triol

D

2697-85-0

5-androstene-3β,7β,17β-triol

Conditions
ConditionsYield
With water In ethanol for 120h; Microbiological reaction;
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