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CAS No.: | 41317-15-1 |
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Name: | Methoxymethyldiphenylamine |
Article Data: | 20 |
Molecular Structure: | |
Formula: | C14H15NO |
Molecular Weight: | 213.279 |
Synonyms: | p-Anisidine,2-methyl-N-phenyl- (6CI);2-Methyl-4-methoxydiphenylamine;3-Methoxy-6-anilinotoluene;4-Methoxy-2-methyl-N-phenylaniline;4-Methoxy-2-methyldiphenylamine;6-Anilino-3-methoxytoluene;N-(2-Methyl-4-methoxyphenyl)aniline; |
EINECS: | 255-310-0 |
Density: | 1.089 g/cm3 |
Melting Point: | 80-83 °C |
Boiling Point: | 344.6 °C at 760 mmHg |
Flash Point: | 140.1 °C |
Solubility: | 16.79mg/L at 25℃ |
Hazard Symbols: | Xn |
Risk Codes: | 22-36 |
Safety: | 26 |
PSA: | 21.26000 |
LogP: | 3.82020 |
1-chloro-4-methoxy-2-methylbenzene
aniline
4-phenylamino-3-methyl-1-methoxybenzene
Conditions | Yield |
---|---|
With potassium phosphate; aniline; triphenylphosphine; tris(dibenzylideneacetone)dipalladium (0) at 184℃; for 8h; Buchwald-Hartwig amination; | 96% |
With potassium phosphate; DavePhos; tris-(dibenzylideneacetone)dipalladium(0) at 184℃; | 96% |
methanol
1-methyl-2-nitrobenzene
phenol
4-phenylamino-3-methyl-1-methoxybenzene
Conditions | Yield |
---|---|
Stage #1: methanol; 1-methyl-2-nitrobenzene With 3 % platinum on carbon; hydrogen In water at 50℃; under 750.075 Torr; for 8h; Autoclave; Inert atmosphere; Stage #2: phenol With 3 % platinum on carbon In cyclohexanone at 250℃; under 7500.75 Torr; for 2h; Autoclave; Inert atmosphere; | 95.4% |
4-bromo-3-methylanisole
Acetanilid
4-phenylamino-3-methyl-1-methoxybenzene
Conditions | Yield |
---|---|
Stage #1: Acetanilid With sodium methylate In 1-methyl-pyrrolidin-2-one at 100℃; Stage #2: 4-bromo-3-methylanisole In 1-methyl-pyrrolidin-2-one at 20 - 40℃; for 1.25h; Stage #3: In 1-methyl-pyrrolidin-2-one; methanol at 100℃; for 1h; Reagent/catalyst; Temperature; Solvent; | 95.3% |
Conditions | Yield |
---|---|
With potassium hydroxide; bis(tri-t-butylphosphine)palladium(0); cetyltrimethylammonim bromide In water; toluene at 90℃; for 0.25h; | 95% |
With caesium carbonate; aniline; DavePhos; tris(dibenzylideneacetone)dipalladium (0) at 184℃; for 8h; Buchwald-Hartwig amination; | 93% |
With caesium carbonate; triphenylphosphine; tris-(dibenzylideneacetone)dipalladium(0) at 184℃; | 93% |
chlorobenzene
2-methyl-4-methoxyaniline
4-phenylamino-3-methyl-1-methoxybenzene
Conditions | Yield |
---|---|
With potassium phosphate; DavePhos; tris(dibenzylideneacetone)dipalladium (0) In toluene at 110℃; for 8h; Buchwald-Hartwig amination; | 95% |
With potassium phosphate; DavePhos; tris-(dibenzylideneacetone)dipalladium(0) In toluene Heating; | 95% |
bromobenzene
2-methyl-4-methoxyaniline
4-phenylamino-3-methyl-1-methoxybenzene
Conditions | Yield |
---|---|
With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris(dibenzylideneacetone)dipalladium (0) In toluene at 110℃; Buchwald-Hartwig amination; | 95% |
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium(0) In toluene Heating; | 95% |
With potassium phosphate; copper(l) iodide; C18H15N3O2 at 25℃; for 24h; Reagent/catalyst; Temperature; Sealed tube; | 93% |
With potassium phosphate; copper(l) iodide In diethylene glycol at 70℃; for 14h; Sealed tube; | 93% |
Conditions | Yield |
---|---|
A n/a B 94% |
4-phenylamino-3-methyl-1-methoxybenzene
Conditions | Yield |
---|---|
With methanol Reagent/catalyst; | 90.99% |
In methanol at 60 - 180℃; for 20h; Sealed tube; Large scale; | 85.6% |
bromobenzene
N-(4-methoxy-2-methylphenyl)acetamide
copper
A
4-phenylamino-3-methyl-1-methoxybenzene
B
3-methoxy-6-(N-acetylanilino) toluene
Conditions | Yield |
---|---|
With iodine; potassium carbonate | A n/a B 90.5% |
phenylhydrazine
2-methyl-4-methoxyaniline
4-phenylamino-3-methyl-1-methoxybenzene
Conditions | Yield |
---|---|
With cobalt(II) phthalocyanine; copper(l) chloride In dichloromethane at 10℃; | 86% |
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Molecular Formula:C14H15NO
Molecular Weight:213.28
EINECS:255-310-0
Density:1.089g/cm3
Melting Point:80-83 °C
Boiling Point:171 °C / 4mmHg
Flash Point:140.1°C
4-Methoxy-2-Methyldiphenylamine's Synonyms: ACME;4-METHOXY-2-METHYLDIPHENYLAMINE;2-METHYL-4-METHOXYDIPHENYLAMINE;methoxymethyldiphenylamine;ANMT/DPA;MMD;4-methoxy-N-phenyl-o-toluidine;2-methyl-4-methoxy diphenylamine C14H15NO
These products are toxic carbon oxides (CO, CO 2), nitrogen oxides (NO, NO2).
Fire Fighting Mediaand Instructions:Small fire: Use dry chemical powder.
Large fire: Use water spray, fog or foam. do not use water jet.