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3567-62-2

Basic Information
CAS No.: 3567-62-2
Name: 1-(3,4-DICHLOROPHENYL)-3-METHYL UREA
Article Data: 9
Molecular Structure:
Molecular Structure of 3567-62-2 (1-(3,4-DICHLOROPHENYL)-3-METHYL UREA)
Formula: C8H8 Cl2 N2 O
Molecular Weight: 219.07
Synonyms: Urea,1-(3,4-dichlorophenyl)-3-methyl- (6CI,7CI,8CI);1-(3,4-Dichlorophenyl)-3-methylurea; 1-Methyl-3-(3,4-dichlorophenyl)urea;3,4-DCPMU; 3-(3,4-Dichlorophenyl)-1-methylurea; DCPMU; Monomethyldiuron;N-(3,4-Dichlorophenyl)-N'-methylurea; N-Demethoxylinuron;N-Methyl-N'-(3,4-dichlorophenyl)urea
Density: 1.411g/cm3
Melting Point: 155.5 °C
Boiling Point: 295.3°Cat760mmHg
Flash Point: 132.4°C
PSA: 41.13000
LogP: 3.20860
Synthetic route
102-36-3

3,4-dichlorophenylisocyanate

74-89-5

methylamine

3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 2h; Substitution;72%
In tetrahydrofuran Addition;
102-36-3

3,4-dichlorophenylisocyanate

74-89-5

methylamine

A

3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

B

100961-22-6

1,5-bis-(3,4-dichloro-phenyl)-3-methyl-biuret

Conditions
ConditionsYield
With benzene
16240-18-9

1-<1-(Cyclohexenyl-(1)>-3-(3,4-dichlor-phenyl)-1-methyl-harnstoff

3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

Conditions
ConditionsYield
With hydrogenchloride

A

34637-13-3

N,N-dimethyl-N'-(3-chloro-4-hydroxy-phenyl)-urea

B

3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

C

69342-26-3

N-(4-chloro-3-hydroxyphenyl)-N',N'-dimethylurea

D

76409-92-2

N-(4,4-dichlorophenyl)-N'-formyl-N'-methylurea

Conditions
ConditionsYield
With Fe(OH)(2+) In water for 4h; pH=3.35; Kinetics; Quantum yield; Further Variations:; Reagents; reagent concentration; Decomposition; Photolysis;
102-36-3

3,4-dichlorophenylisocyanate

3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: toluene
2: aq. HCl
View Scheme
624-83-9

methyl isocyanate

95-76-1

m,p-dichloroaniline

3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

Conditions
ConditionsYield
In di-isopropyl ether
3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

372-09-8

cyanoacetic acid

126381-34-8

1-(2-Cyano-acetyl)-3-(3,4-dichloro-phenyl)-1-methyl-urea

Conditions
ConditionsYield
With acetic anhydride at 60℃; for 3h;46%
3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

298-12-4

Glyoxilic acid

A

134124-32-6

1-(3,4-Dichloro-phenyl)-5-hydroxy-3-methyl-imidazolidine-2,4-dione

B

38655-54-8

3-(3,4-dichloro-phenyl)-5-hydroxy-1-methyl-imidazolidine-2,4-dione

Conditions
ConditionsYield
In chloroform Heating;
3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

126381-37-1

6-Amino-1-(3,4-dichloro-phenyl)-3-methyl-1H-pyrimidine-2,4-dione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 46 percent / acetic anhydride / 3 h / 60 °C
2: 74 percent / 33 percent NaOH / 0.17 h / 80 °C
View Scheme
3567-62-2

3-(3,4-Dichlorophenyl)-1-methylurea

126381-40-6

6-Amino-1-(3,4-dichloro-phenyl)-3-methyl-5-nitroso-1H-pyrimidine-2,4-dione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 46 percent / acetic anhydride / 3 h / 60 °C
2: 63 percent / NaNO2 / H2O / 0.17 h / 95 °C
View Scheme
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    Diuron-desmethyl

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