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CAS No.: | 4316-33-0 |
---|---|
Name: | 1-methoxy-4-(trimethoxymethyl)benzene |
Article Data: | 10 |
Molecular Structure: | |
Formula: | C11H16O4 |
Molecular Weight: | 212.246 |
Synonyms: | 4-Methoxy-orthobenzoesaeure-trimethylester;p-Methoxybenzoic acid methyl orthoester;1-methoxy-4-trimethoxymethyl-benzene;trimethyl p-methoxyorthobenzoate;Trimethyl ortho-p-anisate;Ortho-p-anisic acid,trimethyl ester;trimethyl 4-methoxyorthobenzoate;trimethyl p-methoxyortobenzoate; |
Density: | 1.065g/cm3 |
Boiling Point: | 244.9°Cat760mmHg |
Flash Point: | 82.1°C |
PSA: | 36.92000 |
LogP: | 1.74470 |
methanol
p-Anisaldehyde dimethyl acetal
A
p-Methoxybenzoic acid methyl orthoester
B
methyl 4-methoxybenzoate
Conditions | Yield |
---|---|
With sodium methylate; lithium perchlorate; Tris(2,4-dibromophenyl)amine In dichloromethane indirect electrochemical oxidation; | A 78.3% B 13.2% |
With sodium methylate; potassium benzenesulfonate; Tris(2,4-dibromophenyl)amine | A 53% B 18.4% |
p-Methoxybenzoic acid methyl orthoester
Conditions | Yield |
---|---|
With silver nitrate; triethylamine In methanol; acetonitrile for 10h; Ambient temperature; | 53% |
methanol
Estragole
A
p-Methoxybenzoic acid methyl orthoester
B
1-(1,1-Dimethoxy-allyl)-4-methoxy-benzene
Conditions | Yield |
---|---|
With sodium methylate at 30℃; for 0.5h; electrolysis; | A 3 % Chromat. B 34 % Chromat. |
methanol
[Dimethoxy-(4-methoxy-phenyl)-methyl]-methyl-phenyl-amine
A
p-Methoxybenzoic acid methyl orthoester
B
N-methylaniline
Conditions | Yield |
---|---|
With acetic acid for 0.166667h; Yield given; |
methanol
anethole
A
p-Anisaldehyde dimethyl acetal
B
p-Methoxybenzoic acid methyl orthoester
Conditions | Yield |
---|---|
With sodium 2,2,2-trifluoroacetate electrooxidation: current 0.8 A, current density 150 mA/cm2, 5F/mole; | A 76 % Chromat. B 11 % Chromat. |
methanol
anethole
A
p-Anisaldehyde dimethyl acetal
B
p-Methoxybenzoic acid methyl orthoester
1-(1,2-Dimethoxy-propyl)-4-methoxy-benzene
1-(1,2-Dimethoxy-propyl)-4-methoxy-benzene
Conditions | Yield |
---|---|
With sodium methylate at 30℃; for 0.75h; Product distribution; electrolysis; other time, other alkenyl phenol ethers; |
Conditions | Yield |
---|---|
With sodium methylate at 30℃; for 0.75h; electrolysis; | 11 % Chromat. |
4-methoxy-N-methyl-N-phenylbenzamide.
p-Methoxybenzoic acid methyl orthoester
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 2: 1.) sodium / 1.) - 2.) CH2Cl2, 30 min 3: glacial acetic acid / 0.17 h View Scheme |
p-Methoxybenzoic acid methyl orthoester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) sodium / 1.) - 2.) CH2Cl2, 30 min 2: glacial acetic acid / 0.17 h View Scheme |