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Basic Information
| CAS No.: | 3490-06-0 | ||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Name: | N-methylhomoveratrylamine | ||||||||||||||
| Article Data: | 29 | ||||||||||||||
| Molecular Structure: | |||||||||||||||
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| Formula: | C11H17 N O2 | ||||||||||||||
| Molecular Weight: | 195.261 | ||||||||||||||
| Synonyms: | Phenethylamine,3,4-dimethoxy-N-methyl- (6CI,7CI,8CI);2-(3,4-Dimethoxyphenyl)-N-methylethanamine; 2-(3,4-Dimethoxyphenyl)-N-methylethylamine;3,4-Dimethoxy-N-methylbenzeneethanamine; 3,4-Dimethoxy-N-methylphenethylamine;3,4-Dimethoxy-N-methylphenylethylamine; 3,4-Dimethoxy-b-phenethylmethylamine;Methyl[2-(3,4-dimethoxyphenyl)ethyl]amine; N-(3,4-Dimethoxyphenethyl)-N-methylamine;N-Methyl-2-(3,4-dimethoxyphenyl)ethylamine; N-Methyl-3,4-dimethoxy-b-phenethylamine;N-Methyl-3,4-dimethoxy-b-phenylethylamine; N-Methyl-3,4-dimethoxybenzeneethanamine;N-Methyl-3,4-dimethoxyphenethylamine; N-Methylhomoveratrylamine; N-[2-(3,4-Dimethoxyphenyl)ethyl]-N-methylamine;NSC 187772; [2-(3,4-Dimethoxyphenyl)ethyl]methylamine | ||||||||||||||
| EINECS: | 222-483-9 | ||||||||||||||
| Density: | 1.059 | ||||||||||||||
| Boiling Point: | 294.4°Cat760mmHg | ||||||||||||||
| Flash Point: | >110 ºC | ||||||||||||||
| Hazard Symbols: |
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| Risk Codes: | R36/37/38 | ||||||||||||||
| Safety: |
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| PSA: | 30.49000 | ||||||||||||||
| LogP: | 1.85660 | ||||||||||||||
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Synthetic route
- 40511-15-7
1-(3,4-dimethoxy-phenyl)-2-methylamino-ethanone; hydrochloride
A
- 3490-06-0
N-methylhomoveratrylamine
B
- 5653-66-7
1-(3,4-dimethoxyphenyl)-2-(methylamino)ethan-1-ol
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 1-(3,4-dimethoxy-phenyl)-2-methylamino-ethanone; hydrochloride With hydrogen; 5%-palladium/activated carbon In water at 75℃; under 2585.81 Torr; for 16 - 40h; Stage #2: With sodium hydroxide In water; toluene pH=12; Product distribution / selectivity; | A n/a B 95.1% |
- 14301-36-1
N-[2-(3,4-dimethoxyphenyl)ethyl]formamide
- 3490-06-0
N-methylhomoveratrylamine
Conditions
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran 1) room temperature, 1 h; 2) reflux, 3 h; | 90% |
| With tetrahydrofuran; lithium aluminium tetrahydride | |
| With lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether |
- 75803-23-5
methanesulphonic acid,2-(3,4-dimethoxyphenyl)ethyl ester
- 74-89-5
methylamine
- 3490-06-0
N-methylhomoveratrylamine
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: methanesulphonic acid,2-(3,4-dimethoxyphenyl)ethyl ester; methylamine In methanol; water at 140℃; under 15514.9 Torr; for 0.166667h; Flow reactor; Stage #2: With potassium hydroxide In water | 90% |
- 13230-71-2
N-[2-(3,4-dimethoxyphenyl)ethyl]-2,2,2-trifluoroacetamide
- 74-88-4
methyl iodide
- 3490-06-0
N-methylhomoveratrylamine
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydride In tetrahydrofuran for 4h; Ambient temperature; | 82% |
- 6380-23-0
3,4-dimethoxystyrene
- 3400-11-1
N-methylhydroxylamine-O-sulphonic acid
- 3490-06-0
N-methylhomoveratrylamine
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 3,4-dimethoxystyrene With Schwartz's reagent In tetrahydrofuran at 25℃; Stage #2: N-methylhydroxylamine-O-sulphonic acid In tetrahydrofuran at 50℃; for 0.5h; | 71% |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 2-(3,4-dimethoxyphenyl)-ethylchloride; methylamine In ethanol at 20℃; for 1h; Stage #2: With triisobutylaluminum In ethanol at 60℃; for 32h; | 68% |
- 157370-07-5
(3,4-dimethoxy-phenyl)-thioacetic acid methylamide
- 3490-06-0
N-methylhomoveratrylamine
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride an Blei-Elektroden; |
- 100-52-7
benzaldehyde
- 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine
- 77-78-1
dimethyl sulfate
- 3490-06-0
N-methylhomoveratrylamine
Conditions
| Conditions | Yield |
|---|---|
| With benzene und Erwaermen des Reaktionsprodukts mit wss.Aethanol; |
...Expand
- 100-52-7
benzaldehyde
- 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine
- 74-88-4
methyl iodide
- 3490-06-0
N-methylhomoveratrylamine
Conditions
| Conditions | Yield |
|---|---|
| und Erwaermen des Reaktionsprodukts mit wss.Aethanol; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With palladium; benzene Hydrogenation; |
Downstream Products
