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| CAS No.: | 4062-60-6 |
|---|---|
| Name: | N,N'-DI-TERT-BUTYLETHYLENEDIAMINE |
| Article Data: | 15 |
| Molecular Structure: | |
|
|
|
| Formula: | C10H24N2 |
| Molecular Weight: | 172.314 |
| Synonyms: | 1,2-Ethanediamine,N,N'-bis(1,1-dimethylethyl)- (9CI);Ethylenediamine, N,N'-di-tert-butyl-(6CI,7CI,8CI);1,2-Bis(tert-butylamino)ethane;N,N'-Bis(tert-butyl)ethylenediamine;N,N'-Di-tert-butyl-1,2-ethanediamine;N,N'-Di-tert-butyl-1,2-ethylenediamine;N,N'-Di-tert-butyl-1,4-diazabutane; |
| EINECS: | 223-769-6 |
| Density: | 0.815 g/cm3 |
| Melting Point: | 53.35°C |
| Boiling Point: | 208.7 °C at 760 mmHg |
| Flash Point: | 76.7 °C |
| Appearance: | COLORLESS TO YELLOW LIQUID |
| Hazard Symbols: |
 C
|
| Risk Codes: | 34 |
| Safety: | 26-36/37/39-45 |
| Transport Information: | UN 2735 8/PG 2 |
| PSA: | 24.06000 |
| LogP: | 2.54440 |
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- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 43224-75-52,2,6,6-Tetramethyl-4-(2-propyleneoxy) Piperidine
- 28227-42-1, 30834-74-3
1,4-di-tert-butyl-1,4-diazabutadiene
- 4062-60-6
N,N'-di-tert-butylethylenediamine
| Conditions | Yield |
|---|---|
| With lithium aluminium tetrahydride at 0 - 20℃; | 89% |
| With sodium tetrahydroborate In methanol at 0 - 25℃; Inert atmosphere; |
- 30834-74-3
N-((E,2E)-2-{[(E)-1,1-dimethylethyl]imino}ethylidene)-2-methyl-2-propanamine
- 4062-60-6
N,N'-di-tert-butylethylenediamine
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In ethanol for 3h; | 81% |
| Conditions | Yield |
|---|---|
| In hexane; water for 72h; Heating; | 72% |
| In water 1.) 0 deg C to ambient temperature (slowly), 2.) reflux, overnight; | 70% |
| Stage #1: ethylene dibromide; tert-butylamine With sodium hydroxide In water at 0℃; for 1h; Stage #2: In water at 25℃; for 72h; | 56% |
| With water |
- 106-93-4
ethylene dibromide
- 75-64-9
tert-butylamine
A
- 4062-60-6
N,N'-di-tert-butylethylenediamine
B
- 24426-18-4
1,4,7-tri-tert-butyl-1,4,7-triazaheptane
C
- 10125-77-6
1,4-di-tert-butylpiperazine
| Conditions | Yield |
|---|---|
| In water at 20℃; for 72h; | A 70% B 2% C 9% |
- 30834-74-3
N-((E,2E)-2-{[(E)-1,1-dimethylethyl]imino}ethylidene)-2-methyl-2-propanamine
A
- 4062-60-6
N,N'-di-tert-butylethylenediamine
B
- 117203-10-8
1-tert-Butyl-3-(tert-butylamino)pyrrol
C
- 117203-11-9
1-tert-Butyl-3,4-bis(tert-butylamino)pyrrol
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In ethanol for 1.5h; | A 8% B 30% C 24% |
| Conditions | Yield |
|---|---|
| With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 24h; |
- 4062-60-6
N,N'-di-tert-butylethylenediamine
- 89437-94-5
1,3-di-tert-butyl-2-chloro-1,3,2-diazaphospholidine
| Conditions | Yield |
|---|---|
| With triethylamine; phosphorus trichloride In toluene at 20℃; for 2h; | 100% |
| With phosphorus trichloride In benzene 1) 18h, r.t., 2) reflux, 24h; | 87% |
| With triethylamine; phosphorus trichloride In toluene at 0 - 20℃; Inert atmosphere; Glovebox; Schlenk technique; | 81% |
- 4062-60-6
N,N'-di-tert-butylethylenediamine
- 4495-50-5, 22687-37-2
1,2-bis(t-butylamino)ethane dihydrochloride
| Conditions | Yield |
|---|---|
| With hydrogenchloride In ethanol; water | 100% |
| With hydrogenchloride In ethanol |
- 4062-60-6
N,N'-di-tert-butylethylenediamine
| Conditions | Yield |
|---|---|
| With water-d2 In dimethylsulfoxide-d6 at 25℃; for 1h; Inert atmosphere; | 100% |
| With deuteromethanol at 20℃; for 1h; | 98% |
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Chemistry
Chemistry informtion about N,N-Di-Tert-Butylethylenediamine (CAS NO.4062-60-6) is:
IUPAC Name: N,N'-Ditert-Butylethane-1,2-Diamine
Synonyms: 1,2-Ethanediamine, N,N'-Bis(1,1-Dimethylethyl)- ; Ar81242 ; N,N’-Bis(1,1-Dimethylethyl)-1,2-Ethanediamine ; N,N’-Bis(1,1-Dimethylethyl)-2-Ethanediamine ; N,N'-Di-Tert-Butylethylenediamine ; N,N-Di-Tert-Butylethylenediamine ; N,N'-Di-T-Butyl Ethylene Diamine ; 1,2-Bis(Tert-Butylamino)Ethane
MF: C10H24N2
MW: 172.31
EINECS: 223-769-6
Density: 0.815 g/cm3
Flash Point: 76.7 °C
Boiling Point: 208.7 °C at 760 mmHg
Vapour Pressure: 0.21 mmHg at 25°C
Enthalpy of Vaporization: 44.5 kJ/mol
Refractive Index: n20/D 1.43(lit.)
BRN: 1738432
Following is the molecular structure of N,N-Di-Tert-Butylethylenediamine (CAS NO.4062-60-6) is:
Toxicity Data With Reference
| 1. | skn-rbt 500 µL/24H MLD | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) OTS0535667 . | ||
| 2. | orl-rat LDLo:5 g/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) OTS0535667 . | ||
| 3. | skn-rbt LDLo:200 mg/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) OTS0535667 . |
Safety Profile
A poison by ingestion. Low toxicity by ingestion. A mild skin irritant. When heated to decomposition it emits toxic vapors of NOx.
Hazard Codes:
C
Risk Statements:
R34:Causes burns.
Safety Statements:
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
S45:In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
RIDADR: UN 2735 8/PG 2
WGK Germany: 3
RTECS: KH8587137
F:
F 10 Keep under argon.
F 34 Sensitive to CO2.
HazardClass: 8
PackingGroup: II