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3332-29-4

Basic Information
CAS No.: 3332-29-4
Name: Ethoxyamine hydrochloride
Article Data: 14
Molecular Structure:
Molecular Structure of 3332-29-4 (Ethoxyamine hydrochloride)
Formula: C2H7 NO.ClH
Molecular Weight: 97.5446
Synonyms: Ethoxyamine,hydrochloride (6CI,7CI);Hydroxylamine, O-ethyl-, hydrochloride (8CI,9CI);(Aminooxy)ethane hydrochloride;Ethoxamine hydrochloride;Ethoxyammoniumchloride;N-Ethoxyamine hydrochloride;O-Ethylhydroxylamine hydrochloride;
EINECS: 222-060-9
Melting Point: 130-133 °C(lit.)
Boiling Point: 75.8 °C at 760 mmHg
Flash Point: 5.9 °C
Solubility: Soluble in water
Appearance: white adhering crystals or crystalline powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
PSA: 46.53000
LogP: 2.43540
Synthetic route
1914-21-2

N-ethoxyphthalimide

3332-29-4

O-ethylhydroxylamine hydrochloride

Conditions
ConditionsYield
Stage #1: N-ethoxyphthalimide With methylhydrazine In dichloromethane at 0 - 20℃; for 2h;
Stage #2: With hydrogenchloride In 1,4-dioxane at 0℃;
100%
With hydrogenchloride; hydrazine hydrate 1.) ethanol, reflux, 20 min; 2.) ethanol, reflux, 20 min; Yield given. Multistep reaction;
With methylhydrazine In dichloromethane
52914-24-6

ethyl acetohydroxamate

3332-29-4

O-ethylhydroxylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In ethanol; water at 65℃;71.2%
With hydrogenchloride In ethanol; water at 65℃;71.2%
22509-51-9

O-ethyl benzoylhydroxamic acid

3332-29-4

O-ethylhydroxylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In ethanol Heating;48%

1-ethoxy-pyrrolidine-2,5-dione

3332-29-4

O-ethylhydroxylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride
624-86-2

O-ethyl hydroxylamine

3332-29-4

O-ethylhydroxylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In ethanol at 0 - 5℃; for 72h;
With hydrogenchloride Large scale;7.2 kg
121-32-4

4-hydroxy-3-ethoxybenzaldehyde

3332-29-4

O-ethylhydroxylamine hydrochloride

3-ethoxy-4-hydroxybenzaldehyde-O-ethyloxime

Conditions
ConditionsYield
With sodium acetate In water at 80℃; for 2h;100%
2233-18-3

4-hydroxy-3,5-dimethylbenzaldehyde

3332-29-4

O-ethylhydroxylamine hydrochloride

3,5-dimethyl-4-hydroxybenzaldehyde-O-ethyloxime

Conditions
ConditionsYield
With sodium acetate In water at 80℃; for 2h;100%
13677-79-7

gallaldehyde

3332-29-4

O-ethylhydroxylamine hydrochloride

3,4,5-trihydroxybenzaldehyde-O-ethyloxime

Conditions
ConditionsYield
With sodium acetate In water at 80℃; for 2h;100%
3332-29-4

O-ethylhydroxylamine hydrochloride

139-85-5

3,4-dihydroxybenzaldehyde

3,4-dihydroxybenzaldehyde-O-ethyloxime

Conditions
ConditionsYield
With sodium acetate In water at 80℃; for 2h;100%
3332-29-4

O-ethylhydroxylamine hydrochloride

23611-75-8

6-chloro-pyrazine-2-carboxylic acid methyl ester

6-chloro-N-ethoxypyrazine-2-carboxamide

Conditions
ConditionsYield
With trimethylaluminum In hexane; dichloromethane at 20℃; Inert atmosphere;100%
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  • O-Ethylhydroxylamine hydrochloride manufacture

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  • High Purity O-Ethylhydroxylamine Hydrochloride 3332-29-4

  • Casno:

    3332-29-4

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Specification

The Ethoxyamine Hydrochloride, with the CAS registry number 3332-29-4, has the IUPAC name of O-ethylhydroxylamine hydrochloride. For being a kind of white or light yellow crystal, it is soluble in water and ethanol, with the product categories including pharmaceutical intermediates.
 
The physical properties of this chemical are as follows: (1)ACD/LogP: 0.30; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 0.15; (4)ACD/LogD (pH 7.4): 0.3; (5)ACD/BCF (pH 5.5): 1; (6)ACD/BCF (pH 7.4): 1; (7)ACD/KOC (pH 5.5): 24.64; (8)ACD/KOC (pH 7.4): 34.62; (9)#H bond acceptors: 2; (10)#H bond donors: 2; (11)#Freely Rotating Bonds: 2; (12)Polar Surface Area: 12.47; (13)Flash Point: 5.9 °C; (14)Enthalpy of Vaporization: 31.69 kJ/mol; (15)Boiling Point: 75.8 °C at 760 mmHg; (16)Vapour Pressure: 104 mmHg at 25°C; (17)Exact Mass: 97.029442; (18)MonoIsotopic Mass: 97.029442; (19)Topological Polar Surface Area: 35.2; (20)Heavy Atom Count: 5; (21)Complexity: 10.

The production method of this chemical: ethyl acetate could react with hydroxylamine sulphate in presence of alkali to have one chemical; Next the chemical has the ethylation with ethyl sulfate and then react in muriatic acid to get this product.

As to its usage, it is widely applied in many ways. It could be used as the intermediates of cycloxydim; It could also be producing a variety of herbicide, and then as a kind of important pesticide.

Additionally, you could obtain the molecular structure by converting the following datas:
(1)Canonical SMILES: CCON.Cl
(2)InChI: InChI=1S/C2H7NO.ClH/c1-2-4-3;/h2-3H2,1H3;1H
(3)InChIKey: NUXCOKIYARRTDC-UHFFFAOYSA-N