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32231-06-4

Basic Information
CAS No.: 32231-06-4
Name: 1-PIPERONYLPIPERAZINE
Article Data: 15
Molecular Structure:
Molecular Structure of 32231-06-4 (1-PIPERONYLPIPERAZINE)
Formula: C12H16N2O2
Molecular Weight: 220.271
Synonyms: Piperazine,1-piperonyl- (7CI,8CI);1-(1,3-Benzodioxolan-5-ylmethyl)piperazine;1-(3,4-Methylenedioxybenzyl)piperazine;1-(4-Piperonyl)piperazine;1-(Benzo[1,3]dioxol-5-ylmethyl)piperazine;1-(Benzodioxol-5-ylmethyl)piperazine;1-[(2H-1,3-Benzodioxol-5-yl)methyl]piperazine;1-[(Benzo[d][1,3]dioxol-5-yl)methyl]piperazine;4-(4-Piperonyl)piperazine;4-[(Benzodioxol-5-yl)methyl]piperazine;5-(Piperazinomethyl)-1,3-benzodioxole;N-Piperonylpiperazine;N-[(1,3-Benzodioxol-5-yl)methyl]piperazine;1-(3,4-Methylenedioxyphenylmethyl)piperazine;
EINECS: 250-968-5
Density: 1.203 g/cm3
Melting Point: 36-40 °C(lit.)
Boiling Point: 330.5 °C at 760 mmHg
Flash Point: 158.4 °C
Solubility: Slightly soluble in water
Appearance: white to yellow or yellow-brownish cryst. solid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-37/39
PSA: 33.73000
LogP: 1.08720
Synthetic route
110-85-0

piperazine

495-76-1

piperonol

32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
In o-xylene at 150℃; for 30h; Inert atmosphere; Sealed tube;81%
With aluminum (III) chloride; water In acetonitrile at 20℃; Irradiation;41%

1-(1,3-benzodioxol-5-ylmethyl)-4-[(2-nitrophenyl)methyl]piperazine

32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
With hydrazine In 1,4-dioxane; water Inert atmosphere; UV-irradiation;80%
110-85-0

piperazine

120-57-0

piperonal

32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In tert-butyl methyl ether at 13 - 18℃; High pressure;78%
110-85-0

piperazine

20850-43-5

5-(chloromethyl)-1,3-benzodioxole

142-64-3

piperazine dihydrochloride

32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
Stage #1: piperazine; piperazine dihydrochloride In ethanol at 65℃; for 1h;
Stage #2: 5-(chloromethyl)-1,3-benzodioxole In ethanol at 78℃; for 2h;

benzyl 4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazine-1-carboxylate

32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 2h;
724428-97-1

4-chloro-6-dimethylamino-3-methylisoxazolo[5,4-d]pyrimidine

32231-06-4

1-Piperonylpiperazine

6-dimethylamino-3-methyl-4-(3,4-methylenedioxybenzylpiperazino)isoxazolo[5,4-d]pyrimidine

Conditions
ConditionsYield
In tetrahydrofuran Heating;99%
24424-99-5

di-tert-butyl dicarbonate

32231-06-4

1-Piperonylpiperazine

1233143-33-3

tert-butyl 4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazine-1-carboxylate

Conditions
ConditionsYield
With triethylamine In methanol at 20℃; for 1.5h; Inert atmosphere;99%
98-59-9

p-toluenesulfonyl chloride

32231-06-4

1-Piperonylpiperazine

305859-64-7

1-(benzo[d][1,3]dioxol-5-ylmethyl)-4-tosylpiperazine

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 4.5h; Inert atmosphere;99%
124-38-9

carbon dioxide

32231-06-4

1-Piperonylpiperazine

C13H16N2O3

Conditions
ConditionsYield
With hydrogen In methanol at 120℃; under 30003 Torr; for 24h; Autoclave;99%
762-42-5

dimethyl acetylenedicarboxylate

32231-06-4

1-Piperonylpiperazine

24726-53-2

tetramethyl 2,2'-(1,4-piperazindiyl)dimaleate

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 1h;98%
Downstream Products
125575-13-5
125575-10-2
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  • 1-Piperonylpiperazine CAS No.32231-06-4

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    1-Piperonylpiperazine CAS No.32231-06-4

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Chemistry

IUPAC Name: 1-(1,3-benzodioxol-5-ylmethyl)piperazine
The MF of 1-PIPERONYLPIPERAZINE(32231-06-4): C12H16N2O2
The MW of 1-PIPERONYLPIPERAZINE(32231-06-4): 220.27
EINECS: 250-968-5
mp: 36-40 °C(lit.)
bp: 147-149 °C at 2 mm Hg(lit.)
Fp: >230 °F
Density: 1.203 g/cm3 
Index of Refraction: 1.577 
Appearance: Crystalline mass.
Solubility in water: Very soluble
Categories: Pharmaceutical Raw Materials;Heterocycles;API intermediates;Building Blocks;Heterocyclic Building Blocks;Piperazines
Synonyms: 3,4-METHYLENEDIOXY-1-(N-PIPERAZINYL)-BENZENE;1-PIPERONYLPIPERAZINE;1-[(1,3-BENZODIOXOL-5-YL)METHYL]PIPERAZINE;1-BENZO[1,3]DIOXOL-5-YLMETHYL-PIPERAZINE;1-(3,4-METHYLENEDIOXYBENZYL)PIPERAZINE;1-(3,4-METHYLENDIOXYBENZYL)PIPERAZINE;AKOS BBS-00006443;AKOS B020126
The Structure of 1-PIPERONYLPIPERAZINE(32231-06-4):

Toxicity Data With Reference

1. mouse LD50 intraperitoneal 50mg/kg (50mg/kg)
   European Journal of Medicinal Chemistry--Chimie Therapeutique. Vol. 9, Pg. 555, 1974.

Safety Profile

Hazard Codes: Xi
Risk Statements: 36/37/38
36/37/38:  Irritating to eyes, respiratory system and skin 
Safety Statements: 26-37/39
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
37/39:  Wear suitable gloves and eye/face protection 
RIDADR: 3259
WGK Germany: 3
RTECS: TM1550000
Hazard Note: Irritant
HazardClass: 8
PackingGroup: II

Specification

1. First Aid Measures
Ingestion:
Do NOT induce vomiting. Allow the victim to rinse his mouth and then to drink 2-4 cupfuls of water, and seek medical advice.
Inhalation:
Remove from exposure to fresh air immediately.
Skin:
Flush skin with plenty of soap and water for at least 15 minutes while removing contaminated clothing and shoes.
Eyes:
If symptoms develop, immediately move individual away from exposure and into fresh air. Flush eyes gently with water for at least 15 minutes while holding eyelids apart; seek immediate medical attention.
2. Handling and Storage
Storage:
Store in a cool, dry place. Keep container closed when not in use.
Handling:
Wash thoroughly after handling. Remove contaminated clothing and wash before reuse. Avoid contact with eyes, skin, and clothing. Avoid ingestion and inhalation.