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411235-57-9

Basic Information
CAS No.: 411235-57-9
Name: Cyclopropylboronic acid
Article Data: 13
Molecular Structure:
Molecular Structure of 411235-57-9 (Cyclopropylboronic acid)
Formula: C3H7BO2
Molecular Weight: 85.8984
Synonyms: Cyclopropylbronic acid;Cyclopropylboronic acid,monohydrate;Boronic acid, cyclopropyl- (9ci);
EINECS: 609-890-0
Density: 1.11 g/cm3
Melting Point: 90-95 °C(lit.)
Boiling Point: 205.1 °C at 760 mmHg
Flash Point: 77.9 °C
Appearance: white powder
Hazard Symbols: HarmfulXn
Risk Codes: 22
Safety: 26-36
PSA: 40.46000
LogP: -0.37680
Synthetic route
74-85-1

ethene

formyl boronic acid

3,5-dinitro-p-toluenesulfonylhydrazide

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
Stage #1: formyl boronic acid; 3,5-dinitro-p-toluenesulfonylhydrazide In methanol Reflux;
Stage #2: With n-butyllithium In tetrahydrofuran at 0℃; for 0.5h;
Stage #3: ethene Reagent/catalyst; Solvent; Further stages;
92%
75927-49-0

pinacol vinylboronate

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
Stage #1: diazomethane; pinacol vinylboronate With palladium diacetate In tert-butyl methyl ether Inert atmosphere;
Stage #2: With sodium periodate In tetrahydrofuran; water at 20℃; for 0.05h; Reagent/catalyst; Temperature;
86%
75-11-6

diiodomethane

75927-49-0

pinacol vinylboronate

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
Stage #1: diiodomethane; pinacol vinylboronate With diethylzinc at 60℃; for 12h; Inert atmosphere;
Stage #2: With 2,2'-iminobis[ethanol] at 55℃; for 4h; Solvent; Temperature; Reagent/catalyst;
82%

tricyclopropylboroxin

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
In water at 20℃; for 1h; Reagent/catalyst;77%
23719-80-4

cyclopropylmagnesium bromide

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
Stage #1: cyclopropylmagnesium bromide With Trimethyl borate In tetrahydrofuran at -78 - 20℃; for 7h;
Stage #2: With hydrogenchloride for 1h;
56%
1104637-36-6

cyclopropylboronic acid methyliminodiacetic acid ester

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
With sodium hydroxide In tetrahydrofuran; water at 23℃; for 0.333333h;53%
121-43-7

Trimethyl borate

23719-80-4

cyclopropylmagnesium bromide

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
Stage #1: Trimethyl borate; cyclopropylmagnesium bromide In tetrahydrofuran at -78 - 20℃;
Stage #2: With hydrogenchloride In tetrahydrofuran; water
27%
1404118-58-6

C5H11BO2

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
With hydrogenchloride; water for 1h;
1104637-36-6

cyclopropylboronic acid methyliminodiacetic acid ester

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
In not given hydrolysis of appropriate N-methyliminodiacetic acid boronate;
1065010-87-8

potassium cyclopropyltrifluoroborate

411235-57-9

cyclopropylboronic acid

Conditions
ConditionsYield
With glass or DBU or Cs2CO3 In tetrahydrofuran; water Kinetics; hydrolysis at 55°C in THF/H2O in the presence of glass powder or DBU or Cs2CO3; not isolated;
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    CAS RN.: 411235-57-9 Molecular Weight: 85.8975 Molecular Formula: C3H7BO

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Chemistry

The Molecular Structure of Cyclopropylboronic acid (CAS NO.411235-57-9):

Empirical Formula: C3H7BO2
Molecular Weight: 85.8975 
Nominal Mass: 86 Da
Average Mass: 85.8975 Da
Monoisotopic Mass: 86.05391 Da 
Index of Refraction: 1.442
Molar Refractivity: 20.4 cm3
Molar Volume: 76.9 cm3
Surface Tension: 34.5 dyne/cm
Density: 1.11 g/cm3
Flash Point: 77.9 °C
Enthalpy of Vaporization: 51.35 kJ/mol
Boiling Point: 205.1 °C at 760 mmHg
Vapour Pressure: 0.0606 mmHg at 25°C
Melting Point: 90-95°C
Storage temp: Store below -20°C 
Product Categories: BORONICACID;blocks;BoronicAcids;Boronic Acids & Esters;Cyclopropyl;Organoborons;Boronic acid;CHIRAL CHEMICALS;Boronic Acids & Esters;Ring Systems;Alkyl;Boronic Acids;Boronic Acids and Derivatives 

Safety Profile

Hazard Codes: HarmfulXn
Risk Statements: 22 
R22: Harmful if swallowed
Safety Statements: 26-36 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
S36: Wear suitable protective clothing
WGK Germany: 3
HazardClass: IRRITANT, IRRITANT-HARMFUL

Specification

 Cyclopropylboronic acid (CAS NO.411235-57-9) can be called as Cyclopropylboronic acid,monohydrate ; Boronic acid, cyclopropyl- (9ci) ; Cyclopropylboronic ; cyclopropylboronic acid 95% .