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35963-20-3

Basic Information
CAS No.: 35963-20-3
Name: (1R)-(-)-10-Camphorsulfonic acid
Article Data: 17
Molecular Structure:
Molecular Structure of 35963-20-3 ((1R)-(-)-10-Camphorsulfonic acid)
Formula: C10H16O4S
Molecular Weight: 232.301
Synonyms: Bicyclo[2.2.1]heptane-1-methanesulfonicacid, 7,7-dimethyl-2-oxo-, (1R)-;(-)-(1R)-7,7-Dimethyl-2-oxobicyclo[2.2.1]heptane-1-methanesulfonic acid;(-)-10-Camphorsulfonic acid;(-)-Camphorsulfonic acid;(1R)-10-Camphorsulfonic acid;(R)-(-)-CSA;(R)-Camphor-10-sulfonic acid;l-10-Camphorsulfonic acid;L-(-) Camphor-10-Sulfonic Acid;
EINECS: 252-817-9
Density: 1.331 g/cm3
Melting Point: 198 °C (dec.)(lit.)
Boiling Point: 467.7°C at 760 mmHg
Flash Point: 236.6°C
Solubility: soluble in water
Appearance: white to light yellow crystal powder
Hazard Symbols: CorrosiveC
Risk Codes: 34
Safety: 26-36/37/39-45-24/25-27
PSA: 79.82000
LogP: 2.35040
Synthetic route
188416-34-4, 137234-71-0

(2R,3S)-2-(2,4-difluorophenyl)-3-(5-fluoro-4-pyrimidinyl)-1-(1H-1,2,4-triazol-1-yl)-2-butanol (1R)-10-camphorsulfonate

35963-20-3

(R)-10-camphorsulfonic acid

Conditions
ConditionsYield
Stage #1: (2R,3S)-2-(2,4-difluorophenyl)-3-(5-fluoro-4-pyrimidinyl)-1-(1H-1,2,4-triazol-1-yl)-2-butanol (1R)-10-camphorsulfonate With potassium carbonate In dichloromethane; water pH=8.9;
Stage #2: In dichloromethane; cyclohexane at 20 - 50℃; for 8h; Reagent/catalyst;
93.2%
357-57-3

brucine

5872-08-2

10-camphorsufonic acid

A

3144-16-9

(1S)-10-camphorsulfonic acid

B

35963-20-3

(R)-10-camphorsulfonic acid

5872-08-2

10-camphorsufonic acid

35963-20-3

(R)-10-camphorsulfonic acid

Conditions
ConditionsYield
With hydrogenchloride; d-phenylglycine
With brucine
35963-20-3

(R)-10-camphorsulfonic acid

brucine salt of/the/ -β-sulfonic acid

brucine salt of/the/ -β-sulfonic acid

35963-20-3

(R)-10-camphorsulfonic acid

Conditions
ConditionsYield
man zerlegt das in der Mutterlauge vom Brucinsalz der d-Saeure vorgekommene Salz mit Barytwasser;
l-camphor

l-camphor

35963-20-3

(R)-10-camphorsulfonic acid

Conditions
ConditionsYield
With sulfuric acid; acetic anhydride
7647-01-0

hydrogenchloride

2935-35-5

(S)-2-phenylglycine

5872-08-2

10-camphorsufonic acid

A

3144-16-9

(1S)-10-camphorsulfonic acid

B

35963-20-3

(R)-10-camphorsulfonic acid

82509-30-6

d-camphor β-sulphonate ammonium salt

35963-20-3

(R)-10-camphorsulfonic acid

Conditions
ConditionsYield
In water; 4-methyl-2-pentanone at 80 - 117℃; Inert atmosphere;
5872-08-2

10-camphorsufonic acid

A

3144-16-9

(1S)-10-camphorsulfonic acid

B

35963-20-3

(R)-10-camphorsulfonic acid

Conditions
ConditionsYield
With barium(II) perchlorate In methanol Solvent; Reagent/catalyst; Resolution of racemate;
35963-20-3

(R)-10-camphorsulfonic acid

59543-81-6

4-(1H-imidazol-1-yl)-2-butanone

1-(3'-oxobutyl)imidazolium (+)-camphor-10-sulfonate

Conditions
ConditionsYield
In dichloromethane at 0℃; for 2h; Inert atmosphere;100%
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    Product Name: (1R)-(-)-10-Camphorsulfonic acid Synonyms: (-)-CAMPHOR-10-SULPHONIC ACID;(-)-CAMPHOR-10-SULFONIC ACID;L-10-(-)-CAMPHOR SULFONIC ACID;L-(-)-CAMPHORSULFONIC ACID;L-(+)-CAMPHOR SULFONIC ACID;L(+)-CAMPHORSULPHONIC ACID;L-CAMPHORSULPHO

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  • Casno:

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    MSDS/COA Download

    (1R)-(-)-10-Camphorsulfonic acid

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Chemistry

Synonyms: (1r)-[7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]methanesulphonic acid;(1R)-(-)-10-CAMPHORSULFONIC ACID; (1R)-(-)-CAMPHOR-10-SULPHONIC ACID;(1R)-(-)-CAMPHOR-10-SULFONIC ACID;(1R)-CAMPHOR-10-SULFONIC ACID;(1R)-(-)-CAMPHORSULFONIC ACID;
(-)-10-CAMPHORSULFONIC ACID;(-)-CAMPHOR-10-SULPHONIC ACID ;(-)-10-CAMPHORSULFONIC ACID;(-)-CAMPHOR-10-SULPHONIC ACID ;
Molecular formula: C10H16O4S
Molecular Weight: 232.3
Molecular Structure :
EINECS: 252-817-9
Melting point: 198 °C (dec.)(lit.)
alpha: -22 o (c=20,H2O)
refractive index : -21.5 ° (C=5, H2O)
storage temp.:2-8°C
Water Solubility:soluble
Sensitive:Hygroscopic

Safety Profile

Hazard Codes:  C
The Risk Statements information of  L(-)-Camphorsulfonic acid:
34:  Causes burns 
The Safety Statements information of  L(-)-Camphorsulfonic acid:
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
27:  Take off immediately all contaminated clothing 
45:  In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) 
24/25:  Avoid contact with skin and eyes 
36/37/39:  Wear suitable protective clothing, gloves and eye/face protection 
RIDADR:UN 3261 8/PG 2
WGK Germany:3
F:3-10
HazardClass:8
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