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3069-25-8

Basic Information
CAS No.: 3069-25-8
Name: N-Methylaminopropyltrimethoxysilane
Article Data: 7
Molecular Structure:
Molecular Structure of 3069-25-8 (N-Methylaminopropyltrimethoxysilane)
Formula: C7H19NO3Si
Molecular Weight: 193.318
Synonyms: Propylamine,N-methyl-3-(trimethoxysilyl)- (7CI,8CI);(Methylaminopropyl)trimethoxysilane;(N-Methyl-3-aminopropyl)trimethoxysilane;(N-Methylaminopropyl)trimethoxysilane;(Trimethoxysilylpropyl)methylamine;3-(N-Methylaminopropyl)trimethoxysilane;Dynasylan 1110;N-Methyl-3-(trimethoxysilyl)-1-propanamine;N-Methyl-3-(trimethoxysilyl)propylamine;N-Methyl-g-aminopropyltrimethoxysilane;N-[3-(Trimethoxysilyl)propyl)methanamine;Silane 1110;Trimethoxy(3-(methylamino)propyl)silane;X 12-636;XZ 2024;[3-(Methylamino)propyl]trimethoxysilane;Trimethoxy[3-(methylamino)propyl]silane;
EINECS: 221-334-5
Density: 0.93 g/cm3
Boiling Point: 181.9 °C at 760 mmHg
Flash Point: 63.8 °C
Solubility: Hydrolyzes in water.
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
PSA: 39.72000
LogP: 0.86490
Synthetic route
74-89-5

methylamine

2530-87-2

3-Chloropropyltrimethoxysilan

3069-25-8

N-methyl-3-trimethoxysilylpropylamine

627-37-2

N-methyl-N-allylamine

2487-90-3

trimethoxysilane

A

3069-25-8

N-methyl-3-trimethoxysilylpropylamine

B

C7H19NO3Si

Conditions
ConditionsYield
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex at 80℃; for 20h; Schlenk technique; Inert atmosphere; Overall yield = 93.2 %Spectr.; regioselective reaction;
108-55-4

glutaric anhydride,

3069-25-8

N-methyl-3-trimethoxysilylpropylamine

C12H25NO6Si

Conditions
ConditionsYield
In tetrahydrofuran at 20℃;100%
30674-80-7

2-Isocyanatoethyl methacrylate

3069-25-8

N-methyl-3-trimethoxysilylpropylamine

1560012-77-2

3,3-dimethoxy-7-methyl-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate

Conditions
ConditionsYield
at 60℃;100%
3069-25-8

N-methyl-3-trimethoxysilylpropylamine

376-68-1

hexafluoroglutaric anhydride

C12H19F6NO6Si

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 0.5h;99%
3069-25-8

N-methyl-3-trimethoxysilylpropylamine

106-89-8

epichlorohydrin

N-(2',3'-epoxypropyl)-(3-N-methylaminopropyl)-trimethoxysilane

Conditions
ConditionsYield
With potassium carbonate In toluene for 16h; Reflux; Inert atmosphere;96%
3069-25-8

N-methyl-3-trimethoxysilylpropylamine

376-68-1

hexafluoroglutaric anhydride

20667-12-3

silver(l) oxide

876734-90-6

(H3CO)3Si(CH2)3N(CH3)C(O)(CF2)3COO(1-)*Ag(1+)=Ag[(H3CO)3Si(CH2)3N(CH3)C(O)(CF2)3COO]

Conditions
ConditionsYield
In further solvent(s) under Ar, Schlenk setup, glutaric anhydride (1.4 mmol) in MTBE added to soln. of silicon compd. (1.4 mmol), stirred for 10 min, added to Ag2O (1.4 mmol) suspd. in MTBE, stirred for 18 h at room temp. in darkness; evapd. (vac.), elem. anal.;93%
3069-25-8

N-methyl-3-trimethoxysilylpropylamine

75-36-5

acetyl chloride

N-methyl-N-(3-(trimethoxysilyl)propyl)acetamide

Conditions
ConditionsYield
Stage #1: N-methyl-3-trimethoxysilylpropylamine With trimethylamine In dichloromethane at 0℃; for 0.166667h; Inert atmosphere;
Stage #2: acetyl chloride In dichloromethane for 4.5h;
85%
3069-25-8

N-methyl-3-trimethoxysilylpropylamine

82113-65-3

bis(trifluoromethanesulfonyl)amide

C32H80N8O12Si8*8C2HF6NO4S2

Conditions
ConditionsYield
In water; dimethyl sulfoxide at 25 - 100℃; for 19h;84%
3069-25-8

N-methyl-3-trimethoxysilylpropylamine

109-64-8

1,3-dibromo-propane

N,N'-bis(trimethoxysilylpropyl)-N,N'-dimethyl-1,3-propanediamine

Conditions
ConditionsYield
at 130℃; for 3h; Inert atmosphere; Industrial scale;80%
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Chemistry

IUPAC Name: N-Methyl-3-trimethoxysilylpropan-1-amine
Systematic of 1-Propanamine,N-methyl-3-(trimethoxysilyl)- (CAS NO.3069-25-8): EINECS 221-334-5 ; N-Methylaminopropyltrimethoxysilane
CAS NO: 3069-25-8
Molecular Formula of 1-Propanamine,N-methyl-3-(trimethoxysilyl)- (CAS NO.3069-25-8): C7H19NO3Si
Molecular Weight: 193.3162
Molecular Structure:

Polar Surface Area: 30.93 Å2
Index of Refraction: 1.415
Molar Refractivity: 52.02 cm3
Molar Volume: 207.7 cm3
Surface Tension: 23.3 dyne/cm
Density of 1-Propanamine,N-methyl-3-(trimethoxysilyl)- (CAS NO.3069-25-8): 0.93 g/cm3
Flash Point: 63.8 °C
Enthalpy of Vaporization: 41.81 kJ/mol
Boiling Point: 181.9 °C at 760 mmHg
Vapour Pressure: 0.834 mmHg at 25°C

Safety Profile

Hazard Codes: IrritantXi
Risk Statements: 36/37/38 
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36: Wear suitable protective clothing.
WGK Germany: 3
TSCA: Yes