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462-34-0

Basic Information
CAS No.: 462-34-0
Name: Boron trifluoride tetrahydrofuran complex
Molecular Structure:
Molecular Structure of 462-34-0 (Boron trifluoride tetrahydrofuran complex)
Formula: C4H8BF3O
Molecular Weight: 139.913
Synonyms: Furan,tetrahydro-, compd. with BF3 (1:1) (7CI);Furan, tetrahydro-, compd. with BF3(6CI);Furan, tetrahydro-, compd. with boron fluoride (BF3) (1:1) (8CI);Furan,tetrahydro-, compd. with trifluoroborane (1:1);Borane, trifluoro-, compd. withtetrahydrofuran (1:1);Boron fluoride (BF3), compd. with tetrahydrofuran (1:1)(8CI);Boron fluoride, compd. with tetrahydrofuran;Boron trifluoride-THFcomplex (1:1);Boron trifluoride-tetrahydrofuran complex (1:1);Borontrifluoride-tetrahydrofuran compound;Trifluoro(tetrahydrofuran)boron;
EINECS: 207-325-9
Density: 1.268 g/cm3
Melting Point: 12 °C
Boiling Point: 68.3 °C at 760 mmHg
Flash Point: 92 °C
Solubility: hydrolysis with water
Appearance: Colorless to light yellow liquid
Hazard Symbols: CorrosiveC, ToxicT
Risk Codes: 34-48/23-35-20/22
Safety: 26-27-36/37/39-45-28A-23-28
Transport Information: UN 3265 8/PG 2
PSA: 17.07000
LogP: 1.67660
Synthetic route
462-34-0

boron trifluoride-tetrahydrofuran complex

1-[(76)Br]bromo-2-phenylethyne

Conditions
ConditionsYield
With peracetic acid; ammonium 76Br-bromide; ammonia In methanol; water at 20℃; for 0.166667h;80%
462-34-0

boron trifluoride-tetrahydrofuran complex

115-77-5

Pentaerythritol

C5H8B2F2O4

Conditions
ConditionsYield
Stage #1: boron trifluoride-tetrahydrofuran complex; Pentaerythritol In acetonitrile at 20℃; for 1h;
Stage #2: With chloro-trimethyl-silane In acetonitrile at 80℃; for 10h; Reagent/catalyst; Temperature;
96%
15097-49-1

N-trimethylsilylpyrrolidine

462-34-0

boron trifluoride-tetrahydrofuran complex

7783-60-0

sulfur tetrafluoride

pyrrolidinodifluorosulfiniumtetrafluoroborate

Conditions
ConditionsYield
Stage #1: N-trimethylsilylpyrrolidine; sulfur tetrafluoride In dichloromethane at -78 - 20℃; Inert atmosphere;
Stage #2: boron trifluoride-tetrahydrofuran complex In dichloromethane at 20 - 25℃; for 2h; Inert atmosphere;
85%
Stage #1: N-trimethylsilylpyrrolidine; sulfur tetrafluoride In dichloromethane at -65 - 20℃; Inert atmosphere;
Stage #2: boron trifluoride-tetrahydrofuran complex In dichloromethane at 25℃; for 2h; Inert atmosphere;
85%
462-34-0

boron trifluoride-tetrahydrofuran complex

7783-60-0

sulfur tetrafluoride

17890-34-5

N-(trimethylsilyl)phenyl(methyl)amine

N-methyl-N-phenylaminodifluorosulfiniumtetrafluoroborate

Conditions
ConditionsYield
Stage #1: sulfur tetrafluoride; N-(trimethylsilyl)phenyl(methyl)amine In dichloromethane at -78 - 20℃; Inert atmosphere;
Stage #2: boron trifluoride-tetrahydrofuran complex In dichloromethane at 20 - 25℃; for 2.16667h; Inert atmosphere;
93%
Stage #1: sulfur tetrafluoride; N-(trimethylsilyl)phenyl(methyl)amine In dichloromethane at -70 - 20℃; Inert atmosphere;
Stage #2: boron trifluoride-tetrahydrofuran complex In dichloromethane at 25℃; for 2.16667h; Inert atmosphere;
93%
462-34-0

boron trifluoride-tetrahydrofuran complex

7783-60-0

sulfur tetrafluoride

92982-38-2

N-trimethylsilyl-N-methyl-2-aminopyridine

N-methyl-N-(2-pyridyl)aminodifluorosulfinium tetrafluoroborate

Conditions
ConditionsYield
Stage #1: sulfur tetrafluoride; N-trimethylsilyl-N-methyl-2-aminopyridine In dichloromethane at -78 - 20℃; Inert atmosphere;
Stage #2: boron trifluoride-tetrahydrofuran complex In dichloromethane at 20 - 21℃; for 1.58333h; Inert atmosphere;
78%
Stage #1: sulfur tetrafluoride; N-trimethylsilyl-N-methyl-2-aminopyridine In dichloromethane at -70 - 20℃; Inert atmosphere;
Stage #2: boron trifluoride-tetrahydrofuran complex In dichloromethane at 21℃; for 1.58333h; Inert atmosphere;
78%
462-34-0

boron trifluoride-tetrahydrofuran complex

38078-09-0

diethylamino-sulfur trifluoride

ethanaminium,N-(difluoro-λ4-sulfanylidene)-N-ethyl-,tetrafluoroborate

Conditions
ConditionsYield
In diethyl ether at 20 - 30℃; for 1.25h; Inert atmosphere;85%
13368-42-8

4-(trimethylsilyl)morpholine

462-34-0

boron trifluoride-tetrahydrofuran complex

7783-60-0

sulfur tetrafluoride

difluoro-4-morpholinylsulfonium tetrafluoroborate

Conditions
ConditionsYield
Stage #1: 4-(trimethylsilyl)morpholine; sulfur tetrafluoride In dichloromethane at -78 - 20℃; Inert atmosphere;
Stage #2: boron trifluoride-tetrahydrofuran complex In dichloromethane at 25℃; for 4h; Inert atmosphere;
92%
462-34-0

boron trifluoride-tetrahydrofuran complex

7783-60-0

sulfur tetrafluoride

996-50-9

N,N-diethyl-1,1,1-trimethylsilanamine

ethanaminium,N-(difluoro-λ4-sulfanylidene)-N-ethyl-,tetrafluoroborate

Conditions
ConditionsYield
Stage #1: sulfur tetrafluoride; N,N-diethyl-1,1,1-trimethylsilanamine In dichloromethane at -78 - 20℃; Inert atmosphere;
Stage #2: boron trifluoride-tetrahydrofuran complex In dichloromethane at 15 - 25℃; for 1.5h; Inert atmosphere;
89%
462-34-0

boron trifluoride-tetrahydrofuran complex

7783-60-0

sulfur tetrafluoride

14884-70-9

N-Methyl-N-(trimethylsilyl)benzylamin

N-benzyl-N-methylaminodifluorosulfinium tetrafluoroborate

Conditions
ConditionsYield
Stage #1: sulfur tetrafluoride; N-Methyl-N-(trimethylsilyl)benzylamin In dichloromethane at -78 - 20℃; Inert atmosphere;
Stage #2: boron trifluoride-tetrahydrofuran complex In dichloromethane at 20 - 25℃; for 1.16667h; Inert atmosphere;
73%
462-34-0

boron trifluoride-tetrahydrofuran complex

553-91-3

lithium oxalate

lithium oxalate-boron trifluoride

Conditions
ConditionsYield
at 23℃; for 24h;94.7%
at 23℃; for 24h;94.7%
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Chemistry

IUPAC Name: Oxolane; trifluoroborane
Synonyms of Boron trifluoride tetrahydrofuran complex (CAS NO.462-34-0): EINECS 207-325-9 ; Boron, trifluoro(tetrahydrofuran)-, (T-4)- ; Trifluoro(tetrahydrofuran)boron
CAS NO: 462-34-0
Molecular Formula of Boron trifluoride tetrahydrofuran complex (CAS NO.462-34-0): C4H8BF3O
Molecular Weight: 139.9119
Molecular Structure:

Melting Point: −123 °C
ProductCategories: Furan&Benzofuran ; Boron ; BoronSynthetic Reagents ; Catalysis and Inorganic Chemistry ; Chemical Synthesis ; Lewis Acids 
Polar Surface Area: 9.23 Å2 
Enthalpy of Vaporization: 29.81 kJ/mol
Boiling Point of Boron trifluoride tetrahydrofuran complex (CAS NO.462-34-0): 68.3 °C at 760 mmHg
Vapour Pressure: 152 mmHg at 25°C

Safety Profile

Hazard Codes: CorrosiveC,ToxicT
Risk Statements: 34-48/23-35-20/22 
R34: Causes burns. 
R48: Danger of serious damage to health by prolonged exposure. 
R23: Toxic by inhalation. 
R35: Causes severe burns. 
R20/22: Harmful by inhalation and if swallowed.
Safety Statements: 26-27-36/37/39-45-23-28 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S27: Take off immediately all contaminated clothing. 
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection. 
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) . 
S23: Do not breathe vapour. 
S28: After contact with skin, wash immediately with plenty of soap-suds.
RIDADR: UN 3265 8/PG 2
WGK Germany: 1
Hazard Note: Toxic/Corrosive
HazardClass: 8
PackingGroup: II