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39831-55-5

Basic Information
CAS No.: 39831-55-5
Name: 4)]-N1-(4-amino-2-hydroxy-1-oxobutyl)-2-deoxy-, (S)-,sulfate (1:2) (salt)
Molecular Structure:
Molecular Structure of 39831-55-5 (4)]-N1-(4-amino-2-hydroxy-1-oxobutyl)-2-deoxy-, (S)-,sulfate (1:2) (salt))
Formula: C22H43N5O13.2(H2SO4)
Molecular Weight: 781.768
Synonyms: Amikacin disulfate salt;4)]-N1-[(2S)-4-amino-2-hydroxy-1-oxobutyl]-2-deoxy-,sulfate (1:2) (salt) (9CI);Amiglyde V;Amika;Amikacin disulfate;Amikacinsulfate;Amikavet;Amikin;Amiklin;Antibiotic BB-K 8 sulfate;Biklin;Biodacyn;Fabianol;Grasil;Kaminax;Mikavir;Pierami;
EINECS: 254-648-6
Density: N/A
Melting Point: 220-230 °C
Boiling Point: 981.8 °C at 760 mmHg
Flash Point: 547.6 °C
Solubility: H2O: 50 mg/mL, clear, colorless
Appearance: white
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
Transport Information: N/A
PSA: 497.90000
LogP: -4.37610
Synthetic route
37517-28-5

amikacin

39831-55-5

amikacin sulfate

Conditions
ConditionsYield
With sulfuric acid In ethanol; water at 10℃; for 6h; Temperature;91.5%
39831-55-5

amikacin sulfate

1448168-07-7

3-C-azido amikacin

Conditions
ConditionsYield
With imidazole-1-sulfonyl azide hydrochloride In water at 20℃; for 40h; pH=7; regioselective reaction;29%
39831-55-5

amikacin sulfate

37517-28-5

amikacin

Conditions
ConditionsYield
With Amberlite ion exchange resin (OH-form) In water for 1h;
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Chemistry

Molecular Structure of Antibiotic bb-k8 sulfate (CAS NO.39831-55-5):

IUPAC Name: (2S)-4-amino-N-[(1R,2S,3S,4R,5S)-5-amino-2-[(2S,3R,4S,5S,6R)-4-amino-3,5-dihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-4-[(2R,3R,4S,5S,6R)-6-(aminomethyl)-3,4,5-trihydroxyoxan-2-yl]oxy-3-hydroxycyclohexyl]-2-hydroxybutanamide
Product Name: Amikacin disulfate salt
Molecular formula: C22H47N5O21S2
Molecular Weight:  781.76
EINECS: 254-648-6
Melting point:220-230 °C
Flash Point: 547.6 °C
Enthalpy of Vaporization: 162.21 kJ/mol
Boiling Point: 981.8 °C at 760 mmHg
Vapour Pressure: 0 mmHg at 25°C
Storage temp: 2-8°C
Solubility: H2O: 50 mg/mL
InChI
InChI=1/C22H43N5O13.2H2O4S/c23-2-1-8(29)20(36)27-7-3-6(25)18(39-22-16(34)15(33)13(31)9(4-24)37-22)17(35)19(7)40-21-14(32)11(26)12(30)10(5-28)38-21;2*1-5(2,3)4/h6-19,21-22,28-35H,1-5,23-26H2,(H,27,36);2*(H2,1,2,3,4)/t6-,7+,8-,9+,10+,11-,12+,13+,14+,15-,16+,17-,18+,19-,21+,22+;;/m0../s1
Smiles
O([C@H]1[C@@H](C[C@@H]([C@H]([C@@H]1O)O[C@H]1O[C@@H]([C@@H](O)[C@@H]([C@H]1O)O)CN)N)NC([C@H](CCN)O)=O)[C@H]1O[C@@H]([C@@H](O)[C@@H]([C@H]1O)N)CO.S(O)(O)(=O)=O.S(O)(O)(=O)=O
Product Categories: Active Pharmaceutical Ingredients

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
dog LD50 intramuscular > 667mg/kg (667mg/kg)   Pharmacological and Biochemical Properties of Drug Substances. Vol. 1, Pg. 125, 1977.
dog LD50 intravenous 383mg/kg (383mg/kg)   Pharmacological and Biochemical Properties of Drug Substances. Vol. 1, Pg. 125, 1977.
monkey LD50 intramuscular > 1335mg/kg (1335mg/kg)   Pharmacological and Biochemical Properties of Drug Substances. Vol. 1, Pg. 125, 1977.
mouse LD50 intramuscular 1247mg/kg (1247mg/kg) BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY)

BEHAVIORAL: ATAXIA

LUNGS, THORAX, OR RESPIRATION: DYSPNEA
Japanese Journal of Antibiotics. Vol. 39, Pg. 3164, 1986.
mouse LD50 intraperitoneal 2930mg/kg (2930mg/kg)   Japanese Journal of Antibiotics. Vol. 28, Pg. 415, 1975.
mouse LD50 intravenous 181mg/kg (181mg/kg) BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY)

LUNGS, THORAX, OR RESPIRATION: DYSPNEA

BEHAVIORAL: ATAXIA
Japanese Journal of Antibiotics. Vol. 39, Pg. 3164, 1986.
mouse LD50 oral > 10679mg/kg (10679mg/kg)   Pharmacological and Biochemical Properties of Drug Substances. Vol. 1, Pg. 125, 1977.
mouse LD50 subcutaneous 2470mg/kg (2470mg/kg)   Pharmacological and Biochemical Properties of Drug Substances. Vol. 1, Pg. 125, 1977.
rabbit LD50 intramuscular > 3gm/kg (3000mg/kg)   Japanese Journal of Antibiotics. Vol. 28, Pg. 415, 1975.
rabbit LD50 intravenous 248mg/kg (248mg/kg)   Pharmacological and Biochemical Properties of Drug Substances. Vol. 1, Pg. 125, 1977.
rabbit LD50 oral > 3gm/kg (3000mg/kg)   Drugs in Japan Vol. -, Pg. 45, 1990.
rat LD50 intramuscular 2244mg/kg (2244mg/kg) BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY)

BEHAVIORAL: ATAXIA

LUNGS, THORAX, OR RESPIRATION: DYSPNEA
Japanese Journal of Antibiotics. Vol. 39, Pg. 3164, 1986.
rat LD50 intraperitoneal 3500mg/kg (3500mg/kg)   Japanese Journal of Antibiotics. Vol. 28, Pg. 415, 1975.
rat LD50 intravenous 234mg/kg (234mg/kg)   Pharmacological and Biochemical Properties of Drug Substances. Vol. 1, Pg. 125, 1977.
rat LD50 oral > 4gm/kg (4000mg/kg)   Japanese Journal of Antibiotics. Vol. 28, Pg. 415, 1975.
rat LD50 subcutaneous 3604mg/kg (3604mg/kg)   Pharmacological and Biochemical Properties of Drug Substances. Vol. 1, Pg. 125, 1977.

Safety Profile

Poison by intravenous route. Moderately toxic by intraperitoneal and subcutaneous routes. An experimental teratogen. Other experimental reproductive effects. When heated to decomposition it emits very toxic fumes of NOx and SOx. See also sulfates.
Hazard Codes: IrritantXi
The Risk Statements information of Antibiotic bb-k8 sulfate (CAS NO.39831-55-5):
36/37/38:  Irritating to eyes, respiratory system and skin 
The Safety Statements information of  Antibiotic bb-k8 sulfate (CAS NO.39831-55-5) :
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing 
WGK Germany: 2
RTECS: WK1961200
F: 3-10

Specification

  Antibiotic bb-k8 sulfate , with CAS number of 39831-55-5, can be called (2S)-4-amino-N-[(1R,2S,3S,4R,5S)-5-amino-2-(3-amino-3-deoxy-alpha-D-glucopyranosyloxy)-4-(6-amino-6-deoxy-alpha-D-glucopyranosyloxy)-3-hydroxycyclohexyl]-2-hydroxybutanamide disulfate ; (R)-4-amino-N-((1R,2R,3S,4R,5S)-5-amino-2-((3R,4S,5S,6R)-4-amino-3,5-dihydroxy-6-(hydroxymethyl)-tetrahydro-2H-pyran-2-yloxy)-4-((3R,4S,5S,6R)-6-(aminomethyl)-3,4,5-trihydroxy-tetrahydro-2H-pyran-2-yloxy)-3-hydroxycyclohexyl)-2-hydroxybutanamide ; amikacin bis(sulphate) ; Amikacin disulfate salt .

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