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41317-15-1

Basic Information
CAS No.: 41317-15-1
Name: Benzenamine,4-methoxy-2-methyl-N-phenyl-
Article Data: 20
Cas Database
Molecular Structure:
Molecular Structure of 41317-15-1 (Benzenamine,4-methoxy-2-methyl-N-phenyl-)
Formula: C14H15NO
Molecular Weight: 213.279
Synonyms: p-Anisidine,2-methyl-N-phenyl- (6CI);2-Methyl-4-methoxydiphenylamine;3-Methoxy-6-anilinotoluene;4-Methoxy-2-methyl-N-phenylaniline;4-Methoxy-2-methyldiphenylamine;6-Anilino-3-methoxytoluene;N-(2-Methyl-4-methoxyphenyl)aniline;
EINECS: 255-310-0
Density: 1.089 g/cm3
Melting Point: 80-83 °C
Boiling Point: 344.6 °C at 760 mmHg
Flash Point: 140.1 °C
Solubility: N/A
Appearance: N/A
Hazard Symbols: Xn
Risk Codes: 22-36
Safety: 26
Transport Information: N/A
PSA: 21.26000
LogP: 3.82020
Synthetic route
13334-71-9

1-chloro-4-methoxy-2-methylbenzene

62-53-3

aniline

41317-15-1

4-phenylamino-3-methyl-1-methoxybenzene

Conditions
ConditionsYield
With potassium phosphate; aniline; triphenylphosphine; tris(dibenzylideneacetone)dipalladium (0) at 184℃; for 8h; Buchwald-Hartwig amination;96%
With potassium phosphate; DavePhos; tris-(dibenzylideneacetone)dipalladium(0) at 184℃;96%
67-56-1

methanol

88-72-2

1-methyl-2-nitrobenzene

108-95-2

phenol

41317-15-1

4-phenylamino-3-methyl-1-methoxybenzene

Conditions
ConditionsYield
Stage #1: methanol; 1-methyl-2-nitrobenzene With 3 % platinum on carbon; hydrogen In water at 50℃; under 750.075 Torr; for 8h; Autoclave; Inert atmosphere;
Stage #2: phenol With 3 % platinum on carbon In cyclohexanone at 250℃; under 7500.75 Torr; for 2h; Autoclave; Inert atmosphere;
95.4%
27060-75-9

4-bromo-3-methylanisole

103-84-4

Acetanilid

41317-15-1

4-phenylamino-3-methyl-1-methoxybenzene

Conditions
ConditionsYield
Stage #1: Acetanilid With sodium methylate In 1-methyl-pyrrolidin-2-one at 100℃;
Stage #2: 4-bromo-3-methylanisole In 1-methyl-pyrrolidin-2-one at 20 - 40℃; for 1.25h;
Stage #3: In 1-methyl-pyrrolidin-2-one; methanol at 100℃; for 1h; Reagent/catalyst; Temperature; Solvent;
95.3%
27060-75-9

4-bromo-3-methylanisole

62-53-3

aniline

41317-15-1

4-phenylamino-3-methyl-1-methoxybenzene

Conditions
ConditionsYield
With potassium hydroxide; bis(tri-t-butylphosphine)palladium(0); cetyltrimethylammonim bromide In water; toluene at 90℃; for 0.25h;95%
With caesium carbonate; aniline; DavePhos; tris(dibenzylideneacetone)dipalladium (0) at 184℃; for 8h; Buchwald-Hartwig amination;93%
With caesium carbonate; triphenylphosphine; tris-(dibenzylideneacetone)dipalladium(0) at 184℃;93%
108-90-7

chlorobenzene

102-50-1

2-methyl-4-methoxyaniline

41317-15-1

4-phenylamino-3-methyl-1-methoxybenzene

Conditions
ConditionsYield
With potassium phosphate; DavePhos; tris(dibenzylideneacetone)dipalladium (0) In toluene at 110℃; for 8h; Buchwald-Hartwig amination;95%
With potassium phosphate; DavePhos; tris-(dibenzylideneacetone)dipalladium(0) In toluene Heating;95%
108-86-1

bromobenzene

102-50-1

2-methyl-4-methoxyaniline

41317-15-1

4-phenylamino-3-methyl-1-methoxybenzene

Conditions
ConditionsYield
With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris(dibenzylideneacetone)dipalladium (0) In toluene at 110℃; Buchwald-Hartwig amination;95%
With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium(0) In toluene Heating;95%
With potassium phosphate; copper(l) iodide; C18H15N3O2 at 25℃; for 24h; Reagent/catalyst; Temperature; Sealed tube;93%
With potassium phosphate; copper(l) iodide In diethylene glycol at 70℃; for 14h; Sealed tube;93%
102-50-1

2-methyl-4-methoxyaniline

A

41317-15-1

4-phenylamino-3-methyl-1-methoxybenzene

B

108-95-2

phenol

Conditions
ConditionsYield
A n/a
B 94%

2-(4-methoxy-2-methylphenylamino)benzoic acid

41317-15-1

4-phenylamino-3-methyl-1-methoxybenzene

Conditions
ConditionsYield
With methanol Reagent/catalyst;90.99%
In methanol at 60 - 180℃; for 20h; Sealed tube; Large scale;85.6%
100-63-0

phenylhydrazine

102-50-1

2-methyl-4-methoxyaniline

41317-15-1

4-phenylamino-3-methyl-1-methoxybenzene

Conditions
ConditionsYield
With cobalt(II) phthalocyanine; copper(l) chloride In dichloromethane at 10℃;86%
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Chemistry

Molecular Formula:C14H15NO
Molecular Weight:213.28
EINECS:255-310-0
Density:1.089g/cm3
Melting Point:80-83 °C
Boiling Point:171 °C / 4mmHg
Flash Point:140.1°C
4-Methoxy-2-Methyldiphenylamine's Synonyms: ACME;4-METHOXY-2-METHYLDIPHENYLAMINE;2-METHYL-4-METHOXYDIPHENYLAMINE;methoxymethyldiphenylamine;ANMT/DPA;MMD;4-methoxy-N-phenyl-o-toluidine;2-methyl-4-methoxy diphenylamine C14H15NO

Uses

4-Methoxy-2-methyldiphenylamine is a synthetic organic chemical used in the production of black color formers

Safety Profile

These products are toxic carbon oxides (CO, CO 2), nitrogen oxides (NO, NO2).
Fire Fighting Mediaand Instructions:Small fire: Use dry chemical powder.
Large fire: Use water spray, fog or foam. do not use water jet.

Specification

4-Methoxy-2-Methyldiphenylamine's handling and storage
Keep away from HEAT. Mechanical exhaust required. When not in use, tightly seal the container and store in a dry, cool
place. Avoid excessive HEAT and light. Do not breathe dust.
Always store away from incompatible compounds such as oxidizing agents.
4-Methoxy-2-Methyldiphenylamine's Hazards Identification
Acute Health Effects:No specific information is available in our data base regarding the toxic effects of this material for humans. However,exposure to any chemical should be kept to a minimum. Skin and eye contact may result in irritation. May be harmful if inhaled or ingested. Always follow safe industrial hygiene practices and wear proper protective equipment when handling
this compound.Follow safe industrial hygiene practices and always wear proper protective equipment when handling this compound.