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Basic Information
CAS No.: 460-00-4
Name: 4-Bromofluorobenzene
Molecular Structure:
Molecular Structure of 460-00-4 (4-Bromofluorobenzene)
Formula: C6H4BrF
Molecular Weight: 175
Synonyms: 1-Bromo-4-fluorobenzene;1-Fluoro-4-bromobenzene;4-Bromo-1-fluorobenzene;Benzene,1-bromo-4-fluoro-;4-Bromophenyl fluoride;4-Fluoro-1-bromobenzene;4-Fluorobenzene bromide;NSC 10268;NSC 9460;p-Bromofluorobenzene;p-Fluorophenyl bromide;
EINECS: 207-300-2
Density: 1.593 g/cm3
Melting Point: -16 °C
Boiling Point: 154.5 °C at 760 mmHg
Flash Point: 49.3 °C
Solubility: Soluble in water(0.14g/L).
Appearance: White to pale yellow crystalline powder
Hazard Symbols: HarmfulXn,FlammableF,IrritantXi,ToxicT
Risk Codes: 10-36/37/38-20-39-23/24/25-11-20/21/22
Safety: 26-36-37/39-16-45-36/37-7
Transport Information: UN 1993 3/PG 3
PSA: 0.00000
LogP: 2.58820
Synthetic route
462-06-6

fluorobenzene

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
With carbon dioxide; bromine at 40℃; under 187519 Torr; for 2h; Supercritical conditions; Green chemistry;100%
With N-Bromosuccinimide; boron trifluoride at 20℃; for 1h;96%
With tribromo-isocyanuric acid In trifluoroacetic acid at 20℃; for 0.5h;74%
823-85-8

4-fluorophenyhydrazine hydrochloride

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
With boron tribromide; dimethyl sulfoxide at 80℃; for 1h;99%
106-41-2

4-bromo-phenol

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
With 1,3-bis(2,6-diisopropylphenyl)-2,2-difluoro-2,3-dihydro-1h-imidazole; cesium fluoride; diphenylzinc In toluene at 80℃; for 20h; Product distribution / selectivity; Sealed vial;95%
With 1,3-bis(2,6-diisopropylphenyl)-2,2-difluoro-2,3-dihydro-1h-imidazole; cesium fluoride In toluene at 23 - 80℃; for 18.5h; Inert atmosphere;88 %Spectr.
459-45-0

4-fluorobenzenediazonium tetrafluoroborate

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
With dibenzo-18-crown-6; N,N,N,N,-tetramethylethylenediamine; potassium bromide; copper(I) bromide; copper(ll) bromide In acetonitrile at 20℃; for 1h; Sandmeyer Reaction;94%
With (triphenylphosphine)gold(I) chloride; sodium bromide In acetonitrile at 50℃; for 5h; Sandmeyer Reaction;81 %Spectr.
With Bromotrichloromethane; tetrabutylammonium perchlorate In N,N-dimethyl-formamide at 20℃; for 3h; Sandmeyer Reaction; Electrochemical reaction;37 %Spectr.
With lithium bromide In acetonitrile at 20℃; for 0.5h; Catalytic behavior; Reagent/catalyst; Time; Sandmeyer Reaction; Inert atmosphere;96 %Spectr.

C14H13BrN3Pol

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
With tetrafluoroboric acid diethyl ether In tetradecafluorohexane at 100℃; for 1h; Balz-Schiemann reaction; Autoclave; solid phase reaction;88%
371-40-4

4-fluoroaniline

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
Stage #1: 4-fluoroaniline With boron trifluoride diethyl etherate; lithium bromide In acetonitrile at 0℃; for 0.166667h;
Stage #2: With tert.-butylnitrite In acetonitrile at 0 - 20℃; for 1h;
82%
Stage #1: 4-fluoroaniline With Bromotrichloromethane; sodium nitrite In dichloromethane; water at 23℃; for 0.0833333h;
Stage #2: With acetic acid In dichloromethane; water at 23℃; for 1h;
51%
106-37-6

1.4-dibromobenzene

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
Stage #1: 1.4-dibromobenzene With n-butyllithium In tetrahydrofuran; hexane at 0℃; Flow reactor;
Stage #2: With N-fluorobis(benzenesulfon)imide In tetrahydrofuran; hexane at 0℃; Flow reactor;
78%
106-37-6

1.4-dibromobenzene

A

108-86-1

bromobenzene

B

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
Stage #1: 1.4-dibromobenzene With n-butyllithium In tetrahydrofuran; hexane at 0℃; Flow reactor;
Stage #2: With 2-fluoro-3,3-dimethyl-2,3-dihydro-1,2-benzisothiazole-1,1-dioxide In tetrahydrofuran; hexane at 0℃; Flow reactor;
A 13%
B 76%
5467-74-3

4-Bromophenylboronic acid

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
Stage #1: 4-Bromophenylboronic acid With sodium hydroxide In methanol at 23℃; for 0.25h; Inert atmosphere;
Stage #2: With silver trifluoromethanesulfonate In methanol at 0℃; for 0.5h; Inert atmosphere;
Stage #3: With Selectfluor In acetone at 23℃; for 1h; Inert atmosphere; Molecular sieve; regiospecific reaction;
73%
With cesium fluoroxysulphate In methanol at 0℃; for 24h;20 % Spectr.
Multi-step reaction with 2 steps
1: diethyl ether / 20 °C / Inert atmosphere; Molecular sieve
2: silver fluoride; (tBuCN)2Cu*OTf; 1-fluoro-2,4,6-trimethylpyridinium hexafluorophosphate / tetrahydrofuran / 18 h / 50 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: methanol; water / 14 h / 23 °C
2: 2,2':6,2''-terpyridine; [(terpy)Pd(MeCN)][BF4]2; sodium fluoride; 1-chloromethyl-4-fluoro-1,4-diazoniabicyclo[2.2.2]octanebis(tetrafluoroborate) / acetonitrile / 15 h / 40 °C
View Scheme
Stage #1: 4-Bromophenylboronic acid With C27H23N4O6PdS; potassium carbonate In methanol; benzene at 23℃; for 3.5h;
Stage #2: With Selectfluor In acetonitrile at 50℃; for 0.5h;
12.8 mg
1063716-78-8

Pd(C5H5N)(C13H8N2SO2C6H4NO2)(C6H4Br)

460-00-4

1-Bromo-4-fluorobenzene

Conditions
ConditionsYield
Stage #1: Pd(C5H5N)(C13H8N2SO2C6H4NO2)(C6H4Br) With Selectfluor In acetonitrile at 50℃; for 0.5h;
Stage #2: With pyridine In acetonitrile at 23℃; Product distribution / selectivity;
73%
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  • 4-bromofluorobenzene CAS NO.460-00-4

  • Casno:

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    4-bromofluorobenzene CAS NO.460-00-4

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Specification

4-Bromofluorobenzene,  its cas register number is 460-00-4. It also can be called 1-bromo-4-fluoro-benzen; 1-Fluoro-4-bromobenzene; 4-Bromfluorbenzol; 4-Fluorbrombenzol; 4-Fluoro-1-bromobenzene; 4-Fluorophenyl bromide; 4-fluorophenylbromide; Benzene, 1-bromo-4-fluoro. 4-Bromofluorobenzene(CAS NO.460-00-4) is a clear colorless liquid and belongs to the Organic chemicals and Derivatives.  4-Bromofluorobenzene is used in pharmaceutical, pesticide synthesis.

Physical properties about 4-Bromofluorobenzene are: (1)ACD/LogP: 2.976; (2)ACD/LogD (pH 5.5): 2.98; (3)ACD/LogD (pH 7.4): 2.98; (4)ACD/BCF (pH 5.5): 107.65; (5)ACD/BCF (pH 7.4): 107.65; (6)ACD/KOC (pH 5.5): 991.10; (7)ACD/KOC (pH 7.4): 991.10; (8)Index of Refraction: 1.53; (9)Molar Refractivity: 33.937 cm3; (10)Molar Volume: 109.828 cm3; (11)Polarizability: 13.454 10-24cm3; (12)Surface Tension: 33.8409996032715 dyne/cm; (13)Density: 1.593 g/cm3; (14)Flash Point: 49.29 °C; (15)Enthalpy of Vaporization: 37.515 kJ/mol; (16)Boiling Point: 154.505 °C at 760 mmHg; (17)Vapour Pressure: 4.07100009918213 mmHg at 25°C

When you are using this chemical, please be cautious about it as the following:
1. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice;
2. Wear suitable protective clothing, gloves and eye/face protection;
3. Keep away from sources of ignition - No smoking;
4. In case of accident or if you feel unwell, seek medical advice immediately (show label where possible);
5. Wear suitable protective clothing and gloves;
6. Keep container tightly closed;

You can still convert the following datas into molecular structure:
(1)InChI=1S/C6H4BrF/c7-5-1-3-6(8)4-2-5/h1-4H;
(2)InChIKey=AITNMTXHTIIIBB-UHFFFAOYSA-N; (
3)Smilesc1(ccc(Br)cc1)F;

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
rat LC50 inhalation 18gm/m3/4H (18000mg/m3) BEHAVIORAL: CHANGES IN MOTOR ACTIVITY (SPECIFIC ASSAY)

BEHAVIORAL: TREMOR

LUNGS, THORAX, OR RESPIRATION: DYSPNEA
National Technical Information Service. Vol. OTS0540496,
rat LD50 oral 2700mg/kg (2700mg/kg) BEHAVIORAL: CHANGES IN MOTOR ACTIVITY (SPECIFIC ASSAY)

BEHAVIORAL: TREMOR

BEHAVIORAL: ATAXIA
National Technical Information Service. Vol. OTS0540497,