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| CAS No.: | 33626-98-1 |
|---|---|
| Name: | Methyl 6-bromo-2-naphthoate |
| Article Data: | 12 |
| Molecular Structure: | |
|
|
|
| Formula: | C12H9BrO2 |
| Molecular Weight: | 265.106 |
| Synonyms: | 2-Naphthoicacid, 6-bromo-, methyl ester (8CI);6-Bromonaphthalene-2-carboxylic acid methylester;6-Bromo-2-naphthalenecarboxylic acid methyl ester;Methyl 6-bromonaphthalene-2-carboxylate;6-Bromo-2-naphthoic acid methyl ester;Methyl 6-bromo-2-naphthalenecarboxylate;2-Bromo-6-naphthoic acid methylester; |
| EINECS: | -0 |
| Density: | 1.492 g/cm3 |
| Melting Point: | 123-126 °C(lit.) |
| Boiling Point: | 357 °C at 760 mmHg |
| Flash Point: | 169.7 °C |
| Appearance: | Pale yellow or light brown powder |
| Hazard Symbols: |
 C
|
| Risk Codes: | 20/21/22-34 |
| Safety: | 24/25-45-36/37/39-27-26 |
| PSA: | 26.30000 |
| LogP: | 3.38890 |
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| Conditions | Yield |
|---|---|
| With sulfuric acid; trimethyl orthoformate for 48h; Reflux; | 100% |
| With sulfuric acid for 36h; Reflux; | 100% |
| With sulfuric acid Reflux; | 100% |
| Conditions | Yield |
|---|---|
| Stage #1: methanol; naphthalene-2-carboxylate at 150℃; under 4560.31 Torr; for 1h; Stage #2: With sodium hypobromite; benzenesulfonic acid; sodium bromide In water at 170℃; under 11400.8 Torr; for 6h; Pressure; Temperature; | 98.3% |
| Conditions | Yield |
|---|---|
| With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 18h; Inert atmosphere; | 98% |
- 123207-11-4
2-[1-(4-Bromo-phenyl)-meth-(Z)-ylidene]-3,3-dimethoxy-butyric acid methyl ester
- 33626-98-1
methyl 6-bromo-2-naphthoate
| Conditions | Yield |
|---|---|
| at 475 - 500℃; vapor-phase pyrolysis; Yield given; |
- 67-56-1
methanol
- 201230-82-2
carbon monoxide
- 151600-02-1
6-bromo-2-naphthalenyl trifluoromethanesulfonate
- 33626-98-1
methyl 6-bromo-2-naphthoate
| Conditions | Yield |
|---|---|
| With 1,3-bis-(diphenylphosphino)propane; palladium diacetate |
- 186581-53-3, 908094-01-9
diazomethane
- 33626-98-1
methyl 6-bromo-2-naphthoate
| Conditions | Yield |
|---|---|
| With diethyl ether |
- 15231-91-1
6-bromo-naphthalen-2-ol
- 33626-98-1
methyl 6-bromo-2-naphthoate
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: DIEA 2: dppp / Pd(OAc)2 View Scheme |
- 33626-98-1
methyl 6-bromo-2-naphthoate
| Conditions | Yield |
|---|---|
| With sulfuric acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone In methanol; water at 0 - 20℃; for 1h; |
- 528894-31-7
4-((2,2,2-trifluoroacetamido)methyl)phenylboronic acid
- 33626-98-1
methyl 6-bromo-2-naphthoate
- 869748-83-4
methyl 6-[4-(N-trifluoroacetylamino)methylphenyl]-2-naphthalenecarboxylate
| Conditions | Yield |
|---|---|
| With potassium fluoride; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran for 20h; Suzuki-Miyaura cross-coupling reaction; Heating; | 100% |
- 33626-98-1
methyl 6-bromo-2-naphthoate
- 100751-63-1
(6-bromo-2-naphthy)methanol
| Conditions | Yield |
|---|---|
| With lithium aluminium tetrahydride In tetrahydrofuran at -10 - -5℃; for 1.33333h; | 99% |
| With diisobutylaluminium hydride In tetrahydrofuran; hexane at 20℃; for 40h; Inert atmosphere; | 99% |
| With diisobutylaluminium hydride In tetrahydrofuran; n-heptane at -78 - 20℃; for 14h; Inert atmosphere; | 98% |
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Chemistry
IUPAC Name: Methyl 6-bromonaphthalene-2-carboxylate
Synonyms of Methyl 6-bromo-2-naphthoate (CAS NO.33626-98-1): 6-Bromo-2-naphthalenecarboxylic acid methyl ester ; 6-Bromo-2-naphthoic acid methyl ester ; Methyl 6-bromo-2-naphthalenecarboxylate ; 2-Bromo-6-naphthoic acid methylester
CAS NO: 33626-98-1
Molecular Formula: C12H9BrO2
Molecular Weight: 265.1027
Molecular Structure:
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Melting Point: 123-126 °C
ProductCategories: blocks Bromides ; Carboxes ; Aromatic Esters ; Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts ; ADAPALENE ; Intermediates of Adapalene ; C12 to C63 ; Carbonyl Compounds ; Esters ; API
Polar Surface Area: 26.3 Å2
Index of Refraction: 1.634
Molar Refractivity: 63.55 cm3
Molar Volume: 177.6 cm3
Surface Tension: 47.5 dyne/cm
Density of Methyl 6-bromo-2-naphthoate (CAS NO.33626-98-1): 1.492 g/cm3
Flash Point: 169.7 °C
Enthalpy of Vaporization: 60.23 kJ/mol
Boiling Point: 357 °C at 760 mmHg
Vapour Pressure: 2.81E-05 mmHg at 25°C
Safety Profile
Hazard Codes: 
C
Risk Statements of Methyl 6-bromo-2-naphthoate (CAS NO.33626-98-1): 20/21/22-34
R20/21/22: Harmful by inhalation, in contact with skin and if swallowed.
R34: Causes burns.
Safety Statements: 24/25-45-36/37/39-27-26
S24/25: Avoid contact with skin and eyes.
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection.
S27: Take off immediately all contaminated clothing.
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
WGK Germany: 3
Specification
Decomposition/conditions to be avoided:
Decomposition will not occur if used and stored according to specifications.
Materials to be avoided: Oxidizing agents
Dangerous reactions: No dangerous reactions known
Dangerous products of decomposition: Carbon monoxide and carbon dioxide; HYDROGEN bromide
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