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CAS No.: | 4097-88-5 | ||||||||||
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Name: | N-METHYL-2,2'-DIAMINODIETHYLAMINE | ||||||||||
Article Data: | 10 | ||||||||||
Molecular Structure: | |||||||||||
Formula: | C5H15 N3 | ||||||||||
Molecular Weight: | 117.194 | ||||||||||
Synonyms: | 1,2-Ethanediamine,N-(2-aminoethyl)-N-methyl- (9CI); Diethylenetriamine, 4-methyl- (6CI,7CI,8CI);1,5-Diamino-3-methyl-3-azapentane; 1,5-Diamino-N'-methyl-3-azapentane;2,2'-Diamino-N-methyldiethylamine; 4-Methyl-1,4,7-triazaheptane;4-Methyldiethylenetriamine; Bis(2-aminoethyl)methylamine;N,N-Bis(2-aminoethyl)methylamine; N,N-Bis(b-aminoethyl)methylamine; N-(2-Aminoethyl)-N-methyl-1,2-ethanediamine;N-(2-Aminoethyl)-N-methylethylenediamine; N2-Methyldiethylenetriamine;N'-Methyl-2,2'-diaminodiethylamine; N'-Methyldiethylenetriamine | ||||||||||
Density: | 0,91 g/cm3 | ||||||||||
Boiling Point: | 84 °C / 14mmHg | ||||||||||
Flash Point: | 84°C | ||||||||||
Risk Codes: | 34 | ||||||||||
Safety: |
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PSA: | 55.28000 | ||||||||||
LogP: | 0.23620 |
N-methyliminodiacetonitrile
A
1-methyl-piperazine
B
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With hydrogen In methanol at 120 - 600℃; under 15001.5 Torr; Temperature; Solvent; Reagent/catalyst; | A 92.4% B 6.8% |
N1-(2-aminoethyl)-N1-methylethane-1,2-diamine trihydrochloride
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With sodium methylate In methanol at 0 - 5℃; for 3h; Large scale; | 88% |
N,N di(dimethyl-2,5 pyrolido-2 ethyl), N methylamine
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 80℃; for 96h; Heating; | 26% |
N,N'-(3-methyl-3-aza-pentanediyl)-bis-benzenesulfonamide
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
(i) phthalimide , (ii) aq. HCl; Multistep reaction; |
phthalimide
N-Methyldiethanolamine
A
1,5-diamino-3-azamethylpentane
B
N-(2-hydroxyethyl)-N-methylethylenediamine
Conditions | Yield |
---|---|
With hydrogenchloride; water 1.) 100 deg C, 4 h; 2.) 90 deg C, 50 h; Yield given. Multistep reaction; | |
With hydrogenchloride; water 1.) 100 deg C, 4 h; 2.) 90 deg C, 50 h; Multistep reaction; |
mechlorethamine hydrochloride
A
1-methyl-piperazine
B
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With ammonia; sodium carbonate In water-d2 Title compound not separated from byproducts; |
1,5-diamino-3-azamethylpentane
Tert-butyl isocyanate
bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 96.2% |
4,7-dichloroquinoline
1,5-diamino-3-azamethylpentane
N1-(2-aminoethyl)-N2-(7-chloroquinolin-4-yl)-N1-methylethane-1,2-diamine
Conditions | Yield |
---|---|
In neat (no solvent) at 125℃; for 2h; | 95% |
at 90 - 135℃; for 4h; | 92% |
at 70℃; | 57% |
In neat (no solvent) at 90℃; Inert atmosphere; | 57% |
With potassium phosphate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 90℃; for 17h; Inert atmosphere; | 1.39 g |
Conditions | Yield |
---|---|
at 20℃; Cooling with ice; | 94% |