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Basic Information
CAS No.: 40932-60-3
Name: 3,5,6-Trichlorosalicylic acid
Article Data: 9
Molecular Structure:
Molecular Structure of 40932-60-3 (3,5,6-Trichlorosalicylic acid)
Formula: C7H3Cl3O3
Molecular Weight: 241.458
Synonyms: Salicylicacid, 3,5,6-trichloro- (7CI);2,3,5-Trichloro-6-hydroxybenzoic acid;3,5,6-Trichloro-2-hydroxybenzoic acid;3,5,6-Trichlorosalicylic acid;
EINECS: 255-144-9
Density: 1.772 g/cm3
Melting Point: 209-211 °C(lit.)
Boiling Point: 335 °C at 760 mmHg
Flash Point: 156.4 °C
Solubility: It has limited solubility in water.
Appearance: white grey solid powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-37/39
PSA: 57.53000
LogP: 3.05060
Related products
Synthetic route
320-72-9

3,5-dichlorosalicylic acid

40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
With sulfuric acid; iodine; chlorine at 70℃;93%
With sulfuric acid; iodine; chlorine at 40 - 70℃; for 6h;81%
With sulfuric acid; chlorine
320-72-9

3,5-dichlorosalicylic acid

A

87-87-6

2,3,5,6-tetrachlorobenzene-1,4-diol

B

40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

C

118-75-2

chloranil

D

tri(3,5,6-trichlorosalicylide)

Conditions
ConditionsYield
With sulfuric acid; chlorine at 80 - 90℃; for 15h;A 3.5%
B 44%
C 10.8%
D 19%
With sulfuric acid; chlorine at 80 - 90℃; for 15h;A 3.5%
B 44%
C 10.8%
D n/a
...Expand
7664-93-9

sulfuric acid

320-72-9

3,5-dichlorosalicylic acid

7782-50-5

chlorine

40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

...Expand
321-14-2

5-chloro-2-hydroxybenzoic acid

40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chlorine / acetic acid / Ambient temperature
2: 81 percent / 65percent oleum, iodine, chlorine / 6 h / 40 - 70 °C
View Scheme
89-55-4

5-bromosalicyclic acid

A

2200-85-3

5-bromo-3-chloro-2-hydroxybenzoic acid

B

4-bromo-3,6-dichlorosalicylic acid

C

40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
With trichloroisocyanuric acid; sulfuric acid; iodine at 0 - 70℃; for 5h;
...Expand
69-72-7

salicylic acid

A

2200-85-3

5-bromo-3-chloro-2-hydroxybenzoic acid

B

40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: bromine; sulfuric acid / 1 h / 20 - 60 °C
2: iodine; trichloroisocyanuric acid; sulfuric acid / 5 h / 0 - 70 °C
View Scheme
Multi-step reaction with 2 steps
1: bromine; sulfuric acid / 1 h / 20 °C
2: iodine; trichloroisocyanuric acid; sulfuric acid / 5 h / 0 - 70 °C
View Scheme
Multi-step reaction with 2 steps
1: bromine; sulfuric acid; acetic acid / 0.5 h / 30 - 60 °C
2: iodine; trichloroisocyanuric acid; sulfuric acid / 5 h / 0 - 70 °C
View Scheme
Multi-step reaction with 2 steps
1: bromine; sulfuric acid; acetic acid / 2 h / 30 °C
2: iodine; trichloroisocyanuric acid; sulfuric acid / 5 h / 0 - 70 °C
View Scheme
89-55-4

5-bromosalicyclic acid

40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chlorine; sulfuric acid / 8.5 h / 3 - 45 °C
2: chlorine; iodine; sulfuric acid / 3.5 h / 5 - 35 °C
View Scheme
69-72-7

salicylic acid

40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: bromine; sulfuric acid / 1.5 h / 3 - 25 °C
2: chlorine; sulfuric acid / 8.5 h / 3 - 45 °C
3: chlorine; iodine; sulfuric acid / 3.5 h / 5 - 35 °C
View Scheme
2200-85-3

5-bromo-3-chloro-2-hydroxybenzoic acid

A

4-bromo-3,6-dichlorosalicylic acid

B

40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

C

3-bromo-6-((3-bromo-2,5-dichloro-6-hydroxybenzoyl)oxy)-2,5-dichlorobenzoic acid

Conditions
ConditionsYield
With sulfuric acid; iodine; chlorine at 5 - 35℃; for 3.5h;
...Expand
40932-60-3

3,5,6-Trichloro-2-hydroxybenzoic acid

100-49-2

cyclohexylmethyl alcohol

C14H15Cl3O3

Conditions
ConditionsYield
titanium (IV) oxide bis(2,4-pentanedionate) In xylene Reflux;99%
Raw Materials
320-72-9
321-14-2
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