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3424-93-9

Basic Information
CAS No.: 3424-93-9
Name: 4-Methoxybenzamide
Article Data: 403
Molecular Structure:
Molecular Structure of 3424-93-9 (4-Methoxybenzamide)
Formula: C8H9NO2
Molecular Weight: 151.165
Synonyms: p-Anisamide(6CI,7CI,8CI);Anisamide;NSC 11139;p-Methoxybenzamide;
EINECS: 222-319-6
Density: 1.144 g/cm3
Melting Point: 164-167 °C(lit.)
Boiling Point: 295.803 °C at 760 mmHg
Flash Point: 161.563 °C
Appearance: White crystalline powder
Hazard Symbols: Xn
Risk Codes: 36/37/38
Safety: 22-24/25
PSA: 52.32000
LogP: 1.49440
Synthetic route
874-90-8

4-methoxybenzonitrile

3424-93-9

4-methoxyphenylacetamide

Conditions
ConditionsYield
With C18H57O3P6Ru2(1+)*C6H5O(1-)*C6H6O; water In 1,4-dioxane for 6h; Time; Sealed tube; Inert atmosphere; Schlenk technique;100%
With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); water; 2-(diphenylphosphino)-N,N-dimethylpyridine-4-amine In 1,2-dimethoxyethane at 80℃; for 5h;99%
With C12H24O16Ru3*2H2O In water at 110℃; for 13h; Catalytic behavior; Schlenk technique; Inert atmosphere;99%
123-11-5

4-methoxy-benzaldehyde

3424-93-9

4-methoxyphenylacetamide

Conditions
ConditionsYield
With hydroxylamine; C33H28F3N5O3Ru(1+)*Cl(1-) In water at 60℃; for 0.5h; Catalytic behavior; Sonication;99%
Stage #1: 4-methoxy-benzaldehyde With hydroxylamine hydrochloride; caesium carbonate In water; dimethyl sulfoxide at 100℃;
Stage #2: With palladium diacetate In water; dimethyl sulfoxide at 125℃; chemoselective reaction;
97%
With copper(ll) sulfate pentahydrate; hydroxylamine hydrochloride; sodium acetate at 110℃; for 2h; Neat (no solvent);97%
100-09-4

4-methoxybenzoic acid

3424-93-9

4-methoxyphenylacetamide

Conditions
ConditionsYield
Stage #1: 4-methoxybenzoic acid With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate In tetrahydrofuran for 0.0166667h; Milling;
Stage #2: With ammonium thiocyanate In tetrahydrofuran for 0.0833333h; Milling;
99%
With pyridine; urea for 0.00833333h; microwave irradiation;90%
Stage #1: 4-methoxybenzoic acid With thionyl chloride In tetrahydrofuran at 50℃; for 1h;
Stage #2: With ammonium hydroxide In tetrahydrofuran at 0℃; for 0.0833333h;
84%
19486-73-8

N-tert-butyl-4-methoxybenzamide

3424-93-9

4-methoxyphenylacetamide

Conditions
ConditionsYield
scandium tris(trifluoromethanesulfonate) In nitromethane at 170℃; for 1h; Irradiation;99%
With t-butyldimethylsiyl triflate In toluene at 100℃; for 8h;74%
619-57-8

p-hydroxybenzamide

616-38-6

carbonic acid dimethyl ester

3424-93-9

4-methoxyphenylacetamide

Conditions
ConditionsYield
With dmap at 135℃; under 3000.3 Torr; for 7h; Pressure; Temperature; Reagent/catalyst;99%
100-07-2

4-methoxy-benzoyl chloride

3424-93-9

4-methoxyphenylacetamide

Conditions
ConditionsYield
With ammonia Inert atmosphere;98%
With ammonia at -10 - 20℃; for 1h; Temperature;96.3%
With ammonia In water at 20℃; for 1h;79%
105-13-5

4-Methoxybenzyl alcohol

3424-93-9

4-methoxyphenylacetamide

Conditions
ConditionsYield
With tert.-butylhydroperoxide; ammonia; oxygen In water; N,N-dimethyl-formamide at 80℃; under 1520.1 Torr; for 5h; Green chemistry;98%
Stage #1: 4-Methoxybenzyl alcohol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ammonia; oxygen; copper(II) nitrate In water; dimethyl sulfoxide at 80℃; under 760.051 Torr; for 5h;
Stage #2: With Acetaldehyde oxime In water; dimethyl sulfoxide at 110℃; for 24h; Inert atmosphere;
97%
With ammonia; oxygen In water at 150℃; under 22502.3 Torr; for 3h;96.5%
2393-23-9

4-methoxy-benzylamine

3424-93-9

4-methoxyphenylacetamide

Conditions
ConditionsYield
With manganese(IV) oxide at 130℃; under 4560.31 Torr; for 3h;98%
With dihydrogen peroxide at 80℃; for 10h; Inert atmosphere;96%
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); potassium tert-butylate In tert-butyl alcohol at 70℃; for 12h;95%
3532-17-0

4-methoxybenzoyl azide

3424-93-9

4-methoxyphenylacetamide

Conditions
ConditionsYield
With (1,4-diazabicyclo{2.2.2}-octane)zinc(II) tetrahydoborate In tetrahydrofuran for 48h; Ambient temperature;97%
With 1,3-diadamantane-4,5-dihydroimidazole chloride; potassium tert-butylate; bis(pinacol)diborane; copper(l) chloride In toluene at 25℃; for 4h; Schlenk technique; Inert atmosphere;94%
With sodium tetrahydroborate; copper(II) sulfate In methanol at 0 - 5℃; for 1h;92%
874-90-8

4-methoxybenzonitrile

A

3424-93-9

4-methoxyphenylacetamide

B

5373-87-5

4-methoxybenzamidoxime

Conditions
ConditionsYield
With hydroxylamine In ethanol for 3h; Reagent/catalyst; Reflux;A 97%
B n/a
With hydroxylamine hydrochloride; sodium hydroxide In ethanol; water Reflux;
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    Product Name: 4-Methoxybenzamide CAS: 3424-93-9 MF: C8H9NO2 MW: 151.16 EINECS: 222-319-6 Mol File: 3424-93-9.mol 4-Methoxybenzamide Structure 4-Methoxybenzamide Chemical Properties Melting point 164-167 °C (lit.) Boiling p

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Chemistry

Product Name: 4-Methoxybenzamide
The MF of 4-Methoxybenzamide (3424-93-9) is C8H9NO2.

                            
The MW of 4-Methoxybenzamide (3424-93-9) is 151.16.
Synonyms of 4-Methoxybenzamide (3424-93-9): p-Anisamide ; p-Methoxybenzamide
Product Categories: Aromatic Carboxylic Acids,Anilides, Anhydrides & Salts
Form: white crystalline powder
Index of Refraction: 1.546  
EINECS: 222-319-6
Density: 1.143 g/ml 
Flash Point: 161.5 °C 
Boiling Point: 295.8 °C
Melting Point: 164-167 °C
BRN: 1862847 

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mammal (species unspecified) LD50 unreported 1gm/kg (1000mg/kg)   Pharmaceutical Chemistry Journal Vol. 28, Pg. 335, 1994.

Safety Profile

Safety information of 4-Methoxybenzamide (3424-93-9):
Risk Statements 
36/37/38  Irritating to eyes, respiratory system and skin 
Safety Statements 
22  Do not breathe dust
24/25  Avoid contact with skin and eyes
WGK Germany  3
RTECS  CV5466666