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34143-74-3

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Basic Information
CAS No.: 34143-74-3
Name: 1H,1H,2H,2H-PERFLUORODECANETHIOL
Article Data: 9
Molecular Structure:
Molecular Structure of 34143-74-3 (1H,1H,2H,2H-PERFLUORODECANETHIOL)
Formula: C10H5 F17 S
Molecular Weight: 480.189
Synonyms: 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-Heptadecanefluoro-10-decanethiol;1,1,2,2-Tetrahydroperfluoro-1-decanethiol;1,1,2,2-Tetrahydroperfluorodecanethiol;1,1,2,2-Tetrahydroperfluorodecylmercaptan; 1-Mercapto-2-(perfluorooctyl)ethane;1H,1H,1H,2H-Perfluorodecanethiol; 1H,1H,2H,2H-Perfluorodecane-1-thiol;1H,1H,2H,2H-Perfluorodecanethiol; 2-(Perfluorooctyl)-1-ethanethiol;2-(Perfluorooctyl)ethanethiol;3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluoro-1-decanethiol; Lodyne 924
Density: 1.597g/cm3
Melting Point: 15 °C
Boiling Point: 82 °C
Flash Point: 75°C
Hazard Symbols:
Risk Codes: 36/37/38
Safety:
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26-36
WGK Germany 3
F 10-23
Hazard Note Irritant
PSA: 38.80000
LogP: 6.31570
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Synthetic route
42977-21-9

1,2-bis(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)disulfide

34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

Conditions
ConditionsYield
With tributylphosphine; water In tetrahydrofuran at 20℃; for 9h; Inert atmosphere;70%
125640-21-3

S-[2-(perfluorooctyl)ethyl]thioacetate

A

34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

B

42977-21-9

1,2-bis(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)disulfide

Conditions
ConditionsYield
With sodium hydroxide In methanol for 3h; Hydroformylation; Oxidative dimerization; Heating;A 68%
B n/a

2-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluoro-decyl)-isothiourea; hydriodide

34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

Conditions
ConditionsYield
With sodium hydroxide In water at 78 - 80℃; for 1h;62%
2043-53-0

2-(n-perfluorooctyl)ethyl iodide

34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

Conditions
ConditionsYield
With thiourea In ethanol for 72h; Heating;52%
Multi-step reaction with 2 steps
1: NaOMe / methanol / 5 h / 70 °C
2: 68 percent / aq. NaOH / methanol / 3 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: ethanol / 20 h / 79 °C
2: 62 percent / NaOH / H2O / 1 h / 78 - 80 °C
View Scheme
Multi-step reaction with 2 steps
1: 5percent trioctylmethylammonium chloride / H2O / 16 h / 100 °C
2: basic hydrolysis
View Scheme
2043-53-0

2-(n-perfluorooctyl)ethyl iodide

17356-08-0

thiourea

34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

Conditions
ConditionsYield
With sodium hydroxide 1.) EtOH, reflux; Multistep reaction;

(diaminomethylene)(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonium iodide

34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

Conditions
ConditionsYield
basic hydrolysis; Yield given;
507-63-1

1-iodoheptadecafluorooctane

34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 92 percent / benzoyl peroxide / 2 h / 92 - 101 °C
2: ethanol / 20 h / 79 °C
3: 62 percent / NaOH / H2O / 1 h / 78 - 80 °C
View Scheme
1318074-61-1

3-(4-chlorobut-2-enyl)-3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-1-(4-methoxybenzyl)-1,3-dihydroindol-2-one

34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: samarium diiodide / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere
1.2: 80 °C / Inert atmosphere; Sealed tube
2.1: tributylphosphine; water / tetrahydrofuran / 9 h / 20 °C / Inert atmosphere
View Scheme
34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

78-94-4

methyl vinyl ketone

4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decylsulfanyl)-butan-2-one

Conditions
ConditionsYield
With sodium methylate at 25℃; for 15h; Addition;100%

N-(2-benzenesulfonylethyl)-N-[2-(3,4-dimethoxyphenyl)ethyl]-2-oxoacetamide

34143-74-3

1H,1H,2H,2H-Perfluorodecanethiol

3-(2-benzenesulfonylethyl)-1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-7,8-dimethoxy-1,3,4,5-tetrahydrobenzo[d]azepin-2-one

Conditions
ConditionsYield
Stage #1: N-(2-benzenesulfonylethyl)-N-[2-(3,4-dimethoxyphenyl)ethyl]-2-oxoacetamide; 1H,1H,2H,2H-Perfluorodecanethiol In dichloromethane for 18h; Pummerer reaction;
Stage #2: With trifluoroacetic anhydride In dichloromethane for 1h;
Stage #3: With boron trifluoride diethyl etherate In dichloromethane for 1h;		100%
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    Product Name: 1H,1H,2H,2H-PERFLUORODECANETHIOL Synonyms: 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-HEPTADECAFLUORO-1-DECANETHIOL;1H,1H,2H,2H-PERFLUORODECANE-1-THIOL;1H,1H,2H,2H-PERFLUORODECANETHIOL;1H,1H,2H,2H-PERFLUORODECYL-1-THIOL;1H,1H,2H,2H-PE

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