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33483-65-7

Basic Information
CAS No.: 33483-65-7
Name: trans-4-Methylcyclohexylamine hydrochloride
Article Data: 37
Molecular Structure:
Molecular Structure of 33483-65-7 (trans-4-Methylcyclohexylamine hydrochloride)
Formula: C7H15N.HCl
Molecular Weight: 149.664
Synonyms: Cyclohexanamine,4-methyl-, hydrochloride, trans- (9CI);Cyclohexylamine, 4-methyl-,hydrochloride, trans- (8CI);trans-4-Methylcyclohexanamine hydrochloride;Cyclohexanamine,4-methyl-, hydrochloride (1:1), trans-;
Melting Point: 260 °C
Boiling Point: 195.9 °C at 760 mmHg
Flash Point: 72.3 °C
Safety: 24/25
PSA: 26.02000
LogP: 3.02610
Synthetic route
100959-19-1

trans-4-methylcyclohexylamine hydrochloride

33483-65-7

trans-4-methylcyclohexylamine hydrochloride

Conditions
ConditionsYield
In methanol; acetone at 25 - 30℃; for 3h;
64-18-6

formic acid

33483-65-7

trans-4-methylcyclohexylamine hydrochloride

26003-39-4

N-(4-methylcyclohexyl)formamide

Conditions
ConditionsYield
With sodium formate at 120 - 140℃; for 2h;
33483-65-7

trans-4-methylcyclohexylamine hydrochloride

2523-88-8

trans-N,4-dimethylcyclohexylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: HCO2Na / 2 h / 120 - 140 °C
2: LiAlH4 / diethyl ether
View Scheme
33483-65-7

trans-4-methylcyclohexylamine hydrochloride

25886-43-5

trans-4.N-Dimetil-N-(2.4-dinitrofenil)cicloesilammina

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: HCO2Na / 2 h / 120 - 140 °C
2: LiAlH4 / diethyl ether
3: NaOEt / ethanol / Heating
View Scheme
54745-92-5

quinoxaline-2-carboxylic acid chloride

ethyl acetate n-hexane

33483-65-7

trans-4-methylcyclohexylamine hydrochloride

589-92-4

1-methylcyclohexan-4-one

A

226877-90-3

N-(trans-4-methylcyclohexyl)-2-quinoxalinecarboxamide

B

N-(trans-4-Methylcyclohexyl)-2-qulinoxalinecarboxamide

N-(trans-4-Methylcyclohexyl)-2-qulinoxalinecarboxamide

Conditions
ConditionsYield
With pyridine; hydroxylamine In ethanol; dichloromethane; water; ethyl acetate
3993-78-0

2-amino-4-chloropyrimidine

33483-65-7

trans-4-methylcyclohexylamine hydrochloride

1401034-42-1

N4-((1r,4r)-4-methylcyclohexyl)pyridine-2,4-diamine

Conditions
ConditionsYield
With triethylamine In butan-1-ol for 36h; Reflux;
With triethylamine In butan-1-ol for 36h; Reflux; Inert atmosphere;1770 g
33483-65-7

trans-4-methylcyclohexylamine hydrochloride

1401033-82-6

9-((1r,4r)-4-methylcyclohexyl)-N-(5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)-9H-pyrido[4′,3′:4,5]pyrrolo[2,3-d]pyrimidin-2-amine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: triethylamine / butan-1-ol / 36 h / Reflux
2.1: N-iodo-succinimide / N,N-dimethyl-formamide / 2 h / 10 - 20 °C / Inert atmosphere
3.1: tetrakis(triphenylphosphine) palladium(0) / hexane; tetrahydrofuran / Reflux
4.1: lithium hexamethyldisilazane / toluene; 1-methyl-pyrrolidin-2-one / 0.5 h / 20 - 90 °C / Inert atmosphere
5.1: hydrogenchloride / water; methanol / 20 °C
5.2: 0 °C / pH 9
View Scheme
Multi-step reaction with 6 steps
1.1: triethylamine / butan-1-ol / 36 h / Reflux; Inert atmosphere
2.1: N-iodo-succinimide / N,N-dimethyl-formamide / 2.16 h / 10 - 20 °C / Inert atmosphere
3.1: 2,2,6,6-tetramethyl-piperidine; n-butyllithium / tetrahydrofuran; hexane / 2.25 h / -74 - 0 °C / Inert atmosphere
3.2: 0.58 h / -60 °C / Inert atmosphere
3.3: Reflux; Inert atmosphere
4.1: lithium hexamethyldisilazane / 1-methyl-pyrrolidin-2-one / 90 °C / Inert atmosphere
5.1: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate / 1,4-dioxane / 0.17 h / Inert atmosphere
5.2: 3 h / 100 °C / Inert atmosphere
6.1: hydrogenchloride; water / methanol / 20 °C / Inert atmosphere
View Scheme
33483-65-7

trans-4-methylcyclohexylamine hydrochloride

1401034-43-2

5-iodo-N4-((1R,4R)-4-methylcyclohexyl)pyrimidine-2,4-diamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / butan-1-ol / 36 h / Reflux
2: N-iodo-succinimide / N,N-dimethyl-formamide / 2 h / 10 - 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: triethylamine / butan-1-ol / 36 h / Reflux; Inert atmosphere
2: N-iodo-succinimide / N,N-dimethyl-formamide / 2.16 h / 10 - 20 °C / Inert atmosphere
View Scheme
33483-65-7

trans-4-methylcyclohexylamine hydrochloride

1401034-44-3

5-(3-fluoropyridin-4-yl)-N4-((1R,4R)-4-methylcyclohexyl)pyrimidine-2,4-diamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: triethylamine / butan-1-ol / 36 h / Reflux
2: N-iodo-succinimide / N,N-dimethyl-formamide / 2 h / 10 - 20 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0) / hexane; tetrahydrofuran / Reflux
View Scheme
Multi-step reaction with 3 steps
1.1: triethylamine / butan-1-ol / 36 h / Reflux; Inert atmosphere
2.1: N-iodo-succinimide / N,N-dimethyl-formamide / 2.16 h / 10 - 20 °C / Inert atmosphere
3.1: 2,2,6,6-tetramethyl-piperidine; n-butyllithium / tetrahydrofuran; hexane / 2.25 h / -74 - 0 °C / Inert atmosphere
3.2: 0.58 h / -60 °C / Inert atmosphere
3.3: Reflux; Inert atmosphere
View Scheme
33483-65-7

trans-4-methylcyclohexylamine hydrochloride

1401034-45-4

9-((1r,4r)-4-methylcyclohexyl)-9H-pyrido[4′,3′:4,5]pyrrolo[2,3-d]pyrimidin-2-amine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: triethylamine / butan-1-ol / 36 h / Reflux
2: N-iodo-succinimide / N,N-dimethyl-formamide / 2 h / 10 - 20 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0) / hexane; tetrahydrofuran / Reflux
4: lithium hexamethyldisilazane / toluene; 1-methyl-pyrrolidin-2-one / 0.5 h / 20 - 90 °C / Inert atmosphere
View Scheme
Multi-step reaction with 4 steps
1.1: triethylamine / butan-1-ol / 36 h / Reflux; Inert atmosphere
2.1: N-iodo-succinimide / N,N-dimethyl-formamide / 2.16 h / 10 - 20 °C / Inert atmosphere
3.1: 2,2,6,6-tetramethyl-piperidine; n-butyllithium / tetrahydrofuran; hexane / 2.25 h / -74 - 0 °C / Inert atmosphere
3.2: 0.58 h / -60 °C / Inert atmosphere
3.3: Reflux; Inert atmosphere
4.1: lithium hexamethyldisilazane / 1-methyl-pyrrolidin-2-one / 90 °C / Inert atmosphere
View Scheme
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Specification

trans-4-Methylcyclohexylamine hydrochloride is an organic compound with the formula C7H15N.HCl, and its systematic name is the same with the product name. With the CAS registry number 33483-65-7, it is also named as Cyclohexanamine,4-methyl-, hydrochloride (1:1), trans-. In addition, the molecular weight is 149.66.

Physical properties of trans-4-Methylcyclohexylamine hydrochloride are: (1)ACD/LogP: 1.887; (2)# of Rule of 5 Violations: 0; (3)#H bond acceptors: 1; (4)#H bond donors: 2; (5)#Freely Rotating Bonds: 1; (6)Polar Surface Area: 26.02 Å2; (7)Flash Point: 72.3 °C; (8)Enthalpy of Vaporization: 44.09 kJ/mol; (9)Boiling Point: 195.9 °C at 760 mmHg; (10)Vapour Pressure: 0.347 mmHg at 25°C.

You can still convert the following datas into molecular structure:
(1)SMILES: Cl.C[C@H]1CC[C@H](N)CC1
(2)Std. InChI: InChI=1S/C7H15N.ClH/c1-6-2-4-7(8)5-3-6;/h6-7H,2-5,8H2,1H3;1H/t6-,7-;
(3)Std. InChIKey: GIRKJSRZELQHDX-MEZFUOHNSA-N