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40851-62-5

Basic Information
CAS No.: 40851-62-5
Name: METHYL O-TOLYLACETATE
Article Data: 47
Molecular Structure:
Molecular Structure of 40851-62-5 (METHYL O-TOLYLACETATE)
Formula: C10H12 O2
Molecular Weight: 164.204
Synonyms: 2-Methylphenylaceticacid methyl ester; Methyl 2-methylphenylacetate; Methyl o-tolylacetate
Density: 1.035g/cm3
Boiling Point: 229.8°Cat760mmHg
Flash Point: 101.9°C
Safety:
Safety Statements 23-24/25
PSA: 26.30000
LogP: 1.71050
Synthetic route
67-56-1

methanol

644-36-0

o-methylphenylacetic acid

40851-62-5

methyl o-tolylacetate

Conditions
ConditionsYield
With sulfuric acid at 0℃; for 8h; Reflux; Inert atmosphere;100%
With sulfuric acid for 6.5h; Inert atmosphere; Reflux;99%
With sulfuric acid at 28℃; for 12h;98%
644-36-0

o-methylphenylacetic acid

40851-62-5

methyl o-tolylacetate

Conditions
ConditionsYield
With sulfuric acid In methanol98%
With sulfuric acid In methanol98%
With sulfuric acid In formic acid for 6h; Reflux;
552-45-4

1-chloromethyl-2-methylbenzene

40851-62-5

methyl o-tolylacetate

Conditions
ConditionsYield
94%
67-56-1

methanol

577-16-2, 122382-54-1

2-Methylacetophenone

40851-62-5

methyl o-tolylacetate

Conditions
ConditionsYield
With sulfuric acid; trimethyl orthoformate at 20℃; for 0.333333h;91%
67-56-1

methanol

577-16-2, 122382-54-1

2-Methylacetophenone

149-73-5

trimethyl orthoformate

40851-62-5

methyl o-tolylacetate

Conditions
ConditionsYield
With iodine; silver nitrate for 5h; Heating;90%
1202873-25-3

1-methoxycarbonylmethyl-2-methyl-2,5-cyclohexadiene-1-carboxylic acid

40851-62-5

methyl o-tolylacetate

Conditions
ConditionsYield
With chlorosulfonic acid In dichloromethane at 0℃; for 0.166667h;87%
67-56-1

methanol

201230-82-2

carbon monoxide

89-95-2

2-methyl-benzyl alcohol

616-38-6

carbonic acid dimethyl ester

40851-62-5

methyl o-tolylacetate

Conditions
ConditionsYield
With palladium(II) trifluoroacetate; 1,3-bis-(diphenylphosphino)propane at 135℃; under 15001.5 Torr; for 24h; Autoclave; Green chemistry;81%
67-56-1

methanol

577-16-2, 122382-54-1

2-Methylacetophenone

A

40851-62-5

methyl o-tolylacetate

B

97728-46-6

2-methoxy-1-(2-methylphenyl)ethanone

Conditions
ConditionsYield
With [bis(acetoxy)iodo]benzene at 60℃; for 1h;A 62%
B 13%
644-36-0

o-methylphenylacetic acid

40851-62-5

methyl o-tolylacetate

Conditions
ConditionsYield
In diethyl ether
14736-50-6

o-(methoxycarbonylmethyl)benzoic acid

40851-62-5

methyl o-tolylacetate

Conditions
ConditionsYield
(i) furan-2-carbonyl chloride, Et3N, (ii) H2, Pd(OH)2-BaSO4; Multistep reaction;
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