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29241-65-4

Basic Information
CAS No.: 29241-65-4
Name: 5-Bromo-2-chloronicotinic acid
Article Data: 13
Molecular Structure:
Molecular Structure of 29241-65-4 (5-Bromo-2-chloronicotinic acid)
Formula: C6H3BrClNO2
Molecular Weight: 236.452
Synonyms: Nicotinicacid, 5-bromo-2-chloro- (8CI);2-Chloro-5-bromonicotinic acid;
Density: 1.917 g/cm3
Melting Point: 173-176 °C
Boiling Point: 345.1 °C at 760 mmHg
Flash Point: 162.5 °C
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/37/39
PSA: 50.19000
LogP: 2.19570
Synthetic route
104612-36-4

5-bromo-2-hydroxynicotinic acid

29241-65-4

5-bromo-2-chloronicotinic acid

Conditions
ConditionsYield
With thionyl chloride In N,N-dimethyl-formamide at 70℃; for 4h;99%
Stage #1: 5-bromo-2-hydroxynicotinic acid With thionyl chloride In N,N-dimethyl-formamide at 70℃; for 4h;
Stage #2: With water In N,N-dimethyl-formamide for 1h;
99%
With thionyl chloride; N,N-dimethyl-formamide85%
609-71-2

2-hydroxy-3-carboxypyridine

29241-65-4

5-bromo-2-chloronicotinic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 78 percent / Br2; aq. NaOH / 18 h / 0 - 50 °C
2: 99 percent / thionyl chloride / dimethylformamide / 4 h / 70 °C
View Scheme
Multi-step reaction with 2 steps
1: 63.5 percent / aq. conc. NaOH, aq. NaOBr / 48 h / Ambient temperature
2: 37 percent / SOCl2 / dimethylformamide / 0.5 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 71 percent / Br2, NaOH / H2O / 90 h / 50 °C
2: 82 percent / SO2Cl2 / dimethylformamide / 2 h / Heating
View Scheme
2942-59-8

2-chloronicotinic acid

29241-65-4

5-bromo-2-chloronicotinic acid

Conditions
ConditionsYield
With bromine In acetic acid
67-56-1

methanol

29241-65-4

5-bromo-2-chloronicotinic acid

78686-79-0

methyl 2-chloro-5-bromonicotinate

Conditions
ConditionsYield
Stage #1: methanol; 5-bromo-2-chloronicotinic acid With sulfuric acid at 60℃; for 36h;
Stage #2: With sodium hydrogencarbonate In water
100%
Stage #1: 5-bromo-2-chloronicotinic acid With thionyl chloride at 70℃;
Stage #2: methanol In benzene at 65℃;
95%
With sulfuric acid for 15h; Reflux;89%
29241-65-4

5-bromo-2-chloronicotinic acid

75-65-0

tert-butyl alcohol

tert-butyl 5-bromo-2-chloronicotinate

Conditions
ConditionsYield
With sulfuric acid; magnesium sulfate In dichloromethane at 25℃; for 16h;94%
46049-49-4

(S)-(2,3-dihydrobenzo[b][1,4]dioxin-2-yl)methanamine

29241-65-4

5-bromo-2-chloronicotinic acid

(S)-5-bromo-2-chloro-N-((2,3-dihydrobenzo[b][1,4]dioxin-2-yl)methyl)nicotinamide

Conditions
ConditionsYield
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0 - 20℃; for 1h;93%
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide
29241-65-4

5-bromo-2-chloronicotinic acid

1117-97-1

N,0-dimethylhydroxylamine

885223-63-2

5-bromo-2-chloro-N-methoxy-N-methylnicotinamide

Conditions
ConditionsYield
Stage #1: 5-bromo-2-chloronicotinic acid With 1,1'-carbonyldiimidazole In dichloromethane at 20℃; for 1h;
Stage #2: N,0-dimethylhydroxylamine In dichloromethane at 20℃;
90%
With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 30℃; for 0.5h;82%
811-98-3

d(4)-methanol

29241-65-4

5-bromo-2-chloronicotinic acid

(2H3)methyl 5-bromo-2-chloropyridine-3-carboxylate

Conditions
ConditionsYield
With sulfuric acid In water at 60℃; for 48h;90%
29241-65-4

5-bromo-2-chloronicotinic acid

150-76-5

4-methoxy-phenol

1215864-79-1

5-bromo-2-(4-methoxyphenoxy)nicotinic acid

Conditions
ConditionsYield
Stage #1: 4-methoxy-phenol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.233333h; Inert atmosphere;
Stage #2: 5-bromo-2-chloronicotinic acid In N,N-dimethyl-formamide; mineral oil at 140℃; for 1h; Inert atmosphere;
83%
Stage #1: 4-methoxy-phenol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.1h;
Stage #2: 5-bromo-2-chloronicotinic acid In N,N-dimethyl-formamide; mineral oil at 20 - 140℃; for 1.16667h;
7664-41-7

ammonia

29241-65-4

5-bromo-2-chloronicotinic acid

75291-85-9

5-bromo-2-chloronicotinamide

Conditions
ConditionsYield
Stage #1: 5-bromo-2-chloronicotinic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 3h;
Stage #2: ammonia In methanol at -10 - 20℃; for 18h;
82%
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    Name: 5-Bromo-2-Chloronicotinic Acid Molecular Formula:C6H3BrClNO2 Molecular Weight:236.45 CAS No.:29241-65-4 Appearance:Similar White To Slight Yellow Solid Appearance:Similar White To Slight Yellow Solid Storage:Store in cool and dry place, awa

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Chemistry

IUPAC Name: 5-Bromo-2-chloropyridine-3-carboxylic acid
Molecular Formula: C6H3BrClNO2
Molecular Weight: 236.450520 g/mol
Melting Point: 173-176 °C
Density: 1.917 g/cm3
Flash Point: 162.5 °C
Storage temp.: Keep cold
Enthalpy of Vaporization: 62.18 kJ/mol
Boiling Point: 345.1 °C at 760 mmHg
Vapour Pressure: 2.39E-05 mmHg at 25 °C
Water Solubility: 699.3 mg/L at 25 °C
Structure of 5-Bromo-2-chloronicotinic acid (CAS NO.29241-65-4):
                            
Categories of 5-Bromo-2-chloronicotinic acid (CAS NO.29241-65-4): Blocks;Bromides;Carboxes;Pyridines;Acids and Derivatives;Heterocycles;pharmacetical;Carboxylic Acids;Pyridine;Carboxylic Acids

Safety Profile

Safety Information of 5-Bromo-2-chloronicotinic acid (CAS NO.29241-65-4):
Hazard Codes: Xi
Risk Statements: 36/37/38
36/37/38:Irritating to eyes, respiratory system and skin
Safety Statements: 26-36/37/39
26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36/37/39:Wear suitable protective clothing, gloves and eye/face protection
Hazard Note: Irritant/Keep Cold

Specification

 5-Bromo-2-chloronicotinic acid , its cas register number is 29241-65-4. It also can be called Acide 5-bromo-2-chloronicotinique ; 5-Bromo-2-chloropyridine-3-carboxylic acid ; and 3-Pyridinecarboxylic acid, 5-bromo-2-chloro- .