Products Categories
| CAS No.: | 29133-55-9 |
|---|---|
| Name: | L-Prolinamide, N-[(1,1-dimethylethoxy)carbonyl]-L-histidyl- |
| Article Data: | 5 |
| Molecular Structure: | |
|
|
|
| Formula: | C16H25N5O4 |
| Molecular Weight: | 351.406 |
| Synonyms: | L-Prolinamide,N-[(1,1-dimethylethoxy)carbonyl]-L-histidyl;Boc-His-Pro-NH2;tert-Butyl ((S)-1-((S)-2-carbamoylpyrrolidin-1-yl)-3-(1H-imidazol-4-yl)-1-oxopropan-2-yl)carbamate; |
| PSA: | 130.41000 |
| LogP: | 1.35090 |
- 483366-12-7(2S,4R)-1-Boc-2-cyano-4-hydroxypyrrolidine
- 361456-36-2METHYL (R)-(+)-ISOCYANATO-3-PHENYLPROPI&
- 5156-58-1N-(1-Benzyl-4-pipperidinyl)-N-phenylpropanamide HCl
- 81281-59-67-Benzylideneaminotheophylline
- 50288-62-5threo-Phenyl-2-piperidyl acetamide
- 82993-81-5D-threo-Ritalinic acid hydrochloride
- 47087-37-6Z-D-Glu-OMe
- 73441-42-6METHYL-5-CHLORO-2,2-DIMETHYLVALERATE
- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 17791-52-5
N-(tert-butoxycarbonyl)-L-histidine
- 7531-52-4
L-prolinamide
- 29133-55-9
N(α)-t-butoxycarbonyl-L-histidyl-L-prolineamide
| Conditions | Yield |
|---|---|
| Stage #1: N-(tert-butoxycarbonyl)-L-histidine With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 25℃; for 2h; Stage #2: L-prolinamide In N,N-dimethyl-formamide at 25℃; for 18h; | 73% |
| Stage #1: N-(tert-butoxycarbonyl)-L-histidine With HONB; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 0.25h; Stage #2: L-prolinamide In N,N-dimethyl-formamide at 20℃; |
- 42429-27-6
L-prolinamide hydrochloride
- 83468-77-3
N(α)-t-butoxycarbonyl-2,5-dibromo-L-histidine
A
- 50654-97-2
N(α)-t-butoxycarbonyl-D-histidyl-L-prolineamide
B
- 29133-55-9
N(α)-t-butoxycarbonyl-L-histidyl-L-prolineamide
| Conditions | Yield |
|---|---|
| With palladium on activated charcoal; Rh on carbon; Amberlite IR 45 (acetate form); hydrogen; triethylamine; dicyclohexyl-carbodiimide 1.) DMF, 0 deg C, 4 h, 2.) aq. AcOH, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
- 42429-27-6
L-prolinamide hydrochloride
- 72240-57-4
N(α)-t-butoxycarbonyl-2,5-di-iodo-L-histidine
A
- 50654-97-2
N(α)-t-butoxycarbonyl-D-histidyl-L-prolineamide
B
- 29133-55-9
N(α)-t-butoxycarbonyl-L-histidyl-L-prolineamide
| Conditions | Yield |
|---|---|
| With palladium on activated charcoal; rhodium on CaCO3; hydrogen; triethylamine; dicyclohexyl-carbodiimide 1.) DMF, 0 deg C, 4 h, 2.) DMF, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
- 42429-27-6
L-prolinamide hydrochloride
- 20898-44-6
Boc-His(Bzl)-OH
A
- 50654-97-2
N(α)-t-butoxycarbonyl-D-histidyl-L-prolineamide
B
- 29133-55-9
N(α)-t-butoxycarbonyl-L-histidyl-L-prolineamide
| Conditions | Yield |
|---|---|
| With palladium on activated charcoal; hydrogen; triethylamine; dicyclohexyl-carbodiimide 1.) DMF, 0 deg C, 4 h, 2.) aq. AcOH, 72 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
- 83468-76-2
(S)-methyl 2-(tert-butoxycarbonylamino)-3-(2,5-dibromo-1H-imidazol-4-yl)propanoate
- 29133-55-9
N(α)-t-butoxycarbonyl-L-histidyl-L-prolineamide
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 73 percent / NaOH / methanol / 1 h 2: 1.) DCC, Et3N, 2.) Pd-C, H2, Rh-C, Amberlite IR 45 (acetate form) / 1.) DMF, 0 deg C, 4 h, 2.) aq. AcOH, 2 h View Scheme |
- 2488-14-4
N-(tert-butoxycarbonyl)-L-histidine methyl ester
- 29133-55-9
N(α)-t-butoxycarbonyl-L-histidyl-L-prolineamide
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: 25 percent / Et3N, Br2 / CHCl3 / 0 deg C to room temperature 2: 73 percent / NaOH / methanol / 1 h 3: 1.) DCC, Et3N, 2.) Pd-C, H2, Rh-C, Amberlite IR 45 (acetate form) / 1.) DMF, 0 deg C, 4 h, 2.) aq. AcOH, 2 h View Scheme |
- 76-05-1
trifluoroacetic acid
- 29133-55-9
N(α)-t-butoxycarbonyl-L-histidyl-L-prolineamide
- 74528-30-6
trifluoroacetate salt of L-histidyl-L-prolinamide
| Conditions | Yield |
|---|---|
| In dichloromethane at 0℃; for 1h; |
- 29133-55-9
N(α)-t-butoxycarbonyl-L-histidyl-L-prolineamide
| Conditions | Yield |
|---|---|
| With hydrogenchloride In methanol |
- Total:32 Page 1 of 1 1
What can I do for you?
Get Best Price
