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30459-70-2

Basic Information
CAS No.: 30459-70-2
Name: 2-Methyl-4-nitrobenzoyl chloride
Article Data: 19
Molecular Structure:
Molecular Structure of 30459-70-2 (2-Methyl-4-nitrobenzoyl chloride)
Formula: C8H6ClNO3
Molecular Weight: 199.594
Synonyms: Benzoyl chloride,2-methyl-4-nitro;2-Methyl-4-nitro-benzoylchlorid;4-nitro-2-methyl-benzoylchloride;2-methyl-4-nitro-benzoic acid chloride;2-methyl-4-nitro-benzoyl chloride;
Density: 1.386±0.06 g/cm3(Predicted)
Melting Point: 34 °C
Boiling Point: 149-153 °C(Press: 14 Torr)
PSA: 62.89000
LogP: 2.80540
Synthetic route
1975-51-5

2-methyl-4-nitrobenzoic acid

30459-70-2

2-methyl-4-nitrobenzoyl chloride

Conditions
ConditionsYield
With thionyl chloride
With thionyl chloride Heating;
With thionyl chloride Substitution;
67-56-1

methanol

30459-70-2

2-methyl-4-nitrobenzoyl chloride

62621-09-4

methyl 2-methyl-4-nitrobenzoate

Conditions
ConditionsYield
In dichloromethane at 0℃; for 0.5h;100%
In dichloromethane at 0℃; for 0.5h;100%
863762-10-1

2,2-dimethylpropionic acid 7-chloro-2,3,4,5-tetrahydro-1H-benzo[b]azepin-5-yl ester

30459-70-2

2-methyl-4-nitrobenzoyl chloride

863762-20-3

2,2-dimethylpropionic acid 7-chloro-1-(2-methyl-4-nitrobenzoyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-5-yl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1h;98%
With triethylamine In dichloromethane at 0 - 20℃; for 1.25h;98%
863762-12-3

2,2-dimethylpropionic acid 7-fluoro-2,3,4,5-tetrahydro-1H-benzo[b]azepin-5-yl ester

30459-70-2

2-methyl-4-nitrobenzoyl chloride

863762-22-5

2,2-dimethylpropionic acid 7-fluoro-1-(2-methyl-4-nitrobenzoyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepin-5-yl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1h;97%
30459-70-2

2-methyl-4-nitrobenzoyl chloride

160129-45-3

7-chloro-1,2,3,4-tetrahydro-5H-benzo[b]azepin-5-one

137982-91-3

1-(4-nitro-2-methylbenzoyl)-7-chloro-5-oxo-2,3,4,5-tetrahydro-1H-1-benzazepine

Conditions
ConditionsYield
Stage #1: 7-chloro-1,2,3,4-tetrahydro-5H-benzo[b]azepin-5-one With magnesium hydroxide In acetonitrile at 10℃; for 0.5h;
Stage #2: 2-methyl-4-nitrobenzoyl chloride In acetonitrile for 5h;
95%
With sodium hydroxide In acetonitrile at 20℃; for 1h;73%
With triethylamine In dichloromethane at 20℃; for 2h; Acylation;32%
30459-70-2

2-methyl-4-nitrobenzoyl chloride

313673-94-8

7-chloro-2,3,4,5-tetrahydro-1H-benzo[b]azepine

313673-96-0

(7-chloro-2,3,4,5-tetrahydro-1H-1-benzazepin-1-yl)-2-methyl-4-nitrobenzamide

Conditions
ConditionsYield
With pyridine In dichloromethane for 1h;91%
30459-70-2

2-methyl-4-nitrobenzoyl chloride

C13H16ClNO4

C21H21ClN2O7

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 4h; Reagent/catalyst;88.7%
30459-70-2

2-methyl-4-nitrobenzoyl chloride

ethyl 4-(4-chlorophenylamino)butanoate

C20H21ClN2O5

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 3h; Reagent/catalyst;88%
30459-70-2

2-methyl-4-nitrobenzoyl chloride

80452-54-6

methyl 4-(2-amino-5-chlorophenyl)-4-oxobutyrate

1417520-49-0

C19H17ClN2O6

Conditions
ConditionsYield
With pyridine In dichloromethane87%
16450-41-2

L-glutamic acid diethyl ester

30459-70-2

2-methyl-4-nitrobenzoyl chloride

80015-10-7

diethyl N-(2-methyl-4-nitrobenzoyl)-L-glutamate

Conditions
ConditionsYield
With pyridine In toluene at 0 - 25℃; for 1.5h;77%
Raw Materials
1975-51-5
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