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4360-63-8

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Basic Information
CAS No.: 4360-63-8
Name: 2-Bromomethyl-1,3-dioxolane
Article Data: 28
Molecular Structure:
Molecular Structure of 4360-63-8 (2-Bromomethyl-1,3-dioxolane)
Formula: C4H7BrO2
Molecular Weight: 167.002
Synonyms: Acetaldehyde,bromo-, cyclic ethylene acetal (6CI);2-(2-Bromomethyl)-1,3-dioxolane;2-(Bromomethyl)-1,3-dioxolane;2-Bromomethyldioxolane;Bromoacetaldehydeethylene acetal;Bromoacetaldehyde ethylene glycol acetal;Bromoacetaldehydeethylene ketal;
EINECS: 224-443-6
Density: 1.589 g/cm3
Boiling Point: 178.7 °C at 760 mmHg
Flash Point: 62.8 °C
Solubility: Immiscible with water.
Appearance: clear colorless liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-24/25
PSA: 18.46000
LogP: 0.75420
Related products
Synthetic route
497-26-7

2-methyl-1,3-dioxolane

4360-63-8

2-bromomethyl-1,3-dioxolane

Conditions
ConditionsYield
With bromine; di-tert-butyldicyclohexano-18-crown-18 In benzene at 20℃; for 0.166667h; Bromination;96%
With 1,4-Dioxane Dibromide In tetrachloromethane at 29.9℃; Rate constant; Thermodynamic data; Mechanism; ΔH(excit.), ΔS(excit.), ΔG(excit.), lg A; further temp., kinetics;
7252-83-7

1-bromo-2,2-dimethoxyethane

107-21-1

ethylene glycol

4360-63-8

2-bromomethyl-1,3-dioxolane

Conditions
ConditionsYield
With Dowex 50(H+) at 120℃; for 1h;94%
With Dowex-x8 (H+) resin75%
With sulfuric acid
With potassium bisulfite; methoxybenzene at 140℃;15 g
at 150℃;
107-21-1

ethylene glycol

2032-35-1

Bromoacetaldehyde diethyl acetal

4360-63-8

2-bromomethyl-1,3-dioxolane

Conditions
ConditionsYield
With toluene-4-sulfonic acid at 110℃; for 2h;87%
With sulfuric acid
at 150℃;
107-21-1

ethylene glycol

75-07-0

acetaldehyde

4360-63-8

2-bromomethyl-1,3-dioxolane

Conditions
ConditionsYield
Stage #1: ethylene glycol; acetaldehyde at 20℃; for 0.5h; Large scale;
Stage #2: With bromine at 0 - 3℃; for 3.5h; Temperature; Large scale;		79.2%
497-26-7

2-methyl-1,3-dioxolane

A

4360-63-8

2-bromomethyl-1,3-dioxolane

B

927-68-4

bromoethyl acetate

Conditions
ConditionsYield
With bromine In tetrachloromethane at 60 - 70℃;A 45%
B 45%
With N-Bromosuccinimide; di-tert-butylcyclohexano-18-crown-6 In benzene Ambient temperature;A 32 % Chromat.
B 68 % Chromat.
108-05-4

vinyl acetate

107-21-1

ethylene glycol

4360-63-8

2-bromomethyl-1,3-dioxolane

Conditions
ConditionsYield
With bromine
6304-35-4

bis-(1,2-dibromo-ethyl) ether

107-21-1

ethylene glycol

A

4360-63-8

2-bromomethyl-1,3-dioxolane

B

540-51-2

2-bromoethanol

...Expand
107-21-1

ethylene glycol

17157-48-1

bromoacetaldehyde

4360-63-8

2-bromomethyl-1,3-dioxolane

2032-35-1

Bromoacetaldehyde diethyl acetal

4360-63-8

2-bromomethyl-1,3-dioxolane

107-21-1

ethylene glycol

ω.ω'-dibromo-paraldehyde

ω.ω'-dibromo-paraldehyde

4360-63-8

2-bromomethyl-1,3-dioxolane

Conditions
ConditionsYield
With sulfuric acid
Raw Materials
6304-35-4
497-26-7
107-21-1
2032-35-1
108-05-4
7252-83-7
17157-48-1
Downstream Products
52509-14-5
57366-77-5
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    4360-63-8

    2-Bromomethyl-1,3-dioxolane

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